CN104328654A - High-performance three-proofing antibiotic fabric and finishing method thereof - Google Patents
High-performance three-proofing antibiotic fabric and finishing method thereof Download PDFInfo
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- CN104328654A CN104328654A CN201410607123.1A CN201410607123A CN104328654A CN 104328654 A CN104328654 A CN 104328654A CN 201410607123 A CN201410607123 A CN 201410607123A CN 104328654 A CN104328654 A CN 104328654A
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- antibacterial
- antibacterial finishing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/11—Oleophobic properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a high-performance three-proofing antibiotic fabric and finishing method thereof. The high-performance three-proofing antibiotic fabric is obtained by one-bath finishing cotton woven by using a compound three-proofing antibiotic finishing agent composed of a nano-silver sol antibiotic finishing agent, an HS1100 three-proofing finishing agent, an ATB9800 antibiotic finishing agent and a TPM9007antibactrial finishing agent. Starch which is a natural degradable polymer is used as a protective agent and a dispersing agent, and a simple liquid-phase chemical reduction method is used for preparing starch cladded nano-silver sol, the process is simple and environment-friendly, the nano-silver sol is good in dispersibility and hard to reunite. The prepared nano-silver three-proofing antibiotic finishing agent can be used for one-bath finishing, and is simple in process and convenient for operation in comparison with dividing-bath finishing.
Description
Technical field
The present invention relates to a kind of three anti-antibiotic facing material and method for sorting thereof.
Background technology
In daily life, bedding existence cannot often be washed or washing time deficiency, and traditional Exposure to Sunlight ultraviolet can only be relied on to kill part harmful fungoid and bacterium.Therefore in use, easily polluted, produce the phenomenons such as jaundice, mouldy, peculiar smell, have impact on the aesthetic measure in product use procedure, comfort level and degree of safety.And three anti-antibiotic finishes can give textile water proof, grease proofing, antifouling and anti-microbial property simultaneously, can overcome the above problems to a great extent.
At present substantially, adopt a point bath to arrange, and point bath three anti-+ antibacterial namely first three anti-after antibacterial or first antibacterial rear three-prevention finishings, this technique makes three anti-anti-microbial properties interact and complex process, long flow path.
Generally, nano antibacterial agent one-bath finishing can make three anti-and antibacterial composite finishing liquid stability declines, even in the favorite generation precipitation of one-bath finishing process, for overcoming above shortcoming, there is provided a kind of technique simple, easy to operate, the Nano Silver three that security is good prevents antibacterial composite finishing agent one-bath finishing method.
Summary of the invention
The object of the present invention is to provide a kind of technique simple, the anti-antibiotic facing material of high-performance three that easy to operate, security is good, antibacterial, NBC protective performance is good and method for sorting thereof.
Technical solution of the present invention is:
The anti-antibiotic facing material of a kind of high-performance three, is characterized in that: carry out one-bath finishing with the anti-antibacterial finishing agent of compound three of nano silver colloidal sol antibacterial finishing agent, HS1100 three-proof finishing agent, ATB9800 antibacterial finishing agent, TPM9007 antibacterial finishing agent composition to COTTON FABRIC and obtain.
A method for sorting for the anti-antibiotic facing material of high-performance three, is characterized in that: comprise following method:
The first step: grey cloth preliminary treatment: be the sodium hydroxide solution of 2% by 30 ~ 40ml/g fabric proportions concentration; Fabric is put into after alkali lye boils 10min and take out; With clear water rinsing fabric, until inspection move back clean '
Second step: one-bath finishing is rolled in two leachings two: padding finishing agent: get the anti-antibacterial finishing agent 20 ~ 100g/L of compound three, is padding temperature 10 ~ 30 DEG C, adopts two leaching two roll process under pick-up rate 60 ~ 90% condition; Dry: hot-air seasoning under 100 ~ 120 DEG C of conditions, the time is 2 ~ 3min; Bake: 160 ?175 DEG C of conditions, bake 60 ~ 120s; Go out cloth: finally complete processing cloth, i.e. the obtained anti-antibiotic facing material of high-performance three;
The anti-antibacterial finishing agent of described compound three forms by with the coated nanometer silver antimicrobial colloidal sol of converted starch, three-proof finishing agent HS1100, antibacterial finishing agent ATB9800, antibacterial finishing agent TPM9007, and each constituent mass percentage is: nano silver colloidal sol: HS1100:ATB9800:TPM9007=0.1 ~ 0.4%:5 ~ 9%:2 ~ 5%:2 ~ 4%.
