CN104326715B - A kind of fast setting binding agent and preparation method thereof - Google Patents
A kind of fast setting binding agent and preparation method thereof Download PDFInfo
- Publication number
- CN104326715B CN104326715B CN201410535418.2A CN201410535418A CN104326715B CN 104326715 B CN104326715 B CN 104326715B CN 201410535418 A CN201410535418 A CN 201410535418A CN 104326715 B CN104326715 B CN 104326715B
- Authority
- CN
- China
- Prior art keywords
- binding agent
- deionized water
- weight part
- fast setting
- glycerine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Adhesives Or Adhesive Processes (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses a kind of fast setting binding agent and preparation method thereof, the weight part of its constitutive material is: silicate cement 110-115, aqueous polyurethane 30-40, polytetrahydrofuran diol 25-30, nanometer titanium dioxide 40-50, jelly powder 15-20, glycerine 4-5, borax 18-25, isocyanic ester 3-5, triethylamine 2-3, hydroxyl polysiloxane 3-4, poly-Synthesis of Oligo Ethylene Glycol 1-1.2, polyoxyethylene glycol monobutyl ether 0.5-0.8 and deionized water 100-120; The present invention prepares binding agent and not only has the adhesiveproperties close with binding agent in prior art, the base material used is more extensive, and there is better curing speed, and simultaneously good with ageing-resistant performance in addition, save the advantage in energy consumption and extension device work-ing life.
Description
Technical field
The invention belongs to building materials technical field, be specifically related to a kind of fast setting binding agent and preparation method thereof.
Background technology
Along with the mankind are to environment protection and healthy pay attention to day by day, environmental protection binding agent obtains using more and more widely, and mostly adopt natural material, aboundresources, price is low, renewable; Petroliferous derivatize chemical product in the component of most of sizing agent, along with petroleum resources reduce day by day, search for oil substitute becomes inevitable; The environmental consciousness of people strengthens, and proposes strict requirement to the discharge of the pollutent such as toxic and harmful, waste water affecting environmental quality.
Summary of the invention
The object of the present invention is to provide a kind of fast setting binding agent and preparation method thereof.。
The present invention adopts following technical scheme:
Fast setting binding agent, the weight part of its constitutive material is: silicate cement 110-115, aqueous polyurethane 30-40, polytetrahydrofuran diol 25-30, nanometer titanium dioxide 40-50, jelly powder 15-20, glycerine 4-5, borax 18-25, isocyanic ester 3-5, triethylamine 2-3, hydroxyl polysiloxane 3-4, poly-Synthesis of Oligo Ethylene Glycol 1-1.2, polyoxyethylene glycol monobutyl ether 0.5-0.8 and deionized water 100-120.
Fast setting binding agent, the weight part of its constitutive material is: silicate cement 112, aqueous polyurethane 35, polytetrahydrofuran diol 28, nanometer titanium dioxide 45, jelly powder 18, glycerine 4.5, borax 20, isocyanic ester 4, triethylamine 2.5, hydroxyl polysiloxane 3.5, poly-Synthesis of Oligo Ethylene Glycol 1.2, polyoxyethylene glycol monobutyl ether 0.6 and deionized water 110.
The making method of fast setting binding agent, comprises the following steps:
(1) each raw material is taken by the weight part of constitutive material, first jelly powder is added in the deionized water of formulation weight part half, be heated to 60-80 DEG C, be uniformly mixed, glycerine, hydroxyl polysiloxane and poly-Synthesis of Oligo Ethylene Glycol is added in whipping process, to be mixed evenly rear for subsequent use;
(2) aqueous polyurethane, polytetrahydrofuran diol are added in remaining half deionized water, after stirring, add borax, isocyanic ester and triethylamine, regulate Ph to neutral, be heated to 45-50 DEG C, stir for subsequent use;
(3) standby material of combining step (1), (2), then adds silicate cement and stirs rapidly, adds other residue constitutive material more wherein, be heated to 85-95 DEG C and stir 30-60min, be cooled to 45 DEG C with bottom discharge after stirring.
