CN104291593A - Air-exhaust port sealing structure and manufacturing method thereof - Google Patents

Air-exhaust port sealing structure and manufacturing method thereof Download PDF

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Publication number
CN104291593A
CN104291593A CN201310298520.0A CN201310298520A CN104291593A CN 104291593 A CN104291593 A CN 104291593A CN 201310298520 A CN201310298520 A CN 201310298520A CN 104291593 A CN104291593 A CN 104291593A
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glass
unit
bleeding point
metal
lower fitting
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CN201310298520.0A
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戴长虹
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Priority to CN201310298520.0A priority Critical patent/CN104291593A/en
Publication of CN104291593A publication Critical patent/CN104291593A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

Abstract

The invention relates to an air-exhaust port sealing structure which is characterized in that upper glass of vacuum glass is perforated, such that an air-exhaust port is formed; an upper insertion part and a lower accommodation part are manufactured, wherein the upper insertion part is connected with the upper glass in a sealed manner, the lower accommodation part can retain liquid, and the upper insertion part is inserted into the lower accommodation part; after edge-sealing of the upper and lower glass, a metal solder is placed into the air-exhaust port or the upper insertion part; the air-exhaust port is vacuumed and heated, such that the metal solder is molten into liquid; the liquid is retained in the lower accommodation part, and the upper insertion part or the lower end thereof is also immersed in the liquid; according to a liquid sealing principle, the air-exhaust port is automatically sealed; when the temperature is reduced, the liquid is solidified, such that air-tight sealing of the air-exhaust port is realized. The method provided by the invention can be used in mass productions. With the method, vacuum glass production efficiency and qualification rate can be greatly improved, and production cost can be reduced.

Description

Sealed structure of bleeding point and preparation method thereof
Technical field
The invention belongs to vacuum glass field, particularly relate to sealed structure of a kind of bleeding point and preparation method thereof.
 
Background technology
Existing vacuum glass is generally made up of two pieces or three blocks of sheet glass, glass surrounding low temperature glass solder edge sealing, and there is small upholder centre, makes the thin vacuum layer forming 0.1 ~ 0.2mm thickness between two blocks of glass by bleeding.Owing to not having the heat transfer of gas, transaudient, the internal surface of glass can have again transparent low heat-emissive film, so vacuum glass has well heat insulation and soundproof effect, is one of best energy-saving glass of performance.
The gordian technique of existing vacuum glass has: one is edge sealing, and two is laying of upholder, and three is acquisition and maintenances of vacuum.The mode that existing vacuum glass obtains vacuum mainly contains the following two kinds: (1) is that first on a sheet glass, bleeding point is prepared in punching, then while adding hot edge seal with low temperature glass solder, on bleeding point, Glass tubing of bleeding is welded, finally heating vacuumizes the Glass tubing and sealing by fusing is bled, owing to bleeding, Glass tubing protrudes from glass surface, so also need to protect bleeding point position; (2) be do not need prefabricated bleeding point above glass, but glass edge being scribbled low temperature glass solder is placed in vacuum furnace after closing sheet, adds hot edge seal under vacuo and directly forms vacuum layer.The shortcoming of first kind of way is that evacuation process is complicated, production efficiency is very low: because pump-line is very thin, vacuum layer is very thin, pumping resistance is large, speed is little, and needs monolithic to extract, so production efficiency is very low; The second way can solve the shortcoming that first kind of way exists, but because low temperature glass solder is made up of many oxide, under a vacuum at high temperature, in the gas that volatile substances in the air of solder wettable and moisture, solder, solder dissolve in process of production and solder, the decomposition etc. of partial oxide all can cause in solder and produce a large amount of bubbles, greatly weaken the properties especially resistance to air loss of solder, cause the feasibility of this kind of mode to be greatly affected.Also have a kind of mode to be between above two kinds of modes, i.e. prefabricated bleeding point on glass, then after high temperature edge sealing, vacuumize again, finally utilize solder by seal weldings such as sheet metals on bleeding point; The shortcoming of which is if adopt glass solder, runs into the difficulty identical with the second way, if adopt brazing metal soldering, how making small and light sheet metal realize resistance to air loss welding under vacuum will run into very large difficulty, and its economic benefit is not necessarily better than first kind of way.
 
