CN104327547A - Natural pigment composition for replacing synthesized pigments and applications thereof - Google Patents
Natural pigment composition for replacing synthesized pigments and applications thereof Download PDFInfo
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- CN104327547A CN104327547A CN201410414352.1A CN201410414352A CN104327547A CN 104327547 A CN104327547 A CN 104327547A CN 201410414352 A CN201410414352 A CN 201410414352A CN 104327547 A CN104327547 A CN 104327547A
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Abstract
The invention relates to the field of natural pigments, and specifically discloses a natural pigment composition for replacing synthesized pigments and applications thereof. The natural pigment composition is prepared by compounding monascus red with xanthophyll, monascus yellow, turmeric, turmeric oleoresin, gardenia yellow, and beta-carotene. The natural pigment composition originates from natural pigments, is prepared by compounding multiple natural pigments together, is capable of replacing the synthesized apple green pigment used in the tobacco sheet field, and fulfills the requirements on safety and original color at the same time.
Description
Technical field
The present invention relates to field of natural pigment, relate to a kind of natural pigment composition and application thereof of alternative synthetic colour in particular.
Background technology
Synthetic colour lemon yellow, Sunset yellow, famille rose, temptation are red, light green is that tobacco industry especially uses tinting material widely in tobacco sheet.This several synthetic colour is with the obtained organic pigment of artificial chemical synthesis process, mainly with the aniline dyestuff separated in coal tar for raw material is made.General toxicity comprised to the harm of human body, causes rushing down property, cause prominent property (transgenation) and carcinogenesis.
Along with the development of society and the raising of people's living standard, increasing people can or can not work the mischief to HUMAN HEALTH for use synthetic colour and propose query.Meanwhile, a large amount of research reports is pointed out, nearly all synthetic colour all can not provide nutritive substance to human body, and some synthetic colour even can be detrimental to health.The scientific research personnel of the states such as American and Britain also found after doing relevant research, many synthetic colours have injury effect to human body, fertility decline, monster etc. may be caused, some pigment may convert carcinogenic substance in human body, and particularly the carcinogenesis of azo-compound class synthetic colour is more obvious.In addition, many edible synthesized coloring matters, except itself or its metabolite are poisonous, also may be mixed into arsenic and lead in process of production.Many countries just more strictly limit synthetic colour, the particularly use of azo pigment in food.Sweden, Finland, Norway, India, Denmark, France etc. prohibit the use azo pigment already, and wherein some countries such as Norway go back total ban and use any chemosynthesis pigment.From 1 day January in 2009, European Union limits the use of 6 kinds of synthetic colours such as lemon yellow, Sunset yellow, temptation are red, quinoline yellow, ponceau, azorubin comprehensively, especially when relating to infant foods, strictly controlling especially, packaging must be indicated the untoward reaction that can cause.
Natural pigment be mainly derived from the flower of plant, root, really, skin, leavened prod etc., not only do not have toxicity, except having colouring function, what have also has certain nutrition, even has certain pharmacological action and nourishing function.As far back as early 1980s, along with the research and development of all kinds of natural pigment, field of natural pigment achieves large quantities of scientific payoffs, along with the conversion of these scientific payoffss, promote the development of Chinese natural pigment, the exploitation of natural pigment and compound product thereof replaces synthetic colour thus also becomes inexorable trend, but because the use color characteristic of synthetic colour in tobacco sheet has given human consumer with deep impression, therefore, for avoiding substituting and the difference sense that brings, need to develop can use safely in tobacco sheet industry, color can replace synthetic colour lemon yellow again, Sunset yellow, carmine, lure red, light green natural pigment product, it is the problem instantly studied and solving.
Summary of the invention
In view of this, the object of the present invention is to provide a kind of natural pigment composition and application thereof of alternative synthetic colour, make this natural pigment composition can substitute light green synthetic colour, on L, a, b and △ Lab and light green no significant difference.
For achieving the above object, the invention provides following technical scheme:
A natural pigment composition for alternative synthetic colour, is made up of the Gardenia Yellow of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 40-80; Or be made up of the xenthophylls of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 80-120; Or be made up of the beta carotene of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 3-7%; Or the red colouring agent for food, also used as a Chinese medicine Huang composition of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 130-170; Or be made up of the turmeric of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 1.5-3.5%; Or be made up of the turmeric oleoresin of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 3-7%.
