CN104313603B - Stud welding unit sanitising agent - Google Patents
Stud welding unit sanitising agent Download PDFInfo
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- CN104313603B CN104313603B CN201410451988.3A CN201410451988A CN104313603B CN 104313603 B CN104313603 B CN 104313603B CN 201410451988 A CN201410451988 A CN 201410451988A CN 104313603 B CN104313603 B CN 104313603B
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- methyl
- welding unit
- stud welding
- sanitising agent
- acid ester
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
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Abstract
The present invention relates to stud welding unit sanitising agent, belong to cleaning supplies technical field.It is by water, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, (1S; 4R; 6R)-1; the raw materials such as 7,7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate, methyl cyclopentenyl ketone are prepared from.This stud welding unit sanitising agent, preparation section is simple, cleaning force is strong, the dirt clean effect common to stud welding unit is especially remarkable, and stable chemical nature under its high temperature, be suitable for HIGH TEMPERATURE PURGE, parts still can clean higher than during room temperature, clean consistent when cleaning performance and room temperature, there is important application value.
Description
Technical field
The present invention relates to stud welding unit sanitising agent, belong to cleaning supplies technical field.
Background technology
Stud welding unit is metallic stud or like parts, through pressurizeing instantaneously and discharging, thus whole end face is welded in the welding machine on workpiece.Although the emergence and development of stud welding unit is subjected only the process of decades, but because arc stud welding has the advantages such as the high and reliable in quality of total cross section welding, standardized work, efficiency, thus stud welding unit is used widely in industrial circle, researches and develops a kind of sanitising agent being applicable to stud welding unit very necessary.Because stud welding unit is that its working position temperature is higher, also very easily saves bit by bit greasy dirt to the pressurization of moment of part and electric discharge, therefore be suitable for HIGH TEMPERATURE PURGE and the strong stud welding unit sanitising agent of cleaning force exists great application prospect.
Summary of the invention
The object of the present invention is to provide and be a kind ofly suitable for HIGH TEMPERATURE PURGE and the strong stud welding unit sanitising agent of cleaning force.
Technical problem of the present invention, is achieved by the following technical programs:
Stud welding unit sanitising agent, special character is to be prepared from by the raw material of following weight: 75 parts, water, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 22-24 part, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 26-28 part, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 18-20 part, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 16-18 part, methyl cyclopentenyl ketone 12-14 part, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone 8-10 part, tetramethylolmethane three (3-'-aziridino) propionic ester 5-7 part, phenylbutazone 1-2 part.
By 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester adds successively in 75-90 DEG C of water bath with thermostatic control and mixes, add 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate again, methyl cyclopentenyl ketone, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone, tetramethylolmethane three (3-'-aziridino) propionic ester, phenylbutazone, stir, be cooled to 35-40 DEG C, left at room temperature 1 hour, i.e. obtained stud welding unit sanitising agent.
This stud welding unit sanitising agent, preparation section is simple, cleaning force is strong, the dirt clean effect common to stud welding unit is especially remarkable, and stable chemical nature under its high temperature, be suitable for HIGH TEMPERATURE PURGE, parts still can clean higher than during room temperature, clean consistent when cleaning performance and room temperature, there is important application value.
Embodiment
Below provide the specific embodiment of the present invention, be used for being further described the present invention.In the present invention, if no special instructions, each raw material all in working substance content for 100%.
In following examples and comparative example, raw material introduction:
1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, CAS accession number: 53-86-1;
(1S, 4R, 6R)-1,7,7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester, CAS accession number: 76-50-6;
1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester, CAS accession number: 89-48-5;
8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate, CAS accession number: 51-56-9;
Methyl cyclopentenyl ketone, CAS accession number: 80-71-7;
Six hydrogen-3a, 7a-dimethyl-4,7-epoxyisobenzofuran-1,3-diketone, CAS accession number: 56-25-7;
Tetramethylolmethane three (3-'-aziridino) propionic ester, CAS accession number: 57116-45-7;
Phenylbutazone, CAS accession number: 50-33-9.
