CN104311146A - High-temperature-resisting coating composite material and preparation method thereof - Google Patents
High-temperature-resisting coating composite material and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a high-temperature-resisting coating composite material, and relates to the technical field of materials. The composite material comprises the following components: (1) epoxy resin and a curing agent, (2) titanium carbide, (3) nano tin oxide, (4) rare earth oxide, (5) alumina silicate fiber, (6) graphite powder, (7) white carbon black and (8) glass fiber powder. A preparation method of the high-temperature resisting coating composite material comprises the following steps: (1) weighing; (2) performing high-temperature calcination; (3) grinding; and (4) mixing and curing. The high-temperature resisting coating composite material prepared by using the preparation method is prepared from multiple metal oxides and rare earth elements in a compounded manner, is excellent in high temperature resistance and wearing resistance, can effectively protect metal or ceramic when used on the surface of metal or ceramic, can avoid the influence of high temperature and corrosion on relevant properties of metal or ceramic, and is a very ideal high-temperature resisting coating material.
Description
Technical field
The invention belongs to field of material technology, particularly one is used for high-temperaure coating matrix materials such as pottery, metal and preparation method thereof.
Background technology
High temperature-resistant coating material be spread upon need to stand hot environment under the coating that uses, thermal conductivity is lower, high temperature effectively can be prevented for the damage of base material, can be used for as coated materials such as pottery, glass, metals.Existing high temperature-resistant coating material has inorganic type, organic type and inorganic organic mixed, every type all there is some superiority and corresponding not enough.
In pottery and metal field, while requiring resistance to elevated temperatures, the corrosion resistant performance of coated material and wear resisting property also be there are certain requirements, also require that coated material sticking power is good simultaneously, hard, long-time use can not be ftractureed non-foaming, keeps good endurance quality.
Application number is the patent documentation " preparation method of carbon/carbon/silicon carbide composite material surface refractory coating " of 200810150372.7, discloses a kind of high temperature-resistant coating material, the preparation method of high-temperaure coating, respectively metal zirconium powder is ground into ZR-I with the iodine sphere of powder
2mixed powder; Washing after the polishing of C/SIC matrix material being thrown, dries; C/SIC matrix material deposits SIC coating and pyrocarbon coating; C/SIC matrix material through above-mentioned steps process is embedded in ZR-I
2in mixed powder, with three layers of stainless steel vessel sealing; By 850 ~ 1100 DEG C of thermal treatment 5 ~ 30 hours under argon atmospher protection in High Temperature Furnaces Heating Apparatus of three-layer sealed stainless steel vessel, then cool to room temperature with the furnace; Point layer open in the operation box of argon shield, takes out product.This is a kind of technical scheme utilizing carbon and silicon carbide to prepare high temperature material, is a kind of inorganic refractory materials, and hardness and the resistance to elevated temperatures of material all reach good level, and shortcoming is: preparation method is too complicated, and the rotproofness of material is poor.
Application number is the patent documentation " a kind of preparation method containing sulphur, silicon, nitrogen high-temperaure coating " of 201210246699.0, disclose a kind of coated material and preparation method thereof, described method comprises following process: the first step: by 4,4 dichloro diphenylsulfones and polyamine, silane, solvent, neutralizing agent react 2-3 hours in 0 DEG C-50 DEG C, removing by product, obtains the component A containing sulphur, silicon, nitrogen; Second step: glycidyl amine type epoxy resin, pigment, filler, flow agent, defoamer, dispersion agent and solvent are carried out mixed grinding and obtains component B; 3rd step: after being mixed in proportion by component A and component B, be coated on protected metallic surface, through 100 DEG C, 2-3 hours and 200 DEG C, is heating and curing, can forms high temperature resistant supercoat for 1-2 hours.
Disclosed in this technical scheme, the preparation method of high-temperaure coating is comparatively simple and easy, and the coating resistance to elevated temperatures of preparation is general, has certain erosion resistance and weathering resistance; comprehensive; this coating is only applicable to the protection of general material, and for metallic coating, its performance still can not meet the demands.
Summary of the invention
The technical problem that the present invention solves: for the defect of prior art, overcome the deficiencies in the prior art, the invention provides a kind of high-temperaure coating matrix material and preparation method thereof.
Technical scheme of the present invention: a kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 30-50 part, solidifying agent 5-11 part;
(2) titanium carbide, 3.5-6.5 part;
(3) nano tin dioxide, 3-6 part
(4) rare earth oxide, 5-7 part;
(5) aluminum silicate fiber, 5-9 part;
(6) Graphite Powder 99,5-10 part;
(7) white carbon black, 3.5-7.5 part;
(8) glass fibre, 3-7 part.
As preferably, solidifying agent is amine curing agent.
As preferably, solidifying agent is Versamid, aliphatic diamine or aromatic polyamine.
As preferably, rare earth oxide is one or more of Praseodymium trioxide, Neodymium trioxide, yttrium oxide or lanthanum trioxide.
As preferably, rare earth oxide is Praseodymium trioxide or yttrium oxide.
A preparation method for high-temperaure coating matrix material, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 0.1-2um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add solidifying agent, stir, namely obtain high-temperaure coating matrix material.