The preparation method of the nanometer silver antimicrobial colloidal sol that described converted starch is coated:
(1) prepare the liquor argenti nitratis ophthalmicus of 0.05mol/L and concentration be 1% sodium citrate solution for subsequent use;
(2) add in there-necked flask by 50 ~ 100ml water, then add 0.25 ~ 0.5g converted starch, open heat collecting type constant-temperature heating magnetic stirring apparatus, put into by above there-necked flask, stir and be warming up to 95 DEG C, about 30min, makes starch gelatinization;
(3) cool the temperature to 60 ~ 70 DEG C, drip the liquor argenti nitratis ophthalmicus for preparing of 10 ~ 20ml in there-necked flask, continuous stirring reaction 10min;
(4) with the sodium citrate solution that the speed of 1/S dropping 2 ~ 5ml prepares, stir and make it fully react;
(5) question response system color no longer changes, and namely after sufficient reacting, is taken out by obtained colloidal sol from reaction flask, naturally cools.
Use natural degradable macromolecule---starch cooks protective agent and dispersant, and adopts simple solution phase chemical reduction to prepare the coated nano silver colloidal sol of starch, and technique is simple, and environmental protection, good dispersion, not easily reunites.Not by chemically composited, but three anti-auxiliary agents and several Antibacterial accessory ingredient are carried out composite, optimize each component ratio, to reach better three anti-and antibacterial Multifunctional effect.The obtained anti-antibacterial finishing agent of Nano Silver three can be used for one-bath finishing, and arrange relative to a point bath, technique is simple, easy to operate.
Table:
1, Nano Silver concentration 0.05%, HS1100 concentration is 2%, ATB9800 concentration when be 1%, TPM9007 concentration being 2%, and antibiotic rate reaches 75%, refuses water contact angle and reaches 110 degree, refuses oily class 6 level.
2, Nano Silver concentration 0.2%, HS1100 concentration is 6%, ATB9800 concentration when be 3%, TPM9007 concentration being 4%, and antibiotic rate reaches 98%, refuses water contact angle and reaches 132 degree, refuses wet goods level 7 grades.
3, Nano Silver concentration 0.6%, HS1100 concentration is 10%, ATB9800 concentration when be 5%, TPM9007 concentration being 6%, and antibiotic rate reaches 98%, refuses water contact angle and reaches 133 degree, refuses wet goods level 8 grades.
4, Nano Silver 0.2% is used alone, antibiotic rate 65%, without three anti-effects.
5, be used alone HS11006%, refuse water contact angle and reach 128 degree, refuse wet goods level 7 grades, without antibiotic property.
6, ATP98003% is used alone, antibiotic rate 85%, without three anti-effects.
7, TPM97004% is used alone, antibiotic rate 88%, without three anti-effects.
Detailed description of the invention
To contribute to understanding the present invention by following embodiment, but not limit content of the present invention.
Embodiment 1:
The Nano Silver preparation that first step converted starch is coated, method is as follows:
(1) prepare the liquor argenti nitratis ophthalmicus of 0.05mol/L and concentration be 1% sodium citrate solution for subsequent use;
(2) add in there-necked flask by 50ml water, then add 0.25g converted starch, open heat collecting type constant-temperature heating magnetic stirring apparatus, put into by above there-necked flask, stir and be warming up to 95 DEG C, about 30min, makes starch gelatinization;
(3) cool the temperature to 70 DEG C, drip the liquor argenti nitratis ophthalmicus for preparing of 10ml in there-necked flask, continuous stirring reaction 10min;
(4) with the sodium citrate solution that the speed of 1/S dropping 2ml prepares, stir and make it fully react;
(5) question response system color no longer changes, and namely after sufficient reacting, is taken out by obtained colloidal sol from reaction flask, naturally cools.
