CN104293129A - Tasteless high-transparency full-matt top-coat paint and preparation method thereof - Google Patents
Tasteless high-transparency full-matt top-coat paint and preparation method thereof Download PDFInfo
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- CN104293129A CN104293129A CN201410479289.XA CN201410479289A CN104293129A CN 104293129 A CN104293129 A CN 104293129A CN 201410479289 A CN201410479289 A CN 201410479289A CN 104293129 A CN104293129 A CN 104293129A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/08—Polyesters modified with higher fatty oils or their acids, or with natural resins or resin acids
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses tasteless high-transparency full-matt top-coat paint and a preparation method thereof. The method comprises the following steps: adding 75.0 percent of benzene-free net-flavor alkyd resin into a dispersing cylinder, regulating the rotating speed to 600-800 revolutions per minute, and stirring to be uniform; adding 0.2 percent of a dispersing agent, 0.2 percent of a defoaming agent and 0.2 percent of a feeling agent into the dispersing cylinder, regulating the rotating speed to 1200-1500 revolutions per minute, and stirring for 10-15 minutes; regulating the rotating speed to 600-800 revolutions per minute, slowly adding 0.5 percent of wax powder, 5.0 percent of extinction powder and 2.0 percent of anti-settling wax slurry, regulating the rotating speed to 1200-1500 revolutions per minute, and dispersing at a high speed for 15-30 minutes until the fineness is less than or equal to 25mu m; regulating the rotating speed to 600-800 revolutions per minute, sequentially adding 1.0 percent of feeling wax slurry, 1.5 percent of a flatting agent, 3.0 percent of a matting agent, 1.0 percent of a drying accelerant and 0.2 percent of a dryer, and dispersing for 10-15 minutes; and adding 4.0 percent of propylene glycol methyl ether acetate and 6.2 percent of n-butyl acetate into the dispersing cylinder, adjusting the viscosity to be qualified, thereby obtaining the paint. The paint disclosed by the invention is tasteless and nontoxic after being dried and is environment-friendly, the coated film has high transparency under full-matt glossiness of like products, the textures of woods are not influenced, and the paint has the advantages of uniform gloss distribution, high solvent corrosion resistance and the like.
Description
Technical field
The present invention relates to paint and preparation method thereof, be specifically related to a kind of clean complete mute clear finish of taste higher-grade and preparation method thereof.
Background technology
Existing furniture generally adopts solid wood or imitative solid wood material to make, and its surface usually adopts paint as surfacecti proteon, outermost layer by spraying varnish to strengthen its luminance brightness and slickness, aesthetic property and water proof anti-soil performance.But, the varnish colour that various furniture uses now, smell is large, containing triphen, has certain injury to human body, and the coating products of full dumb light often occurs that gloss distributing homogeneity is not good, poor transparency, causes laccase prodution, can not appear the grain of timber itself, the variation such as sight, the loose corrosion being easily subject to organic solvent and family expenses daily necessities of compact in paint film degree causes furniture to shorten work-ing life.
The patent of invention that name is called " a kind of three light splitting clear finishs and preparation method thereof " is disclosed in the Chinese patent that application number is " 201310023977.0 ", its technical scheme is as follows: modified alkyd resin 65-70, dimethylbenzene 8-10, dispersion agent 0.15-0.25, defoamer 0.08-0.12, white slurry 4-5, flatting silica 3.5-4.5, wax slurry 0.2-0.4, wax powder 0.4-0.6, methyl iso-butyl ketone (MIBK) 1.5-2.5, nitro-cotton liquid 2.5-3.5, pimelinketone 1.0-2.0, flow agent 0.3-0.4, ethylene glycol ether acetate 1-2, siccative 0.1-0.2, N-BUTYL ACETATE 4.5-5.5.Although clear finish of the present invention has stronger scratch resistance capability, its poor transparency, smell is heavier, and anti-organic solvent corrosive power is poor.
The patent of invention that name is called " a kind of seven light splitting clear finishs and preparation method thereof " is disclosed in the Chinese patent that application number is " 201310023183.4 ", its technical scheme is as follows: modified alkyd resin 110-115, Synolac, 115-125, dimethylbenzene 15-18, N-BUTYL ACETATE 7-9, toluene 13-15, dispersion agent 0.45-0.55, defoamer 0.4-0.5, flatting silica 7-9, wax slurry 0.8-1.2, nitro-cotton liquid 8-10, pimelinketone 4.5-5.5, flow agent 0.7-0.8, ethylene glycol ether acetate 4-6, siccative 0.5-0.7.Although clear finish of the present invention has stronger scratch resistance capability, its poor transparency, smell is heavier, and anti-organic solvent corrosive power is poor.
