CN104307586B - Solid material annealing device and processing method thereof under a kind of atmosphere - Google Patents
Solid material annealing device and processing method thereof under a kind of atmosphere Download PDFInfo
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- CN104307586B CN104307586B CN201410612568.9A CN201410612568A CN104307586B CN 104307586 B CN104307586 B CN 104307586B CN 201410612568 A CN201410612568 A CN 201410612568A CN 104307586 B CN104307586 B CN 104307586B
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- 238000000137 annealing Methods 0.000 title claims abstract description 21
- 239000011343 solid material Substances 0.000 title claims abstract description 17
- 238000003672 processing method Methods 0.000 title claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 38
- 238000000034 method Methods 0.000 claims description 5
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 230000000740 bleeding effect Effects 0.000 description 3
- 230000001276 controlling effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 1
- 230000005492 condensed matter physics Effects 0.000 description 1
- 239000002305 electric material Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
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Abstract
The invention discloses solid material annealing device and processing method thereof under a kind of atmosphere, annealing device comprises four-way pipe and heat treatment pipe, described four-way pipe has first mouth of pipe, second mouth of pipe, the 3rd mouth of pipe, the 4th mouth of pipe, described heat treatment pipe is connected with first mouth of pipe, described second mouth of pipe is provided with Pressure gauge, described 3rd mouth of pipe is provided with the first valve and is connected with vavuum pump, and described 4th mouth of pipe is provided with the second valve and is connected with gas tube.Processing method, comprises the following steps: pull down the first valve, sample is wrapped the bottom putting into heat treatment pipe, then is connected with four-way pipe by the first valve; Open the first valve, close the second valve, start to bleed by vavuum pump; Close the first valve, open the second valve, being filled with by gas tube needs gas; Close the second valve, the bottom of heat treatment pipe is heated.Apparatus structure is simple, and easy and simple to handle, cost is low.
Description
Technical field
The present invention relates to technical field of heat treatment equipment, especially relate to solid material annealing device and processing method thereof under a kind of atmosphere.
Background technology
Current in Condensed Matter Physics experiment, often need to regulate and control the molecularly oriented of material, such as, in organic sun electric material, regulatory molecule orientation can obtain higher efficiency.
When to material molecule orientation controlling, normally used method be carry out quenching or anneal under the environment of vacuum, gas doping etc., its principle is that temperature and gas can change molecular solids structure, and then regulatory molecule orientation.But required equipment is comparatively rare at present, and the equipment price of similar functions is very high, and complex structure, complex operation, conventional efficient is low.
Summary of the invention
Not enough for prior art, technical problem to be solved by this invention is to provide solid material annealing device and processing method thereof under a kind of atmosphere, simple to reach structure, object easy and simple to handle.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
Solid material annealing device under a kind of atmosphere, comprise four-way pipe and heat treatment pipe, described four-way pipe has first mouth of pipe, second mouth of pipe, the 3rd mouth of pipe, the 4th mouth of pipe, described heat treatment pipe is connected with first mouth of pipe, described second mouth of pipe is provided with Pressure gauge, described 3rd mouth of pipe is provided with the first valve and is connected with vavuum pump, and described 4th mouth of pipe is provided with the second valve and is connected with gas tube.
Described heat treatment pipe is stainless steel tube.
The outer end of described heat treatment pipe is provided with end socket.
Described first valve is ball valve.
Described second valve is needle-valve.
Described first mouth of pipe and the 3rd mouth of pipe are oppositely arranged.
Described second mouth of pipe is connected by pipeline with Pressure gauge, and is provided with relief valve on pipeline.
Be connected by screw thread between described end socket with heat treatment pipe.
Be connected by screw thread between described first valve with the 3rd mouth of pipe.
Utilize a processing method for solid material annealing device under described atmosphere, comprise the following steps:
1) pull down the first valve, sample is wrapped the bottom putting into heat treatment pipe, then the first valve is connected with four-way pipe;
2) open the first valve, close the second valve, start to bleed by vavuum pump;
3) close the first valve, open the second valve, being filled with by gas tube needs gas;
4) close the second valve, the bottom of heat treatment pipe is heated.