Embodiment 1
Weigh: water 75kg, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 23kg, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 28kg, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 18kg, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 17kg, methyl cyclopentenyl ketone 14kg, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone 9kg, tetramethylolmethane three (3-'-aziridino) propionic ester 5kg, phenylbutazone 1kg.
The present embodiment stud welding unit sanitising agent preparation method: by 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester adds successively in 75-90 DEG C of water bath with thermostatic control and mixes, add 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate again, methyl cyclopentenyl ketone, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone, tetramethylolmethane three (3-'-aziridino) propionic ester, phenylbutazone, stir, be cooled to 35-40 DEG C, left at room temperature 1 hour, i.e. this stud welding unit sanitising agent obtained.
Embodiment 2
Weigh: water 75kg, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 24kg, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 27kg, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 20kg, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 18kg, methyl cyclopentenyl ketone 12kg, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone 10kg, tetramethylolmethane three (3-'-aziridino) propionic ester 7kg, phenylbutazone 2kg.
The preparation method of this embodiment stud welding unit sanitising agent is with embodiment 1.
Embodiment 3
Weigh: water 75kg, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 22kg, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 26kg, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 19kg, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 16kg, methyl cyclopentenyl ketone 13kg, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone 8kg, tetramethylolmethane three (3-'-aziridino) propionic ester 6kg, phenylbutazone 1.5kg.
The preparation method of this embodiment stud welding unit sanitising agent is with embodiment 1.
Comparative example 1
Weigh: water 75kg, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 23kg, (1S; 4R, 6R)-1,7; 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 28kg; 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 17kg, methyl cyclopentenyl ketone 14kg, six hydrogen-3a; 7a-dimethyl-4; 7-epoxyisobenzofuran-1,3-diketone 9kg, phenylbutazone 1kg.
This comparative example stud welding unit sanitising agent preparation method: by 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester adds successively in 75-90 DEG C of water bath with thermostatic control and mixes, add 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate again, methyl cyclopentenyl ketone, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone, phenylbutazone, stir, be cooled to 35-40 DEG C, left at room temperature 1 hour, i.e. this comparative example stud welding unit sanitising agent obtained.
Comparative example 2
Weigh: water 75kg; 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 23kg; 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 18kg; 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 17kg, six hydrogen-3a, 7a-dimethyl-4; 7-epoxyisobenzofuran-1; 3-diketone 9kg, tetramethylolmethane three (3-'-aziridino) propionic ester 5kg, phenylbutazone 1kg.
This comparative example stud welding unit sanitising agent preparation method: by 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester adds successively in 75-90 DEG C of water bath with thermostatic control and mixes, add 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate again, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone, tetramethylolmethane three (3-'-aziridino) propionic ester, phenylbutazone, stir, be cooled to 35-40 DEG C, left at room temperature 1 hour, i.e. this comparative example stud welding unit sanitising agent obtained.
Test case
Choose a certain region of stud welding unit processing component as test zone, processing component entirety is weighed W1, and test zone applies the dirt that one deck is about 60g, roasting 2 hours at 1000 DEG C, test zone temperature reaches 300 DEG C, rear check weighing W2.
1. 5g stud welding unit sanitising agent is evenly sprayed on parts fouled surfaces, ambient temperatare puts 5 minutes, then evenly sprays tap water, check weighing W3 after 2 minutes.Soil removal efficiency is drawn by weighting method.
Above-mentioned dirt is made up of 60wt% machine oil, 20wt% pitch, 10wt% dust, 5wt% pitch, 5wt% particulate sugar.