Second step is according to each constituent optimization result, preparation of nano silver three anti-antibacterial finishing agents, specific as follows: (1) is according to nano silver colloidal sol: HS1100:ATB9800:TPM9007=0.2:6:3:2, take nano silver colloidal sol 2g, HS1100 three-proof finishing agent 60g, ATB9800 antibacterial finishing agent 30g, TPM9007 antibacterial finishing agent 20g (the heavy 1000g of total liquid)
(2) first 60g HS1100 three-proof finishing agent is placed in the there-necked flask of band stirring, then add the nano silver colloidal sol of 2g gradually, the ATB9800 antibacterial finishing agent of 30g, the TPM9007 antibacterial finishing agent of 20g, add water to the heavy 1000g of total liquid.
(3) composite three good anti-antiseptics are stirred 10min at normal temperatures and pressures until evenly.
3rd step grey cloth preliminary treatment
(1) be the sodium hydroxide solution of 2% by 35ml/g fabric proportions concentration;
(2) fabric is put into after alkali lye boils 10min and take out;
(3) with clear water rinsing fabric, until inspection is moved back clean.
4th step: one-bath finishing is rolled in two leachings two
(1) padding finishing agent: take from the anti-antibacterial finishing agent 50g/L of compound three processed, is padding temperature 15 DEG C, adopts two leaching two roll process under pick-up rate 70% condition;
(2) dry: hot-air seasoning under 100 DEG C of conditions, the time is 2min;
(3) bake: 170 DEG C of conditions, bake 100s;
(4) cloth is gone out: finally complete processing cloth, i.e. the obtained anti-antibiotic facing material of high-performance three.
Embodiment 2:
Preparation compound three anti-antibacterial finishing agent, its preparation process, technique and embodiment 1 first step, second step are identical.
3rd step grey cloth preliminary treatment
(1) be the sodium hydroxide solution of 2% by 40ml/g fabric proportions concentration;
(2) fabric is put into after alkali lye boils 10min and take out;
(3) with clear water rinsing fabric, until inspection is moved back clean.
4th step: one-bath finishing is rolled in two leachings two
(1) padding finishing agent: take from the anti-antibacterial finishing agent 60g/L of compound three processed, is padding temperature 20 DEG C, adopts two leaching two roll process under pick-up rate 80% condition;
(2) dry: hot-air seasoning under 110 DEG C of conditions, the time is 2min;
(3) bake: 175 DEG C of conditions, bake 90s;
(4) cloth is gone out: finally complete processing cloth, i.e. the obtained anti-antibiotic facing material of high-performance three.
Embodiment 3:
Preparation compound three anti-antibacterial finishing agent, its preparation process, technique and embodiment 1 first step, second step are identical.
3rd step grey cloth preliminary treatment
(1) be the sodium hydroxide solution of 2% by 30ml/g fabric proportions concentration;
(2) fabric is put into after alkali lye boils 10min and take out;
(3) with clear water rinsing fabric, until inspection is moved back clean.
4th step: one-bath finishing is rolled in two leachings two
(1) padding finishing agent: take from the anti-antibacterial finishing agent 30g/L of compound three processed, is padding temperature 30 DEG C, adopts two leaching two roll process under pick-up rate 75% condition;
(2) dry: hot-air seasoning under 120 DEG C of conditions, the time is 2min;
(3) bake: 165 DEG C of conditions, bake 90s;
(4) cloth is gone out: finally complete processing cloth, i.e. the obtained anti-antibiotic facing material of high-performance three.
Claims (3)
1. the anti-antibiotic facing material of high-performance three, is characterized in that: carry out one-bath finishing with the anti-antibacterial finishing agent of compound three of nano silver colloidal sol antibacterial finishing agent, HS1100 three-proof finishing agent, ATB9800 antibacterial finishing agent, TPM9007 antibacterial finishing agent composition to COTTON FABRIC and obtain.