The present invention compared with prior art, has the following advantages:
Annealing device structure of the present invention is simple, and adopt standard component to complete, cost is low, and the various environment such as vacuum, gas doping, variations in temperature can be selected to heat-treat, and whole device is simple, easy and simple to handle, improves conventional efficient.
Accompanying drawing explanation
Below the content expressed by each width accompanying drawing of this description and the mark in figure are briefly described:
Fig. 1 is annealing device structural representation of the present invention.
In figure: 1. four-way pipe, 2. end socket, 3. Pressure gauge, 4. the first valve, 5. bleeding point, 6. the second valve, 7. gas tube.
Detailed description of the invention
Contrast accompanying drawing below, by the description to embodiment, the specific embodiment of the present invention is described in further detail.
As shown in Figure 1, solid material annealing device under this atmosphere, comprises four-way pipe 1 and heat treatment pipe and Pressure gauge 3, wherein, four-way pipe 1 has first mouth of pipe, second mouth of pipe, the 3rd mouth of pipe, the 4th mouth of pipe, four-way pipe 1 is cross structure, first mouth of pipe and the corresponding setting of the 3rd mouth of pipe, second mouth of pipe and the corresponding setting of the 4th mouth of pipe, four-way pipe 1 and heat treatment pipe are stainless steel tube, heat treatment pipe is long tube, and structure is simple, be convenient to make, and cost is low.
One end of heat treatment pipe and first mouth of pipe of four-way pipe 1 are by being welded and fixed and being connected, the other end of heat treatment pipe is provided with end socket 2, by end socket, this end is sealed, near end socket position, catch is installed in heat treatment pipe, to heat treated Sample location, be connected by screw thread between end socket 2 with heat treatment pipe, be convenient to pull down end socket, sample is put into heat treatment pipe.
By end socket 2 position mounting temperature sensor on heat treatment pipe, temperature sensor is connected with the display of outside, in heat treatment process, is convenient to control heating-up temperature.
Second mouth of pipe is provided with Pressure gauge 3.Have for, second mouth of pipe is connected by pipeline with Pressure gauge 3, and is provided with relief valve on pipeline, ensures reliability and security in heat treatment process by relief valve.The experimental needs of Pressure gauge can select the range of different accuracy, are convenient to directly observe inner air pressure.
3rd mouth of pipe being provided with the first valve 4, first valve 4 is ball valve, and ball valve Single port is bleeding point 5, and bleeding point 5 is connected with vavuum pump, is extracted out by the air in heat treatment pipe by vavuum pump, to avoid air to the interference of experiment.
Be connected by screw thread between first valve 4 with the 3rd mouth of pipe, the first valve adopts this structure, end socket 2 and heat treatment pipe welded seal can being got up, by pulling down the first valve, sample being put into the bottom position of heat treatment pipe.First valve can be dismantled repeatedly, for ensureing that air-tightness uses the sealing of O type circle.
4th mouth of pipe of four-way pipe 1 is provided with the second valve 6 and is connected with gas tube 7, by gas tube 7 with treat that the gas cylinder of inflatable body is connected, can experimentally need to select different gas.Second valve 6 is needle-valve, and noticeable degree is accurate, is convenient to the gas flow controlling to enter heat treatment pipe.
Utilize annealing device of the present invention to heat-treat the solid material under atmosphere, heat treatment method comprises the following steps:
Pull down the first valve, sample is wrapped the bottom putting into heat treatment pipe, then the first valve is connected with four-way pipe;
Open the first valve, close the second valve, start to bleed by vavuum pump, when manometric registration display heat treatment pipe inside pressure close to 0 time, close the first valve;
Open the second valve, by gas tube with treat that the gas cylinder of inflatable body is connected, being filled with by gas tube needs gas;
Close the second valve, the bottom of heat treatment pipe is heated.
Annealing device structure of the present invention is simple, and the various environment such as vacuum, gas doping, variations in temperature can be selected to heat-treat, and easy and simple to handle, cost is low.
Above by reference to the accompanying drawings to invention has been exemplary description; obvious specific implementation of the present invention is not subject to the restrictions described above; as long as have employed the improvement of the various unsubstantialities that design of the present invention and technical scheme are carried out; or design of the present invention and technical scheme directly applied to other occasion, all within protection scope of the present invention without to improve.