As shown in the table to stud welding unit processing component cleaning effect at 300 DEG C:
Soil removal efficiency=[(W2-W3)/(W2-W1)] * 100%
| Soil removal efficiency, % | |
| Embodiment 1 | 98.5 |
| Embodiment 2 | 98.7 |
| Embodiment 3 | 97.8 |
| Comparative example 1 | 82.1 |
| Comparative example 2 | 62.4 |
2. test zone is cooled, when being cooled to 20-30 DEG C, 5g stud welding unit sanitising agent is evenly sprayed on parts fouled surfaces, leave standstill 5 minutes, then evenly spray tap water, check weighing W3 after 2 minutes.Soil removal efficiency is drawn by weighting method.
Above-mentioned dirt is made up of 60wt% machine oil, 20wt% pitch, 10wt% dust, 5wt% pitch, 5wt% particulate sugar.
As shown in the table to stud welding unit processing component cleaning effect at 20-30 DEG C:
Soil removal efficiency=[(W2-W3)/(W2-W1)] * 100%
| Soil removal efficiency, % | |
| Embodiment 1 | 98.7 |
| Embodiment 2 | 98.9 3 --> |
| Embodiment 3 | 97.8 |
| Comparative example 1 | 82.4 |
| Comparative example 2 | 62.2 |
Claims (1)
1. stud welding unit sanitising agent, it is characterized in that being prepared from by the raw material of following weight: 75 parts, water, 1-(4-chlorobenzene formacyl)-5-methoxyl group-2-Methyl-1H-indole-3-acetic acid 22-24 part, (1S, 4R, 6R)-1, 7, 7-trimethylammonium two ring [2.2.1]-2-in heptan base 3 Methylbutanoic acid ester 26-28 part, 1-isopropyl-4-methyl cyclohexyl-2-alcohol acetic ester 18-20 part, 8-methyl-8-azabicyclo [3.2.1] pungent-3-alcohol alpha-hydroxyl phenylacetic acid ester hydrobromate 16-18 part, methyl cyclopentenyl ketone 12-14 part, six hydrogen-3a, 7a-dimethyl-4, 7-epoxyisobenzofuran-1, 3-diketone 8-10 part, tetramethylolmethane three (3-'-aziridino) propionic ester 5-7 part, phenylbutazone 1-2 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410451988.3A CN104313603B (en) | 2014-09-08 | 2014-09-08 | Stud welding unit sanitising agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410451988.3A CN104313603B (en) | 2014-09-08 | 2014-09-08 | Stud welding unit sanitising agent |
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| Publication Number | Publication Date |
|---|---|
| CN104313603A CN104313603A (en) | 2015-01-28 |
| CN104313603B true CN104313603B (en) | 2016-04-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410451988.3A Expired - Fee Related CN104313603B (en) | 2014-09-08 | 2014-09-08 | Stud welding unit sanitising agent |
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Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3470571D1 (en) * | 1983-07-22 | 1988-05-26 | Kao Corp | Metal cleaning compositions |
| CN103484270A (en) * | 2013-10-10 | 2014-01-01 | 青岛三立新源电器有限公司 | Efficient cleaning agent for machinery equipment |
| CN103668284A (en) * | 2013-11-19 | 2014-03-26 | 青岛汇而通商贸有限公司 | Cleaning agent for metal parts |
| CN103668280A (en) * | 2013-11-19 | 2014-03-26 | 青岛汇而通商贸有限公司 | Strong and fast cleaning agent |
| CN103668295B (en) * | 2013-12-18 | 2016-03-02 | 常熟市天河机械设备制造有限公司 | Bearing water-based clean-out system |
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| CN104313603A (en) | 2015-01-28 |
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Effective date of registration: 20210802 Address after: 528300 workshop 2, No. 1, No. 2, Xinglong 10th Road, Guanglong Industrial Zone, Shizhou village committee, Chencun Town, Shunde District, Foshan City, Guangdong Province Patentee after: Guangdong Yuegang heat treatment Co.,Ltd. Address before: 239000 No. 12, Shuixi village, Shuikou Town, Shuikou Town, Lai An county, Chuzhou, Anhui Patentee before: Liu Xinxia |
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Granted publication date: 20160427 |