Beneficial effect of the present invention:
The present invention prepares binding agent and not only has the adhesiveproperties close with binding agent in prior art, the base material used is more extensive, and there is better curing speed, and simultaneously good with ageing-resistant performance in addition, save the advantage in energy consumption and extension device work-ing life.
Embodiment
Embodiment 1: fast setting binding agent, the weight part (kg) of its constitutive material is: silicate cement 112, aqueous polyurethane 35, polytetrahydrofuran diol 28, nanometer titanium dioxide 45, jelly powder 18, glycerine 4.5, borax 20, isocyanic ester 4, triethylamine 2.5, hydroxyl polysiloxane 3.5, poly-Synthesis of Oligo Ethylene Glycol 1.2, polyoxyethylene glycol monobutyl ether 0.6 and deionized water 110.
The making method of fast setting binding agent, comprises the following steps:
(1) each raw material is taken by the weight part of constitutive material, first jelly powder is added in the deionized water of formulation weight part half, be heated to 70 DEG C, be uniformly mixed, glycerine, hydroxyl polysiloxane and poly-Synthesis of Oligo Ethylene Glycol is added in whipping process, to be mixed evenly rear for subsequent use;
(2) aqueous polyurethane, polytetrahydrofuran diol are added in remaining half deionized water, after stirring, add borax, isocyanic ester and triethylamine, regulate Ph to neutral, be heated to 45-50 DEG C, stir for subsequent use;
(3) standby material of combining step (1), (2), then adds silicate cement and stirs rapidly, adds other residue constitutive material more wherein, be heated to 90 DEG C and stir 50min, be cooled to 45 DEG C with bottom discharge after stirring.
The performance index of above-mentioned obtained binding agent: titre: 55 droplets/minute, rate of drying 25-30 minute; Bond strength: 12-15Kgf/10cm is stupefied; Ultimate compression strength 650-680Kgf.
Claims (3)
1. a fast setting binding agent, is characterized in that the weight part of its constitutive material is: silicate cement 110-115, aqueous polyurethane 30-40, polytetrahydrofuran diol 25-30, nanometer titanium dioxide 40-50, jelly powder 15-20, glycerine 4-5, borax 18-25, isocyanic ester 3-5, triethylamine 2-3, hydroxyl polysiloxane 3-4, poly-Synthesis of Oligo Ethylene Glycol 1-1.2, polyoxyethylene glycol monobutyl ether 0.5-0.8 and deionized water 100-120.
2. fast setting binding agent according to claim 1, is characterized in that the weight part of its constitutive material is: silicate cement 112, aqueous polyurethane 35, polytetrahydrofuran diol 28, nanometer titanium dioxide 45, jelly powder 18, glycerine 4.5, borax 20, isocyanic ester 4, triethylamine 2.5, hydroxyl polysiloxane 3.5, poly-Synthesis of Oligo Ethylene Glycol 1.2, polyoxyethylene glycol monobutyl ether 0.6 and deionized water 110.
3. a making method for fast setting binding agent as claimed in claim 1, is characterized in that comprising the following steps:
(1) each raw material is taken by the weight part of constitutive material, first jelly powder is added in the deionized water of formulation weight part half, be heated to 60-80 DEG C, be uniformly mixed, glycerine, hydroxyl polysiloxane and poly-Synthesis of Oligo Ethylene Glycol is added in whipping process, to be mixed evenly rear for subsequent use;
(2) aqueous polyurethane, polytetrahydrofuran diol are added in remaining half deionized water, after stirring, add borax, isocyanic ester and triethylamine, regulate pH to neutral, be heated to 45-50 DEG C, stir for subsequent use;
(3) standby material of combining step (1), (2), then adds silicate cement and stirs rapidly, adds other residue constitutive material more wherein, be heated to 85-95 DEG C and stir 30-60min, be cooled to 45 DEG C with bottom discharge after stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410535418.2A CN104326715B (en) | 2014-10-13 | 2014-10-13 | A kind of fast setting binding agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410535418.2A CN104326715B (en) | 2014-10-13 | 2014-10-13 | A kind of fast setting binding agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104326715A CN104326715A (en) | 2015-02-04 |
| CN104326715B true CN104326715B (en) | 2016-03-16 |