Summary of the invention
Technical problem to be solved by this invention is the defect being to exist for existing vacuum glass pumping hole, a kind of novel vacuum glass pumping hole and preparation method thereof is provided, the making method technique of this vacuum glass pumping hole is simple, made vacuum glass comprises toughened vacuum glass and can overcome deficiency of the prior art, effectively can ensure the work-ing life of the resistance to air loss of vacuum glass and heat insulation performance, prolongation vacuum glass, and can improve vacuum glass production efficiency, reduce production cost.
In order to solve the problems of the technologies described above, the invention provides a kind of sealed structure of bleeding point, it is characterized in that: on the upper glass of vacuum glass, bleeding point is made in punching, produce plug-in unit and lower fitting on one, described upper plug-in unit and described upper glass capsulation link together, and there is the passage connecting vacuum layer and bleeding point the centre of described upper plug-in unit, and described lower fitting can remaining liquid, described upper plug-in unit inserts in described lower fitting, is bleed-off passage between described upper plug-in unit and described lower fitting; After upper and lower glazing gasket brazing metal put into described bleeding point or on plug-in unit, being vacuumized by described bleeding point and heating makes described brazing metal be fused into liquid, described liquid retention is in described lower fitting, described upper plug-in unit or its lower end are also submerged in described liquid, utilize hydraulic seal principle by described bleeding point self-sealing, after cooling, described liquid solidifies, and realizes the airtight sealing to described bleeding point.
Wherein, described upper plug-in unit and described lower fitting are preferably made up of metal or glass, when described upper plug-in unit and described lower fitting are made of metal, preferably adopt the metal close with glass expansion coefficient; When described upper plug-in unit and described lower fitting are made up of glass, the preferably position paint metals slurry of plug-in unit and described lower fitting contacting metal solder on described, and utilize high temperature sintering metal paste, metal paste contributes to combining closely of brazing metal and glass.
Wherein, described upper plug-in unit and described lower fitting can be ring or the pipes of arbitrary shape;
Further, described upper plug-in unit and described lower fitting are the annulus concentric with described bleeding point or pipe;
Further, described upper plug-in unit is the pipe that edge is arranged at top.
Wherein, the described upper plug-in unit employing directly mode such as preparation or indirect welding is produced on described upper glass, and the modes such as the direct preparation of described lower fitting employing or indirectly welding are produced on described upper plug-in unit or described lower-glass.
Further, when described upper plug-in unit and described lower fitting adopt and directly prepare, glass paste, metal paste or the electric slurries etc. such as preferred employing cryogenic glass powder or glass ink utilize artificial or mechanical mode to be produced on described upper glass, form through high temperature sintering, the mode that the mode of described machinery preferably sprays or prints, can one to spraying for several times or printing one to several slurries;
Further, described lower fitting can be directly be prepared in pit on lower-glass or groove;
Further, when described upper plug-in unit and described lower fitting adopt indirect welding process to prepare, preferably adopt glass solder or metal paste welding; Described material is existing commercial commodity;
Further, described metal paste (or electric slurry) contributes to welding between brazing metal with glass, and described metal paste can also serve as the transition layer between glass paste and brazing metal;
Further, make the fusing point of its fusing point of material higher than glazing gasket low temperature glass solder or the use temperature of binding agent of described upper plug-in unit and described lower fitting, ensure that, in glazing gasket process, described wear ring does not change.