As preferably, in step (2), the temperature of high-temperature calcination is 500-800 DEG C.
As preferably, in step (2), the time of high-temperature calcination is 1-3h.
Beneficial effect: high-temperaure coating matrix material provided by the invention and preparation method thereof; comprise rare earth oxide for main raw with metal oxide; take epoxy resin as binding agent, a kind of stable performance of preparation is used for the high temperature-resistant coating material of metal or pottery protection.Be different from traditional method, simple various additive is simply mixing cured, the present invention is the performance ensureing coated material, first calcines constituent part, then pulverizes, form " high temperature resistant " material, this material has good resistance to elevated temperatures and wear resisting property, then by pigment shredder, powder and epoxy resin and related component is carried out Homogeneous phase mixing, last ambient cure, namely obtains high-temperaure coating matrix material.
High-temperaure coating matrix material provided by the invention is prepared from Multimetal oxide and rare earth element compound; there is excellent resistance to elevated temperatures and wear resisting property; for metal or ceramic surface; can available protecting metal or pottery; avoiding high temperature and corrode the impact on metal or ceramic correlated performance, is a kind of ideal high temperature-resistant coating material.
Embodiment
In order to understand the present invention further, below in conjunction with embodiment, the preferred embodiment of the invention is described, but should be appreciated that these describe just for further illustrating the features and advantages of the present invention, instead of limiting to the claimed invention.
Embodiment 1:
A kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 30 parts, polyamide curing agent 5 parts; (2) titanium carbide 3.5 parts; (3) nano tin dioxide 3 parts of (4) Praseodymium trioxides 5 parts; (5) aluminum silicate fiber 5 parts; (6) Graphite Powder 99 5 parts; (7) white carbon black 3.5 parts; (8) 3 parts, glass fibre.
Prepare above-mentioned high-temperaure coating matrix material according to preparation method provided by the invention, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine, temperature is 600 DEG C, time 2h;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 0.5um;
(4) join in powder by epoxy resin, glass fibre and white carbon black, put into water-powder mixer and mix, be mixed to evenly, take out, polymeric amide adds solidifying agent, stirs, and namely obtains high-temperaure coating matrix material.
Embodiment 2:
A kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 50 parts, polyamide curing agent 11 parts; (2) titanium carbide 6.5 parts; (3) nano tin dioxide 6 parts of (4) Praseodymium trioxides 7 parts; (5) aluminum silicate fiber 9 parts; (6) Graphite Powder 99 10 parts; (7) white carbon black 7.5 parts; (8) 7 parts, glass fibre.
Prepare above-mentioned high-temperaure coating matrix material according to preparation method provided by the invention, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine, temperature is 600 DEG C, time 2h;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 1um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add polyamide curing agent, stir, namely obtain high-temperaure coating matrix material.
Embodiment 3:
A kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 42 parts, polyamide curing agent 7 parts; (2) titanium carbide 5 parts; (3) nano tin dioxide 4.5 parts of (4) yttrium oxide 6 parts; (5) aluminum silicate fiber 6 parts; (6) Graphite Powder 99 7 parts; (7) white carbon black 5.5 parts; (8) 5 parts, glass fibre.
Prepare above-mentioned high-temperaure coating matrix material according to preparation method provided by the invention, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine, temperature is 700 DEG C, time 2h;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 0.5um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add solidifying agent, stir, namely obtain high-temperaure coating matrix material.
Embodiment 4:
A kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 40 parts, the two alkyl monomethyl tertiary amine 7 parts of solidifying agent; (2) titanium carbide 5 parts; (3) nano tin dioxide 4.5 parts of (4) yttrium oxide 6.5 parts; (5) aluminum silicate fiber 7 parts; (6) Graphite Powder 99 7.5 parts; (7) white carbon black 6 parts; (8) 6 parts, glass fibre.
Prepare above-mentioned high-temperaure coating matrix material according to preparation method provided by the invention, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine, temperature is 700 DEG C, time 2h;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 0.1um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add the two alkyl monomethyl tertiary amine of solidifying agent, stir, namely obtain high-temperaure coating matrix material.
Embodiment 5:
A kind of high-temperaure coating matrix material, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 45 parts, the two alkyl monomethyl tertiary amine 9 parts of solidifying agent; (2) titanium carbide 6 parts; (3) nano tin dioxide 5.5 parts of (4) lanthanum trioxides 5.5 parts; (5) aluminum silicate fiber 7 parts; (6) Graphite Powder 99 8 parts; (7) white carbon black 7 parts; (8) 6 parts, glass fibre.
Prepare above-mentioned high-temperaure coating matrix material according to preparation method provided by the invention, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine, temperature is 800 DEG C, time 1.5h;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 2um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add the two alkyl monomethyl tertiary amine of solidifying agent, stir, namely obtain high-temperaure coating matrix material.