Family
ID=52401542
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410535418.2A Expired - Fee Related CN104326715B (en) | 2014-10-13 | 2014-10-13 | A kind of fast setting binding agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104326715B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114155684A (en) * | 2021-12-21 | 2022-03-08 | 中国地质调查局水文地质环境地质调查中心 | Geological disaster rainfall emergency monitoring and early warning system |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19919163A1 (en) * | 1999-04-28 | 2000-11-02 | Bayer Ag | Binders containing isocyanate |
| US7919567B2 (en) * | 2006-06-07 | 2011-04-05 | Dow Global Technologies Llc | Oligomeric halogenated chain extenders for preparing epoxy resins |
| CN101357976B (en) * | 2007-07-31 | 2011-04-27 | 上海富臣化工有限公司 | Ambient self-crosslinking waterborne polyurethane dispersion and preparation method thereof |
| CN101298548B (en) * | 2008-06-13 | 2012-01-04 | 江苏科技大学 | Epoxy modified polyurethane cryogenic adhesive |
| CN102558828A (en) * | 2011-12-29 | 2012-07-11 | 华南理工大学 | Method for preparing polyurethane hybridization material for hydroxyl-containing filler |
-
2014
- 2014-10-13 CN CN201410535418.2A patent/CN104326715B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN104326715A (en) | 2015-02-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103435925A (en) | Environmental-friendly packing material and preparation method thereof | |
| CN103030301A (en) | Glass frosting powder for processing anti-dazzle glass and preparation method thereof | |
| CN104804662A (en) | Glutinous rice wet glue for wallpaper and preparation method of glutinous rice wet glue | |
| CN104386999A (en) | Fireproof acoustic panel | |
| CN104326715B (en) | A kind of fast setting binding agent and preparation method thereof | |
| CN104371343A (en) | High-performance plant fiber packaging material and preparation method thereof | |
| CN102040747B (en) | Plant modified polymer powder | |
| CN105462515A (en) | Starch adhesive and preparation method thereof | |
| CN103921382A (en) | Latex glove preparation method | |
| CN105155338A (en) | Anti-ultraviolet (UV) water-based paper impregnant and preparation method thereof | |
| CN104861899A (en) | Adhesive composition for plywood and preparation process of adhesive composition | |
| CN107163218A (en) | A kind of Precasting synthetic surface track and its manufacture method | |
| CN105646723B (en) | A kind of dialdehyde starch and preparation method thereof | |
| CN103739801B (en) | Raw materials of resin adhesive for sympodial bamboo integrated profile and preparation method of resin adhesive | |
| CN104177660A (en) | Degradable plastic formula | |
| CN103131379B (en) | High-elasticity and high-stretchability shadowless glue and preparation method thereof | |
| CN102051083A (en) | Environmentally-friendly crack-resistant exterior wall putty powder and preparation process thereof | |
| CN104909657A (en) | Thermal insulation energy-saving environmentally friendly plant fiber cement composite plate and producing method thereof | |
| CN103525078A (en) | Footwear leather environment-friendly type solvent-free foaming base material and preparation method thereof | |
| CN104327749B (en) | Insulating adhesive and making method thereof | |
| CN104530379A (en) | Single-component polyurethane material for preparing waterproof glue and preparation method thereof | |
| CN103450580A (en) | Method for preparing board from waste polyurethane foam, waste plant fiber and waste polystyrene foam | |
| CN104876475A (en) | Ecological construction material | |
| CN103450505A (en) | Method for preparing board from waste polyurethane foam, waste plant fiber and waste xylonite | |
| CN107916080A (en) | A kind of environmental protection type packing binding agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180917 Address after: 510800 A3, East Xiu Road, Xinhua Street, Huadu District, Guangzhou, Guangdong Patentee after: GUANGZHOU BONXL ENVIRONMENTAL PROTECTION BUILDING MATERIALS CO., LTD. Address before: 230601 room 803, 25 West Wen Jin new town, jadeite Road, Hefei, Anhui Patentee before: HEFEI TINGSUO ENVIRONMENTAL PROTECTION MATERIALS CO., LTD. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160316 Termination date: 20181013 |