Wherein, described brazing metal comprises low-temperature metal solder and solder, and described material is existing commercial commodity.
Further, the fusing point of fusing point lower than glass solder of described brazing metal or the use temperature of binding agent, during brazing metal fusing, the glass solder of edge sealing or binding agent remain unchanged;
Further, the shape of described brazing metal is powdery, strip, sheet or bulk, ring-type, tubulose etc.
Wherein, the height of described liquid is preferably close with the degree of depth of described lower fitting.
Wherein, described in vacuumize and bleeding point sealing, can in vacuum furnace batch carry out, also can monolithic implement; Overallly can heat glass, also can local heating bleeding point.
Wherein, described heating, can adopt conventional heating, Infrared Heating, also can adopt induction heating, LASER HEATING, can also adopt microwave heating and other suitable heating unit or heater means.
Further, described heating, can heat bulk glass, also can local heating bleeding point.
Wherein, described bleeding point after brazing metal sealing, then uses sealant sealing, and be trade mark or the metal decorative sheet of product above seal gum, seal gum can protect brazing metal, can realize two seals again to bleeding point.
Further, described seal gum preferably has secret sealing, more preferably hot melt adhesive, hot-setting adhesive or two component sealing gum.
In order to solve the problems of the technologies described above, the invention provides the making method of above-mentioned vacuum glass pumping hole, it comprises:
The first step, according to the size of required making bleeding point, on upper glass, boring makes bleeding point;
Second step, plug-in unit in making, upper plug-in unit adopts the directly mode such as preparation or indirect welding to be produced on glass; Make lower fitting, the modes such as the direct preparation of lower fitting employing or indirectly welding are produced on plug-in unit or lower-glass; Upper plug-in unit inserts in lower fitting, leaves bleed-off passage between upper plug-in unit and lower fitting;
3rd step, after upper and lower glazing gasket, loads brazing metal in bleeding point or upper plug-in unit, and sends in vacuum furnace;
4th step, heating under vacuum sole is vacuumized, limit heating, be evacuated to below 0.1Pa, be warming up to more than the temperature of fusion of brazing metal, brazing metal is fused into liquid, liquid retention is in lower fitting, and upper plug-in unit or its lower end are also flooded in a liquid, and liquid is by bleeding point self-sealing; Stop heating, with stove cooling, brazing metal solidifies and realizes airtight sealing to bleeding point afterwards, opens vacuum furnace, takes out vacuum glass;
5th step, puts into seal gum in bleeding point, Paste Product trade mark or metal decorative sheet on seal gum.
Wherein, described upper plug-in unit and described lower fitting are preferably made up of metal or glass, when described upper plug-in unit and described lower fitting are made of metal, preferably adopt the metal close with glass expansion coefficient; When described upper plug-in unit and described lower fitting are made up of glass, the preferably position paint metals slurry of plug-in unit and described lower fitting contacting metal solder on described, and utilize high temperature sintering metal paste, metal paste contributes to combining closely of brazing metal and glass.
Wherein, described upper plug-in unit and described lower fitting can be ring or the pipes of arbitrary shape;
Further, described upper plug-in unit and described lower fitting are the annulus concentric with described bleeding point or pipe;
Further, described upper plug-in unit is the pipe that edge is arranged at top.
Wherein, the described upper plug-in unit employing directly mode such as preparation or indirect welding is produced on described upper glass, and the modes such as the direct preparation of described lower fitting employing or indirectly welding are produced on described upper plug-in unit or described lower-glass.
