CN104328668A - Artificially synthetic fiber after-treatment hand feeling comprehensive auxiliary agent and preparation and dipping methods thereof - Google Patents
Artificially synthetic fiber after-treatment hand feeling comprehensive auxiliary agent and preparation and dipping methods thereof Download PDFInfo
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- CN104328668A CN104328668A CN201410548613.9A CN201410548613A CN104328668A CN 104328668 A CN104328668 A CN 104328668A CN 201410548613 A CN201410548613 A CN 201410548613A CN 104328668 A CN104328668 A CN 104328668A
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- auxiliary agent
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Abstract
The invention relates to an artificially synthetic fiber after-treatment hand feeling comprehensive auxiliary agent and preparation and dipping methods thereof, the artificially synthetic fiber after-treatment hand feeling comprehensive auxiliary agent is prepared by mixing the following components by weight: 5-20% of a mixing emulsifier, 1-5% of an auxiliary emulsifier, 5-20% of ternary copolymerization silicone oil, 5-20% amino modified silicone oil, 5-20% of epoxy modified silicone oil, 1-5% hydroxyl modified silicone oil, and 10-78% of water. The artificially synthetic fiber after-treatment hand feeling comprehensive auxiliary agent A63 can be diluted with water in any ratio, is simple and convenient to use in dipping, especially has good treatment effect to artificial fiber, after dipping treatment, has long-term soft, smooth, nourishing, moisturizing and other multi functional hand feeling, the production equipment is simple, and the cost is low.
Description
[technical field]
The present invention relates to fibre trimmer, be specifically related to the comprehensive auxiliary agent of a kind of artificial synthetic fiber Final finishing feel and preparation thereof, dipping method.
[background technology]
Hair product industry, before fibre completes, mostly will carry out impregnation process through various silicone oil auxiliary agent.Through the fiber of auxiliary agent impregnation process, one deck silicon oil membrane can be formed to give product multiple excellent performance at fiber surface, thus improve quality scale and the added value of product.Silicone oil auxiliary agent develops into the amido silicon oil of the second generation from the dimethicone that the first generation is single, can cross and give fiber softening smooth feel, but because the feel persistence of fiber hair is poor, in this, silicone oil can not meet, so present invention employs third generation silicone oil technology and seek most suitable proportioning in conjunction with the first generation and the second generation in two generation.
[summary of the invention]
The object of the invention is to the problem of the fabric hand persistence difference solving existing silicone oil impregnation process.
To achieve these goals, provide a kind of artificial synthetic fiber Final finishing feel comprehensive auxiliary agent, mix obtained by each component of following percentage by weight:
The blended emulsifier of 5 ~ 20%;
The assistant for emulsifying agent of 1 ~ 5%;
The ternary polymerization silicone oil of 5 ~ 20%;
The modified amino silicon oil of 5 ~ 20%;
The epoxy modified polysiloxane of 5 ~ 20%;
The hydroxyl modification silicone oil of 1 ~ 5%;
The water of 10 ~ 78%.
Above-mentioned formula also has following prioritization scheme:
Described blended emulsifier is mixed to get by two kinds of different AEO nonionic emulsifiers, can have good emulsification to silicone oil, and the emulsion after emulsification is more even, and that sprawls on fiber is more even simultaneously.
Described assistant for emulsifying agent adopts the solvent of alcohols, can make being more prone to of silicone oil emulsification, shortens emulsification times.
The present invention also comprises the preparation method of the comprehensive auxiliary agent of a kind of artificial synthetic fiber Final finishing feel, by the blended emulsifier of 5 ~ 20%, 1 ~ 5% assistant for emulsifying agent, the ternary polymerization silicone oil of 5 ~ 20%, modified amino silicon oil, the epoxy modified polysiloxane of 5 ~ 20%, the hydroxyl modification silicone oil of 1 ~ 5% of 5 ~ 20%; The water mixing of 10 ~ 78% is obtained.