Claims (8)
1. solid material annealing device under an atmosphere, it is characterized in that: comprise four-way pipe and heat treatment pipe, described four-way pipe has first mouth of pipe, second mouth of pipe, the 3rd mouth of pipe, the 4th mouth of pipe, described heat treatment pipe is connected with first mouth of pipe, described second mouth of pipe is provided with Pressure gauge, described 3rd mouth of pipe is provided with the first valve and is connected with vavuum pump, and described 4th mouth of pipe is provided with the second valve and is connected with gas tube; The outer end of described heat treatment pipe is provided with end socket; Described first mouth of pipe and the 3rd mouth of pipe are oppositely arranged.
2. solid material annealing device under atmosphere as claimed in claim 1, is characterized in that: described heat treatment pipe is stainless steel tube.
3. solid material annealing device under atmosphere as claimed in claim 1, is characterized in that: described first valve is ball valve.
4. solid material annealing device under atmosphere as claimed in claim 1, is characterized in that: described second valve is needle-valve.
5. solid material annealing device under atmosphere as claimed in claim 1, is characterized in that: described second mouth of pipe is connected by pipeline with Pressure gauge, and is provided with relief valve on pipeline.
6. solid material annealing device under atmosphere as claimed in claim 1, be is characterized in that: be connected by screw thread between described end socket with heat treatment pipe.
7. solid material annealing device under atmosphere as claimed in claim 1, be is characterized in that: be connected by screw thread between described first valve with the 3rd mouth of pipe.
8. utilize a processing method for solid material annealing device under atmosphere as claimed in claim 1, it is characterized in that: the treating method comprises following steps:
1) pull down the first valve, sample is wrapped the bottom putting into heat treatment pipe, then the first valve is connected with four-way pipe;
2) open the first valve, close the second valve, start to bleed by vavuum pump;
3) close the first valve, open the second valve, being filled with by gas tube needs gas;
4) close the second valve, the bottom of heat treatment pipe is heated.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410612568.9A CN104307586B (en) | 2014-11-04 | 2014-11-04 | Solid material annealing device and processing method thereof under a kind of atmosphere |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410612568.9A CN104307586B (en) | 2014-11-04 | 2014-11-04 | Solid material annealing device and processing method thereof under a kind of atmosphere |
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| Publication Number | Publication Date |
|---|---|
| CN104307586A CN104307586A (en) | 2015-01-28 |
| CN104307586B true CN104307586B (en) | 2016-03-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410612568.9A Expired - Fee Related CN104307586B (en) | 2014-11-04 | 2014-11-04 | Solid material annealing device and processing method thereof under a kind of atmosphere |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107525406A (en) * | 2017-09-14 | 2017-12-29 | 华侨大学 | A kind of tubular type furnace system |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201245704Y (en) * | 2008-08-28 | 2009-05-27 | 上海宝钢设备检修有限公司 | Uniform injection apparatus for spray copper plate heat treatment remelting gas |
| CN201245687Y (en) * | 2008-08-28 | 2009-05-27 | 上海宝钢设备检修有限公司 | Flow capacity increasing device for spray copper plate heat treatment remelting gas |
| CN202893297U (en) * | 2012-11-14 | 2013-04-24 | 中国计量学院 | High-pressure heat treatment device |
| CN204247251U (en) * | 2014-11-04 | 2015-04-08 | 安徽师范大学 | Solid material annealing device under a kind of atmosphere |
-
2014
- 2014-11-04 CN CN201410612568.9A patent/CN104307586B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201245704Y (en) * | 2008-08-28 | 2009-05-27 | 上海宝钢设备检修有限公司 | Uniform injection apparatus for spray copper plate heat treatment remelting gas |
| CN201245687Y (en) * | 2008-08-28 | 2009-05-27 | 上海宝钢设备检修有限公司 | Flow capacity increasing device for spray copper plate heat treatment remelting gas |
| CN202893297U (en) * | 2012-11-14 | 2013-04-24 | 中国计量学院 | High-pressure heat treatment device |
| CN204247251U (en) * | 2014-11-04 | 2015-04-08 | 安徽师范大学 | Solid material annealing device under a kind of atmosphere |
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| CN104307586A (en) | 2015-01-28 |
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