Further, when described upper plug-in unit and described lower fitting adopt and directly prepare, glass paste, metal paste or the electric slurries etc. such as preferred employing cryogenic glass powder or glass ink utilize artificial or mechanical mode to be produced on described upper glass, form through high temperature sintering, the mode that the mode of described machinery preferably sprays or prints, can one to spraying for several times or printing one to several slurries;
Further, described lower fitting can be directly be prepared in pit on lower-glass or groove;
Further, when described upper plug-in unit and described lower fitting adopt indirect welding process to prepare, preferably adopt glass solder or metal paste welding; Described material is existing commercial commodity;
Further, described metal paste (or electric slurry) contributes to welding between brazing metal with glass, and described metal paste can also serve as the transition layer between glass paste and brazing metal;
Further, make the fusing point of its fusing point of material higher than glazing gasket low temperature glass solder of described upper plug-in unit and described lower fitting, ensure that, in glazing gasket process, described wear ring does not change.
Wherein, described brazing metal comprises low-temperature metal solder and solder, and described material is existing commercial commodity.
Further, the fusing point of fusing point lower than glass solder of described brazing metal or the use temperature of binding agent, during brazing metal fusing, the glass solder of edge sealing or binding agent remain unchanged;
Further, the shape of described brazing metal is powdery, strip, sheet or bulk, ring-type, tubulose etc.
Wherein, the height of described liquid is preferably close with the degree of depth of described lower fitting.
Wherein, described in vacuumize and bleeding point sealing, can in vacuum furnace batch carry out, also can monolithic implement; Overallly can heat glass, also can local heating bleeding point.
Wherein, described heating, can adopt conventional heating, Infrared Heating, also can adopt induction heating, LASER HEATING, can also adopt microwave heating and other suitable heating unit or heater means.
Further, described heating, can heat bulk glass, also can local heating bleeding point.
Wherein, described seal gum preferably has secret sealing, more preferably hot melt adhesive, hot-setting adhesive or two component sealing gum.
Beneficial effect of the present invention:
Vacuum glass pumping hole of the present invention, with reference to " water seal " structure of the water exhaust system especially floor drain of falling bell-jar, according to hydraulic seal principle, is fused into the self-sealing of metal realization to bleeding point of liquid under utilizing high temperature, vacuum glass pumping hole structure of the present invention is simple, it is reliable, convenient for production, with low cost to seal, directly seal in a vacuum furnace, avoid the existing possibility of Glass tubing in melting moment air inlet of bleeding, and the exhaust temperature of glass can be improved, glass absorption and dissolved gases are thoroughly got rid of, can not there is chemical transformation in brazing metal under vacuum, solidify rear resistance to air loss good, effectively can ensure the vacuum tightness of vacuum glass vacuum layer, compared with the bleeding point of existing vacuum glass, its size of bleeding point of the present invention can be very large, its bleed-off passage sectional area is tens times of existing Glass tubing of bleeding to tens times, pumping resistance, inside and outside differential pressure is less, pumping speed, the vacuum tightness of vacuum layer is higher, thus be conducive to improving the heat insulation of vacuum glass, sound-proofing properties, extend its work-ing life, self-sealing in vacuum oven, can mass production, greatly can improve production efficiency and qualification rate, the reduction production cost of vacuum glass, the fusing point of brazing metal is easy to select, and can carry out entirety heating to toughened glass and ensure that toughened glass is unannealed, realize mass and make toughened vacuum glass.
 