Preferably, by look valency be 60 chlorophyll and look valency be 60 Gardenia Yellow form; Or by look valency be 60 chlorophyll and look valency be 100 xenthophylls form; Or by look valency be 60 chlorophyll and mass percent be 5% beta carotene form; Or look valency be 60 chlorophyll and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang composition; Or by look valency be 60 chlorophyll and mass percent be 2.5% turmeric form; Or by look valency be 60 chlorophyll and mass percent be 5% turmeric oleoresin form.
Preferably, by look valency be 80 sodium copper chlorophyllin and look valency be 60 Gardenia Yellow form; Or by look valency be 80 sodium copper chlorophyllin and look valency be 100 xenthophylls form; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 5% beta carotene form; Or look valency be 80 sodium copper chlorophyllin and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang composition; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 2.5% turmeric form; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 5% turmeric oleoresin form.
Preferably, the weight ratio of described chlorophyll or its copper sodium and Gardenia Yellow is 1-50:1.More preferably, the weight ratio of described chlorophyll and Gardenia Yellow is 5-40:1, or the weight ratio of described sodium copper chlorophyllin and Gardenia Yellow is 4-45:1.
Preferably, the weight ratio of described chlorophyll or its copper sodium and xenthophylls is 1-40:1.More preferably, the weight ratio of described chlorophyll and xenthophylls is 10-30:1, or the weight ratio of described sodium copper chlorophyllin and xenthophylls is 3-30:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the beta carotene of 3-7% is 1-45:1.More preferably, the weight ratio of the beta carotene of described chlorophyll and 3-7% is 5-45:1, or the weight ratio of the beta carotene of described sodium copper chlorophyllin and 3-7% is 5-40:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the beta carotene of 5% is 1-45:1.More preferably, described chlorophyll and 5% the weight ratio of beta carotene be 5-45:1, or described sodium copper chlorophyllin and 5% the weight ratio of beta carotene be 5-40:1.
Preferably, the weight ratio of described chlorophyll or its copper sodium and red colouring agent for food, also used as a Chinese medicine Huang is 1-60:1.More preferably, the weight ratio of described chlorophyll and red colouring agent for food, also used as a Chinese medicine Huang is 6-50:1, or the weight ratio of described sodium copper chlorophyllin and red colouring agent for food, also used as a Chinese medicine Huang is 10-50:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric of 1.5-3.5% is 1-30:1.More preferably, the weight ratio of the turmeric of described chlorophyll and 1.5-3.5% is 2-25:1, or the weight ratio of the turmeric of described sodium copper chlorophyllin and 1.5-3.5% is 6-25:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric of 2.5% is 1-30:1.More preferably, described chlorophyll and 2.5% the weight ratio of turmeric be 2-25:1, or described sodium copper chlorophyllin and 2.5% the weight ratio of turmeric be 6-25:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric oleoresin of 3-7% is 1-20:1.More preferably, the weight ratio of the turmeric oleoresin of described chlorophyll and 3-7% is 2-15:1, or the weight ratio of the turmeric oleoresin of described sodium copper chlorophyllin and 3-7% is 8-20:1.
Preferably, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric oleoresin of 5% is 1-20:1.More preferably, described chlorophyll and 5% the weight ratio of turmeric oleoresin be 2-15:1, or described sodium copper chlorophyllin and 5% the weight ratio of turmeric oleoresin be 8-20:1.
The present invention adopts suitable natural pigment composite, effectively play the toning complementary action of various pigment, it is made to press close to synthetic colour to greatest extent light green, meet the requirement of people to its processing performance, and realize pigment and use simplification, the consumption of single pigment can be reduced simultaneously, make up the defect of some natural pigment.
Adopt colour-difference meter to contrast the composite natural pigment composition of the present invention and synthetic colour light green, on L, a, b and △ Lab and light green extremely close, there is no significant difference.Therefore, the present invention also provides described natural pigment composition preparing the application in tobacco sheet.
From above technical scheme, the present invention is from natural pigment, carry out composite with the multiple natural pigment of proper types, obtaining can the light green natural pigment of the synthetic colour of alternate application in tobacco sheet field, meets the demand of people to safety and original tone simultaneously.
Embodiment
The invention discloses a kind of natural pigment composition and application thereof of alternative synthetic colour.Those skilled in the art can use for reference present disclosure, and suitable improving technique parameter realizes.Special needs to be pointed out is, all similar replacements and change apparent to those skilled in the art, they are all deemed to be included in the present invention.Product of the present invention and method are described by preferred embodiment, related personnel obviously can not depart from content of the present invention, spirit and scope methods and applications as herein described are changed or suitably change with combination, realize and apply the technology of the present invention.