Summary of the invention
In order to solve the problem, the invention discloses a kind of clean complete mute clear finish of taste high transparency and preparation method thereof, having without triphen clean taste type, transparency is high, gloss is even, solvent resistant and the strong advantage of daily necessities corrosive nature.
A kind of clean complete mute clear finish of taste high transparency, is made up of (by weight percentage) following raw material: taste is without benzene Synolac 75.0% only, dispersion agent 0.2%, defoamer 0.2%, hand feeling agent 0.2%, wax powder 0.5%, flatting silica 5.0%, anti-settling wax slurry 2.0%, feel wax slurry 1.0%, flow agent 1.5%, delustring auxiliary agent 3.0%, dry promotor 1.0%, siccative 0.2%, solvent 10.2%.，
Further, described solvent is 1-Methoxy-2-propyl acetate 4.0%, N-BUTYL ACETATE 6.2%.
The making method of the complete mute clear finish of clean taste high transparency, comprises following processing step:
(1) first, clean taste is dropped in dispersion cylinder without benzene Synolac, under rotating speed being adjusted to 600-800r/min, dispersion agent, defoamer and hand feeling agent are dropped in dispersion cylinder, under rotating speed being adjusted to 1200-1500r/min state, stir 10-15 minute;
(2) slowly drop into wax powder, flatting silica and anti-settling wax slurry under rotating speed being adjusted to 600-800r/min state, then rotating speed is adjusted to 1200-1500r/min and disperses 15-30 minute, until fineness≤25 um;
(3) after rotating speed being recalled to 600-800r/min, feel wax slurry, flow agent, delustring auxiliary agent, dry promotor, siccative is dropped into successively, dispersion 10-15 minute;
(4) 1-Methoxy-2-propyl acetate and N-BUTYL ACETATE are dropped in dispersion cylinder, adjusting viscosity is qualified.
The invention has the advantages that: (1) clean taste is without the selected pure vegetable oil acid of benzene Synolac, and N-BUTYL ACETATE, and the environmentally friendly Raw material processing such as 1-Methoxy-2-propyl acetate forms, therefore, it is light that product has smell, has no irritating odor, the characteristic little to human injury; (2) with the addition of the composition such as flatting silica, delustring auxiliary agent in product, delustring auxiliary agent is the polymers soln containing acidic-group, there is following characteristic a, assist flatting silica at coating surface in paint drying process arranged evenly, make final gloss of film even; B, to use as dispersion agent, effectively shorten the required time being distributed to qualified fineness, save energy consumption; C, the dry process of quickening paint, the addition of flatting silica under identical gloss is reduced in a large number, thus makes the transparency of the finished product splendid, after spraying, the perception of product is effective; (3) flatting silica consumption reduce and wax slurry use, make coating surface hardness and density high, therefore, there is stronger anti-organic solvent and daily necessities corrosive property.
Embodiment
The invention discloses a kind of clean complete mute clear finish of taste high transparency and preparation method thereof, have without triphen clean taste type, transparency is high, gloss is even, solvent resistant and the strong advantage of daily necessities corrosive nature.
Be clearly and completely described to the technical scheme in the present invention below, obviously, described is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art obtain under the prerequisite of not making creative work, all belongs to the scope of protection of the invention.
A kind of clean complete mute clear finish of taste high transparency, is made up of (by weight percentage) following raw material: taste is without benzene Synolac 75.0% only, dispersion agent 0.2%, defoamer 0.2%, hand feeling agent 0.2%, wax powder 0.5%, flatting silica 5.0%, anti-settling wax slurry 2.0%, feel wax slurry 1.0%, flow agent 1.5%, delustring auxiliary agent 3.0%, dry promotor 1.0%, siccative 0.2%, solvent 10.2%., described solvent is 1-Methoxy-2-propyl acetate 4.0%, N-BUTYL ACETATE 6.2%.
A making method for the complete mute clear finish of clean taste high transparency, comprises following processing step:
(1) first, dropped in dispersion cylinder by clean taste without benzene Synolac, be adjusted to by rotating speed by dispersion agent under 600-800r/min, defoamer and hand feeling agent drop in dispersion cylinder, stir 10-15 minute under rotating speed being adjusted to 1200-1500r/min state;
(2) slowly drop into wax powder, flatting silica and anti-settling wax slurry under rotating speed being pulled back to 600-800r/min state, then rotating speed is adjusted to 1200-1500r/min and disperses 15-30 minute, until fineness≤25 um;
(3) after rotating speed being pulled back to 600-800r/min, drop into feel wax slurry, flow agent, delustring auxiliary agent, dry promotor, siccative successively, dispersion 10-15 minute;
(4) 1-Methoxy-2-propyl acetate and N-BUTYL ACETATE are dropped in dispersion cylinder, adjustment paint viscosity.