Accompanying drawing explanation
Fig. 1 is the structural representation of the bleeding point of plug-in unit and lower fitting in direct preparation of the present invention;
Fig. 2 is the structural representation of the bleeding point of plug-in unit and lower fitting in indirect welding of the present invention.
In figure: 1. go up glass, 2. lower-glass, 3. brazing metal, 4. go up plug-in unit, 5. descends fitting, 6. seal gum, 7. trade mark or tinsel.
 
Embodiment
Below adopt embodiment and accompanying drawing to describe embodiments of the present invention in detail, to the present invention, how utilisation technology means solve technical problem whereby, and the implementation procedure reaching technique effect can fully understand and implement according to this.
Embodiment 1: see Fig. 1, vacuum glass is made up of upper glass 1 and lower-glass 2, upper glass 1 bores a through hole and forms bleeding point, the upper surface of the upper and lower glass of lower surface 2 of upper glass 1 utilize mechanical application or printing technology glass paste or metal paste print are made plug-in unit 4 and two lower fittings 5 on one concentric with bleeding point respectively, the upper plug-in unit 4 of upper glass 1 can insert between two lower fittings 5 of lower-glass 2, is bleed-off passage between upper plug-in unit 4 and lower fitting 5; Upper lower-glass is sent in High Temperature Furnaces Heating Apparatus or annealing furnace and make upper plug-in unit 4 sinter on upper lower-glass with lower fitting 5, then the upper lower-glass of low temperature glass solder in constant-pressure and high-temperature stove after involution piece is utilized to carry out edge sealing, after glass after edge sealing takes out from High Temperature Furnaces Heating Apparatus, while hot brazing metal 3 such as tin alloy is put into bleeding point, tin alloy foil is rolled into cylindrical shape, is inserted between plug-in unit 4 and lower fitting 5; Send in vacuum furnace with by glass, once can send into multiple pieces of glass; Heating under vacuum sole is vacuumized, limit heating, be evacuated to below 0.1Pa, be warming up to the temperature of fusion of brazing metal 3 tin alloy as more than 350 DEG C, brazing metal 3 tin alloy is fused into liquid retention in two lower fittings 5, upper plug-in unit 4 also floods in a liquid, and liquid is by bleeding point self-sealing; Stop heating, with stove cooling, brazing metal 3 tin alloy condenses into solid, realizes airtight sealing, open vacuum furnace to bleeding point, takes out vacuum glass.
Embodiment 2: see Fig. 2, vacuum glass is made up of upper glass 1 and lower-glass 2, the through hole that upper glass 1 bores a big upper and lower small mouth forms bleeding point, produce one with the metal at edge or Glass tubing as upper plug-in unit 4, edge and the upper glass 1 of upper plug-in unit 4 are welded together by glass solder or metal paste, and the top of upper plug-in unit 4 is lower than the upper surface of upper glass 1; Produce one with the metal of bottom or Glass tubing as lower fitting 5, lower fitting 5 connects together with upper plug-in unit 4 or is placed directly on lower-glass or is placed in the pit on lower-glass; When upper plug-in unit 4 adopts metal tube, preferably close with thermal expansion coefficient of glass metal as kovar alloy, when upper plug-in unit 4 and lower fitting 5 adopt Glass tubing, preferably at junction metallizing slurry, with reinforced seal effect; Upper plug-in unit 4 can insert in lower fitting 5, is bleed-off passage between upper plug-in unit 4 and lower fitting 5; The upper lower-glass of low temperature glass solder in constant-pressure and high-temperature stove after involution piece is utilized to carry out edge sealing, after glass after edge sealing takes out from High Temperature Furnaces Heating Apparatus, while hot by brazing metal 3 as zinc alloy puts into bleeding point or upper plug-in unit 4, send in vacuum furnace with by glass, once can send into multiple pieces of glass; Heating under vacuum sole is vacuumized, limit heating, be evacuated to below 0.1Pa, be warming up to the temperature of fusion of brazing metal 3 zinc alloy as more than 380 DEG C, brazing metal 3 zinc alloy is fused into liquid retention in lower fitting 5, the lower end of upper plug-in unit 4 is also flooded in a liquid, and liquid is by bleeding point self-sealing; Stop heating, with stove cooling, brazing metal 3 zinc alloy condenses into solid, realizes airtight sealing, open vacuum furnace to bleeding point, takes out vacuum glass.Seal gum 6 is put into while hot as butyl rubber, the product brand 7 of covering above of seal gum 6, the upper surface flush of trade mark 7 and upper glass 1 in bleeding point.
All above-mentioned this intellecture properties of primary enforcement, not setting restriction this product innovation of other forms of enforcement and/or novel method.Those skilled in the art will utilize this important information, and foregoing is revised, to realize similar implementation status.But all modifications or transformation belong to the right of reservation based on product innovation of the present invention.
The above is only preferred embodiment of the present invention, and be not restriction the present invention being made to other form, any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the Equivalent embodiments of equivalent variations.But everyly do not depart from technical solution of the present invention content, any simple modification, equivalent variations and the remodeling done above embodiment according to technical spirit of the present invention, still belong to the protection domain of technical solution of the present invention.

