CN104342268A - Fire resistant hydraulic oil and preparation method thereof - Google Patents

Fire resistant hydraulic oil and preparation method thereof Download PDF

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Publication number
CN104342268A
CN104342268A CN201410522798.6A CN201410522798A CN104342268A CN 104342268 A CN104342268 A CN 104342268A CN 201410522798 A CN201410522798 A CN 201410522798A CN 104342268 A CN104342268 A CN 104342268A
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CN
China
Prior art keywords
hydraulic oil
fire resistant
parts
resistant hydraulic
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410522798.6A
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Chinese (zh)
Inventor
杨龙兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuxi Yanggong Machinery Manufacturing Co Ltd
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Wuxi Yanggong Machinery Manufacturing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wuxi Yanggong Machinery Manufacturing Co Ltd filed Critical Wuxi Yanggong Machinery Manufacturing Co Ltd
Priority to CN201410522798.6A priority Critical patent/CN104342268A/en
Publication of CN104342268A publication Critical patent/CN104342268A/en
Pending legal-status Critical Current

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Abstract

The invention provides fire resistant hydraulic oil. The fire resistant hydraulic oil comprises the following components in parts by mass: 980-992 parts of 150N third type base oil, 2-5 parts of sulfurized polyisobutene, 5-6 parts of benzotriazole, 1.2-1.5 parts of sodium tripolyphosphate, 0.5-0.8 part of triazole fatty acid amine salt, 0.08-0.12 part of di-iso-octyldiphenylamine, a proper amount of demulsifier and 0.7-0.9 part of ethylenediamine tetraacetic acid. The invention also provides a preparation method of the hydraulic oil. The fire resistant hydraulic oil has good high temperature and low temperature stability, can be widely used in ironmaking, steelmaking, pressure casting, continuous casting, hot rolling, coal mining and glass product processing and in the hydraulic systems of various equipment which is close to heat sources and has fire dangers, such as excavators, is simple in preparation method, has good lubricating property, also has good abrasion resistance and causes small damages to oil pumps and hydraulic valves.

Description

A kind of fire resistant hydraulic oil and preparation method thereof
Technical field
The present invention relates to a kind of fire resistant hydraulic oil.
Background technology
Hydrostatic transmission be by means of the liquid pressure that is in encloses container can transmission carry out operation element parts, because its volume is little, quality light, be quick on the draw, transmit steady, easy for installation, easy handling, thus the switch telechirics etc. of the steering wheel of boats and ships, windlass, navigationsystem and valve is widely used in, pressure medium is the medium of transferring energy in hydrostatic transmission, plays the vital role such as transferring energy, lubrication equipment, antiseptic and rustproof and cooling in hydraulic efficiency installation.If oil pump is the heart of whole hydraulic efficiency system, so pressure medium is exactly the blood of hydraulic efficiency system, and it plays vital effect to the working reliability of hydraulic efficiency system and life-span.A large amount of facts shows, the hydraulic fault of more than 70% is caused by working medium, and therefore, selecting properly and use pressure medium are all of great significance the serviceability and working reliability, security and prolongs life cycle that improve hydraulic efficiency system.The fire resistant hydraulic oil the most extensively adopted is at present water-ethylene glycol liquid, but it in use exists corroding metal and the problem such as oilness is bad.
Summary of the invention
The invention provides a kind of fire resistant hydraulic oil, there is good fire-resistant effect; For this reason, the present invention also provides its preparation method.
The invention provides a kind of fire resistant hydraulic oil, described fire resistant hydraulic oil is made up of each component of following mass fraction: 150N tri-class base oil 980-992 part, sulfurized polyisobutylene 2-5 part, benzotriazole 5-6 part, tripoly phosphate sodium STPP 1.2-1.5 part, 124 Triazole lipid acid amine salt 0.5-0.8 part, di-iso-octyldiphenylamine 0.08-0.12 part, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.7-0.9 part.
Preferably, described fire resistant hydraulic oil is made up of each component of following mass fraction: 150N tri-class base oil 986 parts, sulfurized polyisobutylene 4 parts, benzotriazole 5.5 parts, tripoly phosphate sodium STPP 1.4 parts, 0.6 part, 124 Triazole lipid acid amine salt, di-iso-octyldiphenylamine 0.1 part, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.8 part.
The present invention also provides the preparation method of above-mentioned fire resistant hydraulic oil, and step is as follows:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 45-50 DEG C, stir 35-40min;
(2) add all the other components of formula ratio, stir 15-20min, be cooled to room temperature, filter and get final product.
Fire resistant hydraulic oil of the present invention has good high-temperature stability and low-temperature stability, can be widely used in the hydraulic efficiency system close to the various equipment of thermal source, fire-prone such as ironmaking, steel-making, die casting, continuous casting, hot rolling, colliery, glasswork processing and excavator.Fire resistant hydraulic oil preparation method of the present invention is simple, lubricity good, meanwhile, has good abrasion resistance, damages little to oil pump and hydraulicvalve.
Embodiment
Following embodiment is convenient to understand the present invention better, but does not limit the present invention.Experimental technique in following embodiment, if no special instructions, is ordinary method.
embodiment 1
The formula of fire resistant hydraulic oil of the present invention is as follows:
150N tri-class base oil 986kg, sulfurized polyisobutylene 4kg, benzotriazole 5.5kg, tripoly phosphate sodium STPP 1.4kg, 124 Triazole lipid acid amine salt 0.6kg, di-iso-octyldiphenylamine 0.1kg, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.8kg.
The preparation method of fire resistant hydraulic oil of the present invention is:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 48 DEG C, stir 38min;
(2) add all the other components of formula ratio, stir 18min, be cooled to room temperature, filter and get final product.
embodiment 2
The formula of fire resistant hydraulic oil of the present invention is as follows:
150N tri-class base oil 980kg, sulfurized polyisobutylene 5kg, benzotriazole 5kg, tripoly phosphate sodium STPP 1.2kg, 124 Triazole lipid acid amine salt 0.8kg, di-iso-octyldiphenylamine 0.12kg, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.9kg.
The preparation method of fire resistant hydraulic oil of the present invention is:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 45 DEG C, stir 40min;
(2) add all the other components of formula ratio, stir 15min, be cooled to room temperature, filter and get final product.
embodiment 3
The formula of fire resistant hydraulic oil of the present invention is as follows:
150N tri-class base oil 992kg, sulfurized polyisobutylene 2kg, benzotriazole 6kg, tripoly phosphate sodium STPP 1.5kg, 124 Triazole lipid acid amine salt 0.5kg, di-iso-octyldiphenylamine 0.08kg, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.7kg.
The preparation method of fire resistant hydraulic oil of the present invention is:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 50 DEG C, stir 35min;
(2) add all the other components of formula ratio, stir 20min, be cooled to room temperature, filter and get final product.
embodiment 4
The formula of fire resistant hydraulic oil of the present invention is as follows:
150N tri-class base oil 988kg, sulfurized polyisobutylene 3kg, benzotriazole 5.8kg, tripoly phosphate sodium STPP 1.3kg, 124 Triazole lipid acid amine salt 0.7kg, di-iso-octyldiphenylamine 0.11kg, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.9kg.
The preparation method of fire resistant hydraulic oil of the present invention is:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 47 DEG C, stir 36min;
(2) add all the other components of formula ratio, stir 19min, be cooled to room temperature, filter and get final product.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (3)

