CN104264449A - Antibiotic finishing method of silk fabric - Google Patents
Antibiotic finishing method of silk fabric Download PDFInfo
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- CN104264449A CN104264449A CN201410443709.9A CN201410443709A CN104264449A CN 104264449 A CN104264449 A CN 104264449A CN 201410443709 A CN201410443709 A CN 201410443709A CN 104264449 A CN104264449 A CN 104264449A
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- silk fabric
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Abstract
The invention discloses an antibiotic finishing method of a silk fabric. The method comprises the following steps: (1) preparing antibiotic finish liquor: uniformly mixing and stirring nanometer titanium oxide powder and deionized water, adding dispersing agent lauryl sodium sulfate and silane coupling agent kH560 in above mixed liquor, ultrasonically stirring for 30min; (2) warming the antibiotic finish liquor to 50-80 DEG.C, placing the silk fabric, dipping twice and rolling twice in the bath ratio of 1: 30 to 1: 60, wherein the pick-up rate is 80-90%; and (3) taking out the silk fabric, drying for 10min at 80 DEG.C, baking for 2-5min at 120-150 DEG.C to obtain the finished silk fabric. The silk fabric finished by using the method disclosed by the invention has good antibiotic performance, is long in validity, non-toxic, and in favor of environmental protection.
Description
Technical field:
The present invention relates to silk technical field of modification, relate to a kind of antibiotic finishing method of silk fabric specifically.
Background technology:
Along with the raising of quality of life, the requirement of people to health is more and more higher, but in life, people inevitably touch some microorganisms such as bacterium, fungi, and the place of natural fabric these microbial colonisation just, antibiotic finish must become the primary method improving natural fabric health.One of natural fabric that silk fabric is liked as people, its antibiotic finishing method is subject to the people's attention.Traditional antibiotic finishing method adds mercury salt, lead salt, hydrochlorate etc., and toxicity is large, the longevity of residure is long, has been prohibited from using; And although it is few to add synthesis organic bactericide consumption, effect is also better, there is the shortcomings such as the term of validity is short, toxicity is large, application surface is narrow, makes it apply and be restricted.Nano titania has excellent ultraviolet shielded, INFRARED ABSORPTION and photocatalysis performance, is applied in the antibiotic finish of silk fabric, makes silk fabric have uvioresistant, antibacterial and self-cleaning performance.
Summary of the invention:
The object of this invention is to provide a kind of antibiotic finishing method of silk fabric.The silk fabric that the method arranges has good anti-microbial property, and the term of validity is long, nontoxic, is conducive to environmental protection.
Object of the present invention is achieved through the following technical solutions:
An antibiotic finishing method for silk fabric, comprises the following steps:
(1) antibiotic finishing solution is prepared: get nano titania, deionized water mixing and stirring, in above-mentioned mixed liquor, add dispersant lauryl sodium sulfate, silane coupler KH560, ultrasonic agitation 30min;
(2) antibiotic finishing solution is warming up to 50-80 DEG C, puts into silk fabric, bath raio is 1:30-1:60, and two leachings two are pricked, and pick-up is 80%-90%;
(3) take out silk fabric, 80 DEG C are dried 10min, 120-150 DEG C and bake 2-5min, obtain the silk fabric after arranging.
Preferred as technique scheme, the particle diameter of the nano titania in described step (1) in antibiotic finishing solution is 5-10nm.
Preferred as technique scheme, each component in described step (1) in antibiotic finishing solution, with parts by weight, comprising: nano titania 2-10 part, lauryl sodium sulfate 1-5 part, silane coupler KH5601-5 part, deionized water 50-100 part.
Preferred as technique scheme, in described step (1), ultrasonic power is 400-500W.
Preferred as technique scheme, in described step (2), bath raio is 1:40.
Beneficial effect of the present invention is: after nano titanium oxide absorbs ultraviolet, and titanium dioxide inside generates electronics and hole.The electronics and the cavity energy that are diffused into surface participate in photocatalyst reaction: the hole that TiO2+UV → e-+h+2 is formed, there is very strong oxidability, with after the hydrone generation oxidation reaction of titanium dioxide surface, generate hydroxyl atomic group: h++HO → OH+H+2, hydroxyl has very high oxidability, can play oxidation reaction with organic compound.React Generation of atoms with oxygen molecule and roll into a ball chain reaction, final oxygen is consumed, and organic compound is decomposed, and becomes carbon dioxide and water, like this can killing microorganisms, also can be decomposed into biology and to depend on for existence the organic nutrient substance of procreation, reach antibacterial object.The silk fabric that the method arranges has good anti-microbial property, and the term of validity is long, nontoxic, is conducive to environmental protection.
Detailed description of the invention:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only for explaining the present invention, does not form limiting the scope of the present invention.Embodiment 1
(1) antibiotic finishing solution is prepared: with parts by weight, get nano titania 2 parts, deionized water 50 parts, mixing and stirring, dispersant lauryl sodium sulfate 1 part is added in above-mentioned mixed liquor, silane coupler KH5601 part, ultrasonic agitation 30min, ultrasonic power 400W;
(2) antibiotic finishing solution is warming up to 50 DEG C, puts into silk fabric, bath raio is 1:30, and two leachings two are pricked, and pick-up is 80%;
(3) take out silk fabric, 80 DEG C are dried 10min, and 120 DEG C bake 5min, obtain the silk fabric after arranging.