Specific embodiment is as follows:
Raw material used in following examples is commercially available, and when not having specified otherwise, unit is (kg):
Embodiment 1
Implementing process is as follows:
(1) first, according to the raw material in upper table and consumption, get out formula, and 210.0 parts of clean taste Synolac are dropped in reaction cylinder, rotating speed is adjusted to 650r/min, stirs, and then 0.6 part of dispersion agent, 0.6 part of defoamer and 0.6 part of hand feeling agent are dropped in reaction cylinder, rotating speed is adjusted to 1300r/min, stirs 12 minutes;
(2) then, slowly drop into 1.5 parts of wax powder, 27.0 parts of flatting silicas and 4.5 parts of anti-settling wax slurries after rotating speed being recalled to 650r/min, then rotating speed is adjusted to 1300r/min, stirs 12 minutes, until fineness≤25 um;
(3) after rotating speed being recalled to 650r/min, successively and drop into 1.5 parts of feel wax slurries, 3.3 parts of flow agents, 3.0 parts of delustring auxiliary agents, 3.0 parts of dry promotor, 0.6 part of siccative, disperse 12 minutes;
(4) 12.0 parts of 1-Methoxy-2-propyl acetates and 18.3 parts of N-BUTYL ACETATEs are dropped in dispersion cylinder, adjusting viscosity.
Embodiment 2
Implementing process is as follows:
(1) first, according to the raw material in upper table and consumption, get out formula, and 360.0 parts of clean taste Synolac are dropped in reaction cylinder, rotating speed is adjusted to 780r/min, stirs, and then 1.0 parts of dispersion agents, 1.0 parts of defoamers and 1.0 parts of hand feeling agents are dropped in reaction cylinder, rotating speed is adjusted to 1450r/min, stirs 15 minutes;
(2) then, slowly drop into 2.5 parts of wax powder, 45.0 parts of flatting silicas and 5.0 parts of anti-settling wax slurries after rotating speed being recalled to 780r/min, then rotating speed is adjusted to 1450r/min, stirs 15 minutes, until fineness≤25 um;
(3) after rotating speed being recalled to 780r/min, successively and drop into 2.5 parts of feel wax slurries, 5.5 parts of flow agents, 5.0 parts of delustring auxiliary agents, 5.0 parts of dry promotor, 1.0 parts of siccative, disperse 15 minutes;
(4) 20.0 parts of 1-Methoxy-2-propyl acetates and 30.5 parts of N-BUTYL ACETATEs are dropped in dispersion cylinder, adjusting viscosity.
Embodiment 3
Implementing process is as follows:
(1) first, according to the raw material in upper table and consumption, get out formula, and 75.0 parts of clean taste Synolac are dropped in reaction cylinder, rotating speed is adjusted to 600r/min, stirs, and then 0.2 part of dispersion agent, 0.2 part of defoamer and 0.2 part of hand feeling agent are dropped in reaction cylinder, rotating speed is adjusted to 1200r/min, stirs 10 minutes;
(2) then, slowly drop into 0.5 part of wax powder, 5.0 parts of flatting silicas and 2.0 parts of anti-settling wax slurries after rotating speed being recalled to 600r/min, then rotating speed is adjusted to 1300r/min, stirs 10 minutes, until fineness≤25 um;
(3) after rotating speed being recalled to 600r/min, successively and drop into 1.0 parts of feel wax slurries, 1.5 parts of flow agents, 3.0 parts of delustring auxiliary agents, 1.0 parts of dry promotor, 0.2 part of siccative, disperse 10 minutes;
(4) 4.0 parts of 1-Methoxy-2-propyl acetates and 6.2 parts of N-BUTYL ACETATEs are dropped in dispersion cylinder, adjusting viscosity.
Known by above embodiment, the invention has the advantages that: (1) clean taste is without the selected pure vegetable oil acid of benzene Synolac, and N-BUTYL ACETATE, the environmentally friendly Raw material processing such as 1-Methoxy-2-propyl acetate forms, therefore, it is light that product has smell, has no irritating odor, the characteristic little to human injury; (2) with the addition of the composition such as flatting silica, delustring auxiliary agent in product, delustring auxiliary agent is the polymers soln containing acidic-group, there is following characteristic a, assist flatting silica at coating surface in paint drying process arranged evenly, make final gloss of film even; B, to use as dispersion agent, effectively shorten the required time being distributed to qualified fineness, save energy consumption; C, the dry process of quickening paint, the addition of flatting silica under identical gloss is reduced in a large number, thus makes the transparency of the finished product splendid, after spraying, the perception of product is effective; (3) flatting silica consumption reduce and wax slurry use, make coating surface hardness and density high, therefore, there is stronger anti-organic solvent and daily necessities corrosive property.