1. a fire resistant hydraulic oil, is characterized in that: described fire resistant hydraulic oil is made up of each component of following mass fraction: 150N tri-class base oil 980-992 part, sulfurized polyisobutylene 2-5 part, benzotriazole 5-6 part, tripoly phosphate sodium STPP 1.2-1.5 part, 124 Triazole lipid acid amine salt 0.5-0.8 part, di-iso-octyldiphenylamine 0.08-0.12 part, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.7-0.9 part.
2. fire resistant hydraulic oil according to claim 1, is characterized in that: described fire resistant hydraulic oil is made up of each component of following mass fraction: 150N tri-class base oil 986 parts, sulfurized polyisobutylene 4 parts, benzotriazole 5.5 parts, tripoly phosphate sodium STPP 1.4 parts, 0.6 part, 124 Triazole lipid acid amine salt, di-iso-octyldiphenylamine 0.1 part, emulsion splitter are appropriate, ethylenediamine tetraacetic acid (EDTA) 0.8 part.
3. the preparation method of the fire resistant hydraulic oil described in claim 1 or 2, is characterized in that: step is as follows:
(1) by the 150N tri-class base oil of formula ratio, benzotriazole, tripoly phosphate sodium STPP, emulsion splitter mixing, be heated to 45-50 DEG C, stir 35-40min;
(2) add all the other components of formula ratio, stir 15-20min, be cooled to room temperature, filter and get final product.
CN201410522798.6A 2014-10-08 2014-10-08 Fire resistant hydraulic oil and preparation method thereof Pending CN104342268A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410522798.6A CN104342268A (en) 2014-10-08 2014-10-08 Fire resistant hydraulic oil and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410522798.6A CN104342268A (en) 2014-10-08 2014-10-08 Fire resistant hydraulic oil and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104342268A true CN104342268A (en) 2015-02-11

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105176651A (en) * 2015-10-23 2015-12-23 陈键 Low-temperature fire-resistant hydraulic oil
CN110257138A (en) * 2019-05-31 2019-09-20 刘凯 A kind of fire resistant hydraulic oil and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101812355A (en) * 2009-12-18 2010-08-25 益田润石(北京)化工有限公司 Novel synthetic fire-resistant hydraulic oil composition
CN102292424A (en) * 2008-12-01 2011-12-21 吉坤日矿日石能源株式会社 Flame retardant hydraulic oil composition
CN102695785A (en) * 2009-11-12 2012-09-26 吉坤日矿日石能源株式会社 Flame-retardant hydraulic oil composition
CN103013635A (en) * 2012-12-27 2013-04-03 安陆市奥森石油化学有限责任公司 Ester type fire-resistant hydraulic fluid and preparation method thereof
CN103122271A (en) * 2012-12-22 2013-05-29 桑达化工(南通)有限公司 Fire-resistant hydraulic oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102292424A (en) * 2008-12-01 2011-12-21 吉坤日矿日石能源株式会社 Flame retardant hydraulic oil composition
CN102695785A (en) * 2009-11-12 2012-09-26 吉坤日矿日石能源株式会社 Flame-retardant hydraulic oil composition
CN101812355A (en) * 2009-12-18 2010-08-25 益田润石(北京)化工有限公司 Novel synthetic fire-resistant hydraulic oil composition
CN103122271A (en) * 2012-12-22 2013-05-29 桑达化工(南通)有限公司 Fire-resistant hydraulic oil
CN103013635A (en) * 2012-12-27 2013-04-03 安陆市奥森石油化学有限责任公司 Ester type fire-resistant hydraulic fluid and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105176651A (en) * 2015-10-23 2015-12-23 陈键 Low-temperature fire-resistant hydraulic oil
CN110257138A (en) * 2019-05-31 2019-09-20 刘凯 A kind of fire resistant hydraulic oil and preparation method thereof
CN110257138B (en) * 2019-05-31 2022-08-12 惠华科技有限公司 Flame-retardant hydraulic oil and preparation method thereof

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Application publication date: 20150211

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