The present invention's natural pigment used commercially, preferably adopts the product of He'nan Zhongda Biological Engineering Co., Ltd..
Below in conjunction with embodiment, set forth the present invention further.
Embodiment 1: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 60 Gardenia Yellow mix by weight the ratio of 5:1, to obtain final product.
Embodiment 2: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 60 Gardenia Yellow mix by weight the ratio of 40:1, to obtain final product.
Embodiment 3: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 100 xenthophylls mix by weight the ratio of 10:1, to obtain final product.
Embodiment 4: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 100 xenthophylls mix by weight the ratio of 30:1, to obtain final product.
Embodiment 5: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 5% beta carotene mix by weight for the ratio of 5:1, to obtain final product.
Embodiment 6: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 5% beta carotene mix by weight for the ratio of 45:1, to obtain final product.
Embodiment 7: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang mix in the ratio of 6:1, to obtain final product.
Embodiment 8: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang mix in the ratio of 50:1, to obtain final product.
Embodiment 9: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 2.5% turmeric mix by weight the ratio of 2:1, to obtain final product.
Embodiment 10: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 2.5% turmeric mix by weight the ratio of 25:1, to obtain final product.
Embodiment 11: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 5% turmeric oleoresin mix by weight the ratio of 2:1, to obtain final product.
Embodiment 12: natural pigment composition of the present invention
By commercially available look valency be 60 chlorophyll and mass percent be 5% turmeric oleoresin mix by weight the ratio of 15:1, to obtain final product.
Embodiment 13: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 60 Gardenia Yellow mix by weight the ratio of 4:1, to obtain final product.
Embodiment 14: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 60 Gardenia Yellow mix by weight the ratio of 45:1, to obtain final product.
Embodiment 15: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 100 xenthophylls mix by weight the ratio of 3:1, to obtain final product.
Embodiment 16: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 100 xenthophylls mix by weight the ratio of 30:1, to obtain final product.
Embodiment 17: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 5% beta carotene mix by weight for the ratio of 5:1, to obtain final product.
Embodiment 18: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 5% beta carotene mix by weight for the ratio of 40:1, to obtain final product.
Embodiment 19: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang mix in the ratio of 10:1, to obtain final product.
Embodiment 20: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang mix in the ratio of 50:1, to obtain final product.
Embodiment 21: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 2.5% turmeric mix by weight the ratio of 6:1, to obtain final product.
Embodiment 22: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 2.5% turmeric mix by weight the ratio of 25:1, to obtain final product.
Embodiment 23: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 5% turmeric oleoresin mix by weight the ratio of 8:1, to obtain final product.
Embodiment 24: natural pigment composition of the present invention
80 sodium copper chlorophyllins be by commercially available look valency and mass percent be 5% turmeric oleoresin mix by weight the ratio of 20:1, to obtain final product.
Embodiment 25: comparison test
In embodiment 1 ~ 24 by prepared natural pigment compound product by joining in tobacco extract after the addition water dissolution of 1 ~ 1.5%, keeping 45 ~ 50 DEG C is coated on cigarette paper uniformly, then in the warm air of 90 ~ 92 DEG C dry 1 minute, then put into that temperature is 36 DEG C, the illumination box of illuminance 10000LUX, relative humidity 34% is placed 7 days, light green for reference with synthetic colour, utilize Konica-Minolta CM3500d colour examining colour-difference-metre to detect chromatic aberration situation before and after illumination, the results are shown in Table 1.
Table 1 natural pigment composition of the present invention and the contrast of light green aberration
From the aberration result of table 1, show natural pigment composition of the present invention and synthetic colour light green between there is no significant difference, cannot differentiate from naked eyes two kinds of products have what difference.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a natural pigment composition for alternative synthetic colour, is characterized in that, is made up of the Gardenia Yellow of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 40-80; Or be made up of the xenthophylls of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 80-120; Or be made up of the beta carotene of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 3-7%; Or the red colouring agent for food, also used as a Chinese medicine Huang composition of look valency to be the chlorophyll of 60-80 or its copper sodium and look valency be 130-170; Or be made up of the turmeric of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 1.5-3.5%; Or be made up of the turmeric oleoresin of look valency to be the chlorophyll of 60-80 or its copper sodium and mass percent be 3-7%.
2. natural pigment composition according to claim 1, is characterized in that, by look valency be 60 chlorophyll and look valency be 60 Gardenia Yellow form; Or by look valency be 60 chlorophyll and look valency be 100 xenthophylls form; Or by look valency be 60 chlorophyll and mass percent be 5% beta carotene form; Or look valency be 60 chlorophyll and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang composition; Or by look valency be 60 chlorophyll and mass percent be 2.5% turmeric form; Or by look valency be 60 chlorophyll and mass percent be 5% turmeric oleoresin form.