2. a method for sorting for the anti-antibiotic facing material of high-performance three, is characterized in that: comprise following method:
The first step: grey cloth preliminary treatment: be the sodium hydroxide solution of 2% by 30 ~ 40ml/g fabric proportions concentration; Fabric is put into after alkali lye boils 10min and take out; With clear water rinsing fabric, until inspection move back clean '
Second step: one-bath finishing is rolled in two leachings two: padding finishing agent: get the anti-antibacterial finishing agent 20 ~ 100g/L of compound three, is padding temperature 10 ~ 30 DEG C, adopts two leaching two roll process under pick-up rate 60 ~ 90% condition; Dry: hot-air seasoning under 100 ~ 120 DEG C of conditions, the time is 2 ~ 3min; Bake: 160-175 DEG C of condition, bake 60 ~ 120s; Go out cloth: finally complete processing cloth, i.e. the obtained anti-antibiotic facing material of high-performance three;
The anti-antibacterial finishing agent of described compound three forms by with the coated nanometer silver antimicrobial colloidal sol of converted starch, three-proof finishing agent HS1100, antibacterial finishing agent ATB9800, antibacterial finishing agent TPM9007, and each constituent mass percentage is: nano silver colloidal sol: HS1100: ATB9800: TPM9007=0.1 ~ 0.4%: 5 ~ 9%: 2 ~ 5%: 2 ~ 4%.
3. the method for sorting of the anti-antibiotic facing material of high-performance three according to claim 2, is characterized in that: the preparation method of the nanometer silver antimicrobial colloidal sol that described converted starch is coated:
(1) prepare the liquor argenti nitratis ophthalmicus of 0.05mol/L and concentration be 1% sodium citrate solution for subsequent use;
(2) add in there-necked flask by 50 ~ 100ml water, then add 0.25 ~ 0.5g converted starch, open heat collecting type constant-temperature heating magnetic stirring apparatus, put into by above there-necked flask, stir and be warming up to 95 DEG C, about 30min, makes starch gelatinization;
(3) cool the temperature to 60 ~ 70 DEG C, drip the liquor argenti nitratis ophthalmicus for preparing of 10 ~ 20ml in there-necked flask, continuous stirring reaction 10min;
(4) with the sodium citrate solution that the speed of 1/S dropping 2 ~ 5ml prepares, stir and make it fully react;
(5) question response system color no longer changes, and namely after sufficient reacting, is taken out by obtained colloidal sol from reaction flask, naturally cools.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410607123.1A CN104328654B (en) | 2014-10-31 | 2014-10-31 | The anti-antibiotic facing material of high-performance three and method for sorting thereof |
| CN201610028498.1A CN105603724B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of easy to operate high-performance three proofings antibiotic facing material |
| CN201610028497.7A CN105525504B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of the simple high-performance three proofings antibiotic facing material of technique |
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| CN201410607123.1A CN104328654B (en) | 2014-10-31 | 2014-10-31 | The anti-antibiotic facing material of high-performance three and method for sorting thereof |
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| CN201610028498.1A Division CN105603724B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of easy to operate high-performance three proofings antibiotic facing material |
| CN201610028497.7A Division CN105525504B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of the simple high-performance three proofings antibiotic facing material of technique |
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| CN104328654A true CN104328654A (en) | 2015-02-04 |
| CN104328654B CN104328654B (en) | 2016-04-27 |
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| CN201610028498.1A Active CN105603724B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of easy to operate high-performance three proofings antibiotic facing material |