Application number be 201210246699.0 patent documentation " a kind of preparation method containing sulphur, silicon, nitrogen high-temperaure coating " disclosed technical scheme prepares high-temperaure coating, is control group; Above-described embodiment and control group are carried out high temperature resistant and corrosion resistance nature mensuration, result is as shown in table 1:
Table 1 coated material is high temperature resistant and corrosion resistance nature measures
As seen from the above table, the acid resistance of embodiment 1-5 and control group is all better; Resistance to elevated temperatures and the alkaline resistance properties of embodiment 1-5 are better than control group.
In sum, high-temperaure coating matrix material of the present invention and preparation method thereof, provides a kind of coated material of corrosion-and high-temp-resistant.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (8)
1. a high-temperaure coating matrix material, is characterized in that, it is each component that matrix material comprises following mass fraction:
(1) epoxy resin and solidifying agent, the mass fraction of its epoxy resin is 30-50 part, solidifying agent 5-11 part;
(2) titanium carbide, 3.5-6.5 part;
(3) nano tin dioxide, 3-6 part
(4) rare earth oxide, 5-7 part;
(5) aluminum silicate fiber, 5-9 part;
(6) Graphite Powder 99,5-10 part;
(7) white carbon black, 3.5-7.5 part;
(8) glass fibre, 3-7 part.
2. high-temperaure coating matrix material according to claim 1, is characterized in that: solidifying agent is amine curing agent.
3. high-temperaure coating matrix material according to claim 2, is characterized in that: solidifying agent is Versamid, aliphatic diamine or aromatic polyamine.
4. high-temperaure coating matrix material according to claim 1, is characterized in that: rare earth oxide is one or more of Praseodymium trioxide, Neodymium trioxide, yttrium oxide or lanthanum trioxide.
5. high-temperaure coating matrix material according to claim 4, is characterized in that: rare earth oxide is Praseodymium trioxide or yttrium oxide.
6. a preparation method for the high-temperaure coating matrix material according to any one of claim 1-5, it is characterized in that, preparation process is as follows:
(1) each component of precise;
(2) titanium carbide, nano tin dioxide, rare earth oxide, aluminium silicate fiber peacekeeping Graphite Powder 99 are mixed, put into High Temperature Furnaces Heating Apparatus after mixing and calcine;
(3) after calcining, to be cooled to room temperature, take out, put into ball mill and grind, the median size to powder is 0.1-2um;
(4) epoxy resin, glass fibre and white carbon black are joined in powder, put into water-powder mixer and mix, be mixed to evenly, take out, add solidifying agent, stir, namely obtain high-temperaure coating matrix material.
7. the preparation method of high-temperaure coating matrix material according to claim 6, is characterized in that: in step (2), the temperature of high-temperature calcination is 500-800 DEG C.
8. the preparation method of high-temperaure coating matrix material according to claim 6, is characterized in that: in step (2), the time of high-temperature calcination is 1-3h.
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| CN104762618A (en) * | 2015-03-05 | 2015-07-08 | 上海应用技术学院 | Wear resistant coated plate for ore hoppers and preparation method thereof |
| CN104804554A (en) * | 2015-04-08 | 2015-07-29 | 牛无畏 | High weather-resistant multifunctional exterior wall coating material and preparation method thereof |
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| CN104762618A (en) * | 2015-03-05 | 2015-07-08 | 上海应用技术学院 | Wear resistant coated plate for ore hoppers and preparation method thereof |
| CN104804554A (en) * | 2015-04-08 | 2015-07-29 | 牛无畏 | High weather-resistant multifunctional exterior wall coating material and preparation method thereof |
| CN106380825A (en) * | 2016-09-09 | 2017-02-08 | 成都九十度工业产品设计有限公司 | Polyurethane acoustic-transmission rubber for spliced-ring energy converters |
| CN106497308A (en) * | 2016-09-30 | 2017-03-15 | 广西超星太阳能科技有限公司 | A kind of aluminium alloy covered |
| CN106497307A (en) * | 2016-09-30 | 2017-03-15 | 广西超星太阳能科技有限公司 | A kind of high-temperature-resistant and anti-corrosion aluminium alloy covered |
| CN106497309A (en) * | 2016-09-30 | 2017-03-15 | 广西超星太阳能科技有限公司 | A kind of aluminium alloy protective coating |
| CN106634405A (en) * | 2016-09-30 | 2017-05-10 | 广西超星太阳能科技有限公司 | Wear-resisting and high-temperature-resisting aluminum alloy coating |
| CN106928655A (en) * | 2017-02-10 | 2017-07-07 | 安徽键合科技有限公司 | A kind of interior delivery pipe exotic material of heat transfer pipeline and preparation method thereof |
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| CN108831606A (en) * | 2018-07-21 | 2018-11-16 | 江苏东强股份有限公司 | Rare earth power cable |
| CN108831606B (en) * | 2018-07-21 | 2024-04-02 | 江苏东强股份有限公司 | Rare earth power cable |
| CN111662635A (en) * | 2020-05-23 | 2020-09-15 | 广东日禾电器有限公司 | High-temperature-resistant protective coating material |
| CN117586696A (en) * | 2024-01-18 | 2024-02-23 | 宁波卓翔科技有限公司 | Ceramic organic-inorganic composite high-temperature anticorrosive paint |
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