3. natural pigment composition according to claim 1, is characterized in that, by look valency be 80 sodium copper chlorophyllin and look valency be 60 Gardenia Yellow form; Or by look valency be 80 sodium copper chlorophyllin and look valency be 100 xenthophylls form; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 5% beta carotene form; Or look valency be 80 sodium copper chlorophyllin and look valency be 150 red colouring agent for food, also used as a Chinese medicine Huang composition; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 2.5% turmeric form; Or by look valency be 80 sodium copper chlorophyllin and mass percent be 5% turmeric oleoresin form.
4. natural pigment composition according to claim 1, it is characterized in that, the weight ratio of described chlorophyll or its copper sodium and Gardenia Yellow is 1-50:1.
5. natural pigment composition according to claim 1, it is characterized in that, the weight ratio of described chlorophyll or its copper sodium and xenthophylls is 1-40:1.
6. natural pigment composition according to claim 1, is characterized in that, described chlorophyll or its copper sodium and mass percent are the weight ratio of the beta carotene of 3-7% is 1-45:1.
7. natural pigment composition according to claim 1, it is characterized in that, the weight ratio of described chlorophyll or its copper sodium and red colouring agent for food, also used as a Chinese medicine Huang is 1-60:1.
8. natural pigment composition according to claim 1, is characterized in that, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric of 1.5-3.5% is 1-30:1.
9. natural pigment composition according to claim 1, is characterized in that, described chlorophyll or its copper sodium and mass percent are the weight ratio of the turmeric oleoresin of 3-7% is 1-20:1.
10. natural pigment composition described in claim 1-9 any one is preparing the application in tobacco sheet.
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| CN201410414352.1A CN104327547A (en) | 2014-08-21 | 2014-08-21 | Natural pigment composition for replacing synthesized pigments and applications thereof |
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| CN201410414352.1A CN104327547A (en) | 2014-08-21 | 2014-08-21 | Natural pigment composition for replacing synthesized pigments and applications thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108659572A (en) * | 2018-06-04 | 2018-10-16 | 河南中大恒源生物科技股份有限公司 | A kind of natural pigment composition substituting sugar-coat synthetic dyestuff |
| CN113893244A (en) * | 2021-10-27 | 2022-01-07 | 四川大学华西医院 | Composition with blue light resisting effect |
| CN115381094A (en) * | 2022-08-18 | 2022-11-25 | 河南中大恒源生物科技股份有限公司 | Low-odor water-soluble copper chlorophyll and preparation method and application thereof |
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| CN101838478A (en) * | 2010-05-27 | 2010-09-22 | 河南中大生物工程有限公司 | Natural pigment composition and preparation method thereof |
| CN102524944A (en) * | 2012-01-19 | 2012-07-04 | 湖北中烟工业有限责任公司 | Color regulator special for improving appearance of recombinant tobacco and preparation method of same |
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2014
- 2014-08-21 CN CN201410414352.1A patent/CN104327547A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101838478A (en) * | 2010-05-27 | 2010-09-22 | 河南中大生物工程有限公司 | Natural pigment composition and preparation method thereof |
| CN102524944A (en) * | 2012-01-19 | 2012-07-04 | 湖北中烟工业有限责任公司 | Color regulator special for improving appearance of recombinant tobacco and preparation method of same |
Non-Patent Citations (2)
| Title |
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| 陈俊成: ""食用天然色素简介 叶绿素"", 《中国食品质量报》 * |
| 陈俊成: ""食用天然色素简介 叶绿素"", 《中国食品质量报》, 5 June 2004 (2004-06-05), pages 007 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108659572A (en) * | 2018-06-04 | 2018-10-16 | 河南中大恒源生物科技股份有限公司 | A kind of natural pigment composition substituting sugar-coat synthetic dyestuff |
| CN113893244A (en) * | 2021-10-27 | 2022-01-07 | 四川大学华西医院 | Composition with blue light resisting effect |
| CN115381094A (en) * | 2022-08-18 | 2022-11-25 | 河南中大恒源生物科技股份有限公司 | Low-odor water-soluble copper chlorophyll and preparation method and application thereof |
| CN115381094B (en) * | 2022-08-18 | 2023-10-24 | 河南中大恒源生物科技股份有限公司 | Low-odor water-soluble copper chlorophyll and preparation method and application thereof |
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