| CN201410607123.1A Active CN104328654B (en) | 2014-10-31 | 2014-10-31 | The anti-antibiotic facing material of high-performance three and method for sorting thereof |
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| CN201610028498.1A Active CN105603724B (en) | 2014-10-31 | 2014-10-31 | The method for sorting of easy to operate high-performance three proofings antibiotic facing material |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105040414A (en) * | 2015-05-25 | 2015-11-11 | 厦门大学 | Preparation method of sliver supporting fabric based on plant material and nanometer sliver synergetic antibacterial |
| CN106192395A (en) * | 2016-07-04 | 2016-12-07 | 浙江理工大学 | The method of modified cotton fabric surface enhanced nanometer silver antimicrobial bafta washing fastness |
| CN108842465A (en) * | 2017-02-27 | 2018-11-20 | 浙江绿龙新材料有限公司 | The preparation method of oil stain preventing function water proof fire retardant person's textile fabric |
| CN111206429A (en) * | 2020-03-13 | 2020-05-29 | 江苏丽洋新材料股份有限公司 | Preparation method of medical and health material with trapping, killing and antibacterial multi-stage barrier functions |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106087419A (en) * | 2016-07-04 | 2016-11-09 | 安徽省曾氏保洁品有限公司 | A kind of cotton mop treatment fluid and its preparation method and application |
| CN106245311A (en) * | 2016-08-03 | 2016-12-21 | 江苏顺远新材料科技股份有限公司 | A kind of production technology of ecological high-performance fiber composite functional fabric |
| CN109811454B (en) * | 2019-02-18 | 2020-09-08 | 浙江龙冉纺织有限公司 | Production process of high-wear-resistance chenille three-proofing fabric |
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| CN1947520A (en) * | 2005-10-12 | 2007-04-18 | 福盈科技化学股份有限公司 | Aqueous solution contg. nano-silver dispersing particles and its prepn. method |
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| CN103485187A (en) * | 2013-09-16 | 2014-01-01 | 苏州志向纺织科研股份有限公司 | Finishing process for self-cleaning anti-bacterial and odor-resistant multifunctional dacron fabric |
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- 2014-10-31 CN CN201610028497.7A patent/CN105525504B/en not_active Expired - Fee Related
- 2014-10-31 CN CN201610028498.1A patent/CN105603724B/en active Active
- 2014-10-31 CN CN201410607123.1A patent/CN104328654B/en active Active
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| CN101941075A (en) * | 2009-07-03 | 2011-01-12 | 北京印刷学院 | Synthetic method of antibacterial agent containing nano-silver |
| CN101731272A (en) * | 2009-12-24 | 2010-06-16 | 中国人民解放军军事医学科学院基础医学研究所 | Method for preparing antibacterial nanometer silver colloid |
| CN102552963A (en) * | 2011-11-21 | 2012-07-11 | 北京科技大学 | Preparation method of starch/nano-silver antibacterial composite film |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105040414A (en) * | 2015-05-25 | 2015-11-11 | 厦门大学 | Preparation method of sliver supporting fabric based on plant material and nanometer sliver synergetic antibacterial |
| CN105040414B (en) * | 2015-05-25 | 2017-05-03 | 厦门大学 | Preparation method of sliver supporting fabric based on plant material and nanometer sliver synergetic antibacterial |
| CN106192395A (en) * | 2016-07-04 | 2016-12-07 | 浙江理工大学 | The method of modified cotton fabric surface enhanced nanometer silver antimicrobial bafta washing fastness |
| CN108842465A (en) * | 2017-02-27 | 2018-11-20 | 浙江绿龙新材料有限公司 | The preparation method of oil stain preventing function water proof fire retardant person's textile fabric |
| CN108842465B (en) * | 2017-02-27 | 2021-04-30 | 浙江敏业新材料股份有限公司 | Preparation method of oil stain-proof, waterproof and flame-retardant home textile fabric |
| CN111206429A (en) * | 2020-03-13 | 2020-05-29 | 江苏丽洋新材料股份有限公司 | Preparation method of medical and health material with trapping, killing and antibacterial multi-stage barrier functions |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105525504B (en) | 2017-12-01 |
| CN105525504A (en) | 2016-04-27 |
| CN104328654B (en) | 2016-04-27 |
| CN105603724B (en) | 2017-12-01 |
| CN105603724A (en) | 2016-05-25 |
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