The present invention also comprises a kind of dipping method adopting the comprehensive auxiliary agent of above-mentioned artificial synthetic fiber Final finishing feel, and fully immersed in the maceration extract being added with the comprehensive auxiliary agent of described artificial synthetic fiber Final finishing feel by pending fiber, parameter is as follows:
Fiber after dipping is taken out, centrifugal dehydration, to dry.
The maximum feature of this kind of silicone oil of ternary polymerization silicone oil is that moisture retention is strong, and can greatly improve the water-soluble of silicone oil in the middle of system, increases the stability of system, and has good moisture retention and permeability to filament.
Modified amino silicon oil is the silicone oil with amino, and one is good oiliness two can be provided to be to provide good adsorptivity to fiber, has good persistence to fabric hand.
Epoxy modified polysiloxane is the silicone oil with epoxy-functional, has good reactivity, can be good at combining the film forming increasing silicone oil with other silicone oil in system
Hydroxyl modification silicone oil hydroxyl can be combined with amino silicone oil in body series, and like this multiple silicone oil be combined with each other, and just considerably increases oil applying rate and the film forming of fiber.
The comprehensive auxiliary agent A 63 of artificial synthetic fiber Final finishing feel provided by the invention, can with water arbitrarily than dilution, flood easy to use, particularly good treatment effect is sent out to artificial fiber, there is after impregnation process soft smooth lastingly, moisten the multi-functional feels such as moisturizing, production equipment is simple, and cost is low.
[detailed description of the invention]
Embodiment 1
1, after-treating auxiliary recipe ingredient (with mass ratio range)
2, preparation method:
First add emulsifying agent and assistant for emulsifying agent, add various silicone oil crude oil again, after stirring, slowly add deionized water, if emulsion is too sticky, add with portions of de-ionized water dilution point acetic acid, be in when profit dissolves each other etc. emulsion and stir about 30 minutes, finally remaining water is all added and obtains uniform silicone oil emulsion, in order to emulsion is more stable can ph value furnishing faintly acid.
3, using method is flooded:
Get 1000ml, the demineralized water of 25 ~ 30 DEG C, add the above-mentioned obtained product of 10 ~ 15g and stir, make it fully dissolve in water, obtain maceration extract (also can additive compound similar with other use); Get pending fiber 100g, put into maceration extract, soak 15 ~ 20min; Fiber after dipping is pulled out, moulding post-drying on request.
Embodiment 2
1, after-treating auxiliary recipe ingredient (with mass ratio range)
2, preparation method:
First add emulsifying agent and assistant for emulsifying agent, add various silicone oil crude oil again, after stirring, slowly add deionized water, because ternary polymerization silicone oil self-emulsifying ability does not need acid adjustment by force, be in when profit dissolves each other etc. emulsion and stir about 30 minutes, finally remaining water is all added and obtain uniform silicone oil emulsion.
3, using method is flooded:
Get 1000ml, the demineralized water of 25 ~ 30 DEG C, add the above-mentioned obtained product of 10 ~ 15g and stir, make it fully dissolve in water, obtain maceration extract (also can use with other flexible smooth additive compound); Get pending fiber 100g, put into maceration extract, soak 15 ~ 20min; Fiber after dipping is pulled out, moulding post-drying on request.
Be more than preferred embodiment of the present invention, all changes done according to technical solution of the present invention, when the function produced does not exceed the scope of technical solution of the present invention, all belong to protection scope of the present invention.
Claims (5)
1. the comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel, is characterized in that mixing obtained by each component of following percentage by weight:
The blended emulsifier of 5 ~ 20%;
The assistant for emulsifying agent of 1 ~ 5%;
The ternary polymerization silicone oil of 5 ~ 20%;
The modified amino silicon oil of 5 ~ 20%;
The epoxy modified polysiloxane of 5 ~ 20%;
The hydroxyl modification silicone oil of 1 ~ 5%;
The water of 10 ~ 78%.