Claims (10)

1. the sealed structure of a bleeding point, it is characterized in that: on the upper glass of vacuum glass, bleeding point is made in punching, produce plug-in unit and lower fitting on one, described upper plug-in unit and described upper glass capsulation link together, there is the passage connecting vacuum layer and bleeding point the centre of described upper plug-in unit, described lower fitting can remaining liquid, and described upper plug-in unit inserts in described lower fitting, is bleed-off passage between described upper plug-in unit and described lower fitting; After upper and lower glazing gasket brazing metal put into described bleeding point or on plug-in unit, being vacuumized by described bleeding point and heating makes described brazing metal be fused into liquid, described liquid retention is in described lower fitting, described upper plug-in unit or its lower end are also submerged in described liquid, utilize hydraulic seal principle by described bleeding point self-sealing, after cooling, described liquid solidifies, and realizes the airtight sealing to described bleeding point.
2. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described upper plug-in unit and described lower fitting are made up of metal or glass; When described upper plug-in unit and described lower fitting are made of metal, preferably adopt the metal close with glass expansion coefficient; When described upper plug-in unit and described lower fitting are made up of glass, the preferably position paint metals slurry of plug-in unit and described lower fitting contacting metal solder on described, and utilize high temperature sintering metal paste.
3. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described upper plug-in unit adopts the mode of directly preparation or welding to be indirectly produced on described upper glass.
4. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described lower fitting adopts the mode of directly preparation or welding to be indirectly produced on described upper plug-in unit or described lower-glass.
5. the sealed structure of the bleeding point as described in claim 1 or 4, is characterized in that: described lower fitting is directly prepared in pit on lower-glass or groove.
6. the sealed structure of the bleeding point as described in claim 3 or 4, it is characterized in that: when described upper plug-in unit or lower fitting are directly prepared, adopt glass paste or metal paste one to spraying for several times or print one to several slurries on described upper glass or lower-glass, forming through high temperature sintering; When described upper plug-in unit or lower fitting weld preparation indirectly, metal ring or metal tube, glass ring or Glass tubing is adopted to utilize glass solder or metal paste to be welded on described upper glass or lower-glass.
7. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described brazing metal comprises low-temperature metal solder and solder.
8. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described in vacuumize with bleeding point sealing be utilize process furnace entirety heating glass or local heating bleeding point, batch carries out or monolithic is implemented.
9. the sealed structure of bleeding point as claimed in claim 1, is characterized in that: described bleeding point after brazing metal sealing, then uses sealant sealing, is trade mark or the metal decorative sheet of product above seal gum.
10. the making method of the vacuum glass pumping hole sealed structure described in any one of claim 1 to 9, is characterized in that, comprising:
The first step, according to the size of required making bleeding point, on upper glass, boring makes bleeding point;
Second step, plug-in unit in making, upper plug-in unit adopts the directly mode such as preparation or indirect welding to be produced on glass; Make lower fitting, the modes such as the direct preparation of lower fitting employing or indirectly welding are produced on plug-in unit or lower-glass; Upper plug-in unit inserts in lower fitting, leaves bleed-off passage between upper plug-in unit and lower fitting;
3rd step, after upper and lower glazing gasket, loads brazing metal in bleeding point or upper plug-in unit, and sends in vacuum furnace;
4th step, heating under vacuum sole is vacuumized, limit heating, be evacuated to below 0.1Pa, be warming up to more than the temperature of fusion of brazing metal, brazing metal is fused into liquid, liquid retention is in lower fitting, and upper plug-in unit or its lower end are also flooded in a liquid, and liquid is by bleeding point self-sealing; Stop heating, with stove cooling, brazing metal solidifies and realizes airtight sealing to bleeding point afterwards, opens vacuum furnace, takes out vacuum glass;
5th step, puts into seal gum in bleeding point, Paste Product trade mark or metal decorative sheet on seal gum.
CN201310298520.0A 2013-07-17 2013-07-17 Air-exhaust port sealing structure and manufacturing method thereof Withdrawn CN104291593A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
CN104291593A true CN104291593A (en) 2015-01-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106977117A (en) * 2016-01-18 2017-07-25 日立化成株式会社 Double glazing and its manufacture method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1676481A (en) * 2004-04-01 2005-10-05 唐健正 vacuum glass edge heating method and vacuum glass made thereby
US20120321822A1 (en) * 2009-11-27 2012-12-20 Luoyang Landglass Technology Co., Ltd Compound Sealing Method for Vacuum Glass
CN102976592A (en) * 2012-10-06 2013-03-20 戴长虹 Flat vacuum glass welded by using metal welding material and provided with strip frame edge sealing, and manufacturing method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1676481A (en) * 2004-04-01 2005-10-05 唐健正 vacuum glass edge heating method and vacuum glass made thereby
US20120321822A1 (en) * 2009-11-27 2012-12-20 Luoyang Landglass Technology Co., Ltd Compound Sealing Method for Vacuum Glass
CN102976592A (en) * 2012-10-06 2013-03-20 戴长虹 Flat vacuum glass welded by using metal welding material and provided with strip frame edge sealing, and manufacturing method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106977117A (en) * 2016-01-18 2017-07-25 日立化成株式会社 Double glazing and its manufacture method

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