Above content is in conjunction with concrete preferred implementation further description made for the present invention, can not assert that specific embodiment of the invention is confined to these explanations.For general technical staff of the technical field of the invention, without departing from the inventive concept of the premise, some simple deduction or replace can also be made, all should be considered as belonging to protection scope of the present invention.
Claims (3)
1. the complete mute clear finish of clean taste high transparency, is made up of (by weight percentage) following raw material: taste is without benzene Synolac 75.0% only, dispersion agent 0.2%, defoamer 0.2%, hand feeling agent 0.2%, wax powder 0.5%, flatting silica 5.0%, anti-settling wax slurry 2.0%, feel wax slurry 1.0%, flow agent 1.5%, delustring auxiliary agent 3.0%, dry promotor 1.0%, siccative 0.2%, solvent 10.2%.
2. the complete mute clear finish of one according to claim 1 clean taste high transparency, is characterized in that, described solvent is 1-Methoxy-2-propyl acetate 4.0%, N-BUTYL ACETATE 6.1%.
3. a making method for the complete mute clear finish of clean taste high transparency, is characterized in that, comprise following processing step:
(1) first, dropped in dispersion cylinder by clean taste without benzene Synolac, be adjusted to by rotating speed by dispersion agent under 600-800r/min, defoamer and hand feeling agent drop in dispersion cylinder, stir 10-15 minute under rotating speed being adjusted to 1200-1500r/min state;
(2) slowly drop into wax powder, flatting silica and anti-settling wax slurry under rotating speed being pulled back to 600-800r/min state, then rotating speed is adjusted to 1200-1500r/min and disperses 15-30 minute, until fineness≤25 um;
(3) after rotating speed being pulled back to 600-800r/min, drop into feel wax slurry, flow agent, delustring auxiliary agent, dry promotor, siccative successively, dispersion 10-15 minute;
(4) 1-Methoxy-2-propyl acetate and N-BUTYL ACETATE are dropped in dispersion cylinder, adjustment paint viscosity.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410479289.XA CN104293129B (en) | 2014-09-19 | 2014-09-19 | A kind of net taste high transparency mute clear finish and preparation method thereof entirely |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410479289.XA CN104293129B (en) | 2014-09-19 | 2014-09-19 | A kind of net taste high transparency mute clear finish and preparation method thereof entirely |
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| CN104293129A true CN104293129A (en) | 2015-01-21 |
| CN104293129B CN104293129B (en) | 2018-04-06 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106147552A (en) * | 2015-04-13 | 2016-11-23 | 富阳科信经济信息咨询有限公司 | A kind of environmental protection clean taste clear finish |
| CN108504267A (en) * | 2018-04-13 | 2018-09-07 | 苏州聚康新材料科技有限公司 | A kind of preparation method of high temperature resistant waterproof furniture lacquer |
| CN108997914A (en) * | 2018-08-09 | 2018-12-14 | 中山市大涂料有限公司 | A kind of PU matt varnish and preparation method thereof |
| CN112480755A (en) * | 2020-12-04 | 2021-03-12 | 浙江哈斯曼涂料有限公司 | Varnish with good waterproof effect |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103102777A (en) * | 2013-01-22 | 2013-05-15 | 重庆市品胜涂料有限公司 | Anti-yellowing quinary spectral white finish and preparation method thereof |
| CN104004169A (en) * | 2014-06-19 | 2014-08-27 | 嘉宝莉化工集团股份有限公司 | Modified alkyd resin, preparing method thereof and double-component matte top clearing paint |
-
2014
- 2014-09-19 CN CN201410479289.XA patent/CN104293129B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103102777A (en) * | 2013-01-22 | 2013-05-15 | 重庆市品胜涂料有限公司 | Anti-yellowing quinary spectral white finish and preparation method thereof |
| CN104004169A (en) * | 2014-06-19 | 2014-08-27 | 嘉宝莉化工集团股份有限公司 | Modified alkyd resin, preparing method thereof and double-component matte top clearing paint |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106147552A (en) * | 2015-04-13 | 2016-11-23 | 富阳科信经济信息咨询有限公司 | A kind of environmental protection clean taste clear finish |
| CN108504267A (en) * | 2018-04-13 | 2018-09-07 | 苏州聚康新材料科技有限公司 | A kind of preparation method of high temperature resistant waterproof furniture lacquer |
| CN108997914A (en) * | 2018-08-09 | 2018-12-14 | 中山市大涂料有限公司 | A kind of PU matt varnish and preparation method thereof |
| CN112480755A (en) * | 2020-12-04 | 2021-03-12 | 浙江哈斯曼涂料有限公司 | Varnish with good waterproof effect |
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| CN104293129B (en) | 2018-04-06 |
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