2. the comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel as claimed in claim 1, is characterized in that described blended emulsifier is mixed to get by two kinds of different AEO nonionic emulsifiers.
3. the comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel as claimed in claim 1, is characterized in that described assistant for emulsifying agent adopts the solvent of alcohols.
4. a preparation method for the comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel, it is characterized in that by the blended emulsifier of 5 ~ 20%, 1 ~ 5% assistant for emulsifying agent, the ternary polymerization silicone oil of 5 ~ 20%, modified amino silicon oil, the epoxy modified polysiloxane of 5 ~ 20%, the hydroxyl modification silicone oil of 1 ~ 5% of 5 ~ 20%; The water mixing of 10 ~ 78% is obtained.
5. a dipping method for the comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel described in claim 1, it is characterized in that pending fiber fully to immerse in the maceration extract being added with the comprehensive auxiliary agent of described artificial synthetic fiber Final finishing feel, parameter is as follows:
Fiber after dipping is taken out, centrifugal dehydration, to dry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410548613.9A CN104328668B (en) | 2014-10-16 | 2014-10-16 | The comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel and preparation, dipping method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410548613.9A CN104328668B (en) | 2014-10-16 | 2014-10-16 | The comprehensive auxiliary agent of artificial synthetic fiber Final finishing feel and preparation, dipping method |
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| Publication Number | Publication Date |
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| CN104328668A true CN104328668A (en) | 2015-02-04 |
| CN104328668B CN104328668B (en) | 2016-08-31 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110791965A (en) * | 2019-10-12 | 2020-02-14 | 苏州联胜化学有限公司 | Fabric softener and preparation method thereof |
| CN112012019A (en) * | 2020-08-26 | 2020-12-01 | 广东宏昊化工有限公司 | Super-smooth silky silicone oil for fabric after-finishing and after-finishing process |
| CN114232139A (en) * | 2021-12-16 | 2022-03-25 | 连云港神鹰复合材料科技有限公司 | Preparation method of carbon fiber oil for dry-jet wet-spun precursor |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4409267A (en) * | 1981-04-15 | 1983-10-11 | Shin-Etsu Chemical Co., Ltd. | Method for the finishing treatment of fabric materials |
| CN101619542A (en) * | 2008-07-01 | 2010-01-06 | 河南瑞贝卡发制品股份有限公司 | Preparation method of organosilicon emulsion straight fiber finishing additive and dipping process |
| CN102839545A (en) * | 2012-09-01 | 2012-12-26 | 中山市巴斯基化工有限公司 | Ice-feeling silicone oil for continuous dip padding process |
-
2014
- 2014-10-16 CN CN201410548613.9A patent/CN104328668B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4409267A (en) * | 1981-04-15 | 1983-10-11 | Shin-Etsu Chemical Co., Ltd. | Method for the finishing treatment of fabric materials |
| CN101619542A (en) * | 2008-07-01 | 2010-01-06 | 河南瑞贝卡发制品股份有限公司 | Preparation method of organosilicon emulsion straight fiber finishing additive and dipping process |
| CN102839545A (en) * | 2012-09-01 | 2012-12-26 | 中山市巴斯基化工有限公司 | Ice-feeling silicone oil for continuous dip padding process |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110791965A (en) * | 2019-10-12 | 2020-02-14 | 苏州联胜化学有限公司 | Fabric softener and preparation method thereof |
| CN112012019A (en) * | 2020-08-26 | 2020-12-01 | 广东宏昊化工有限公司 | Super-smooth silky silicone oil for fabric after-finishing and after-finishing process |
| CN114232139A (en) * | 2021-12-16 | 2022-03-25 | 连云港神鹰复合材料科技有限公司 | Preparation method of carbon fiber oil for dry-jet wet-spun precursor |
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| Publication number | Publication date |
|---|---|
| CN104328668B (en) | 2016-08-31 |
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