Embodiment 2
(1) antibiotic finishing solution is prepared: with parts by weight, get nano titania 10 parts, deionized water 100 parts, mixing and stirring, dispersant lauryl sodium sulfate 5 parts is added in above-mentioned mixed liquor, silane coupler KH5605 part, ultrasonic agitation 30min, ultrasonic power is 500W;
(2) antibiotic finishing solution is warming up to 80 DEG C, puts into silk fabric, bath raio is 1:60, and two leachings two are pricked, and pick-up is 90%;
(3) take out silk fabric, 80 DEG C are dried 10min, and 150 DEG C bake 2min, obtain the silk fabric after arranging.
Embodiment 3
(1) antibiotic finishing solution is prepared: with parts by weight, get nano titania 3 parts, deionized water 60 parts, mixing and stirring, dispersant lauryl sodium sulfate 2 parts is added in above-mentioned mixed liquor, silane coupler KH5602 part, ultrasonic agitation 30min, ultrasonic power is 400W;
(2) antibiotic finishing solution is warming up to 60 DEG C, puts into silk fabric, bath raio is 1:40, and two leachings two are pricked, and pick-up is 80%;
(3) take out silk fabric, 80 DEG C are dried 10min, and 130 DEG C bake 3min, obtain the silk fabric after arranging.
Embodiment 4
(1) antibiotic finishing solution is prepared: with parts by weight, get nano titania 4 parts, deionized water 70 parts, mixing and stirring, dispersant lauryl sodium sulfate 3 parts is added in above-mentioned mixed liquor, silane coupler KH5603 part, ultrasonic agitation 30min, ultrasonic power is 400W;
(2) antibiotic finishing solution is warming up to 70 DEG C, puts into silk fabric, bath raio is 1:50, and two leachings two are pricked, and pick-up is 90%;
(3) take out silk fabric, 80 DEG C are dried 10min, and 140 DEG C bake 4min, obtain the silk fabric after arranging.
Claims (5)
1. an antibiotic finishing method for silk fabric, is characterized in that comprising the following steps:
(1) antibiotic finishing solution is prepared: get nano titania, deionized water mixing and stirring, in above-mentioned mixed liquor, add dispersant lauryl sodium sulfate, silane coupler KH560, ultrasonic agitation 30min;
(2) antibiotic finishing solution is warming up to 50-80 DEG C, puts into silk fabric, bath raio is 1:30-1:60, and two leachings two are pricked, and pick-up is 80%-90%;
(3) take out silk fabric, 80 DEG C are dried 10min, 120-150 DEG C and bake 2-5min, obtain the silk fabric after arranging.
2. the antibiotic finishing method of a kind of silk fabric as claimed in claim 1, is characterized in that: the particle diameter of the nano titania in described step (1) in antibiotic finishing solution is 5-10nm.
3. the antibiotic finishing method of a kind of silk fabric as claimed in claim 1, it is characterized in that: each component in described step (1) in antibiotic finishing solution is with parts by weight, comprise: nano titania 2-10 part, lauryl sodium sulfate 1-5 part, silane coupler KH5601-5 part, deionized water 50-100 part.
4. the antibiotic finishing method of a kind of silk fabric as claimed in claim 1, is characterized in that: in described step (1), ultrasonic power is 400-500W.
5. the antibiotic finishing method of a kind of silk fabric as claimed in claim 1, is characterized in that: in described step (2), bath raio is 1:40.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410443709.9A CN104264449A (en) | 2014-09-03 | 2014-09-03 | Antibiotic finishing method of silk fabric |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410443709.9A CN104264449A (en) | 2014-09-03 | 2014-09-03 | Antibiotic finishing method of silk fabric |
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| CN104264449A true CN104264449A (en) | 2015-01-07 |
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| CN201410443709.9A Pending CN104264449A (en) | 2014-09-03 | 2014-09-03 | Antibiotic finishing method of silk fabric |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350278A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of antibiotic finish liquid for fabric |
| CN107724066A (en) * | 2017-09-30 | 2018-02-23 | 张建仁 | Perspire rapid-curing cutback nightwear and preparation method thereof |
| CN107938328A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of nano antibacterial finishing agent |
| CN108532289A (en) * | 2018-05-09 | 2018-09-14 | 重庆丝玛帛科技有限公司 | Multifunctional silk azelon finishing agent and Multifunctional silk azelon and its preparation process and application |
| CN111648134A (en) * | 2020-07-20 | 2020-09-11 | 刘开江 | Antistatic fabric and preparation method thereof |
| CN112647282A (en) * | 2020-12-29 | 2021-04-13 | 湖南寐家居科技有限公司 | Antibacterial finishing method of silk fabric |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350278A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of antibiotic finish liquid for fabric |
| CN107724066A (en) * | 2017-09-30 | 2018-02-23 | 张建仁 | Perspire rapid-curing cutback nightwear and preparation method thereof |
| CN107938328A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of nano antibacterial finishing agent |
| CN108532289A (en) * | 2018-05-09 | 2018-09-14 | 重庆丝玛帛科技有限公司 | Multifunctional silk azelon finishing agent and Multifunctional silk azelon and its preparation process and application |
| CN108532289B (en) * | 2018-05-09 | 2021-02-09 | 四川丝玛帛科技有限公司 | Multifunctional fibroin fiber finishing agent, multifunctional fibroin fiber, preparation process and application thereof |
| CN111648134A (en) * | 2020-07-20 | 2020-09-11 | 刘开江 | Antistatic fabric and preparation method thereof |
| CN112647282A (en) * | 2020-12-29 | 2021-04-13 | 湖南寐家居科技有限公司 | Antibacterial finishing method of silk fabric |
| CN112647282B (en) * | 2020-12-29 | 2022-03-15 | 湖南寐家居科技有限公司 | Antibacterial finishing method of silk fabric |
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Application publication date: 20150107 |