CN104212313A - Quick-drying friction-resisting high-temperature-resistant primer and preparation method thereof - Google Patents
Quick-drying friction-resisting high-temperature-resistant primer and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a quick-drying friction-resisting high-temperature-resistant primer. The primer consists of bisphenol F type liquid epoxy resin, iron oxide red powder, titanium dioxide, silicon micro-powder, a multifunctional auxiliary agent AMP-95, graphite powder, polyethylene glycol and organic fluorine modified acrylic resin; the primer comprises the following components in percentage by weight: 23-25% of bisphenol F type liquid epoxy resin, 5-8% of iron oxide red powder, 12-15% of titanium dioxide, 10-12% of silicon micro-powder, 15-18% of multifunctional auxiliary agent AMP-95, 12-15% of graphite powder, 3-8% of polyethylene glycol and the balance of organic fluorine modified acrylic resin. The invention also provides a preparation method of the quick-drying friction-resisting high-temperature-resistant primer. The primer disclosed by the invention is quick to dry, is odor-free, has stability in alkali and most of solvents, has good anti-corrosion, gas-blocking and water-stopping properties and the like, has good friction resistance and high temperature resistance, and is long in service life.
Description
Technical field
The present invention relates to a kind of priming paint and preparation method thereof, specifically a kind of quick-drying rub resistance, high temperature resistant primer and preparation method thereof.
Background technology
At present, need to be coated with priming after many mechanical surface treatment, its Main Function is that protection steel are subject to atomospheric corrosion less in the course of processing.Present priming paint kind is on the market more, but ubiquity is dry slowly, the defect of corrosion-resistant, heat-resisting ability difference, not only reduce the work-ing life of equipment, increase cost, and due to time of drying long, cause inefficiency, and easily give out chemical odor in the course of processing, bring harm to the healthy of operator.
Summary of the invention
Technical problem to be solved by this invention is, for the shortcoming of above prior art, propose a kind of quick-drying rub resistance, high temperature resistant primer and preparation method thereof, this priming paint has fast drying, free from extraneous odour, to alkali and most of solvent-stable; Anticorrosion, choke, the performance such as to block water are good, and rub resistance and the resistant to elevated temperatures performance of priming paint are good, and long service life.
In order to solve the problems of the technologies described above, technical scheme of the present invention is achieved in the following ways: a kind of quick-drying rub resistance, high temperature resistant primer, this priming paint is by bisphenol F-type epoxy resin, iron oxide red, titanium dioxide, silicon powder, multifunctional assistant AMP-95, Graphite Powder 99, polyoxyethylene glycol and the acrylic resin modified composition of organic fluorine, its weight percent composition is: bisphenol F-type epoxy resin: 23-25%, iron oxide red: 5-8%, titanium dioxide: 12-15%, silicon powder: 10-12%, multifunctional assistant AMP-95:15-18%, Graphite Powder 99: 12-15%, polyoxyethylene glycol: 3-8%, surplus is that organic fluorine is acrylic resin modified, the preparation method of this quick-drying rub resistance, high temperature resistant primer carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 60-62 DEG C, setting stirring velocity 900-920r/min, churning time 2-3h, then put into iron oxide red to continue to stir, churning time is 1-2h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 860-870r/min, churning time 1-2h, adds multifunctional assistant AMP-95 and continues to stir 40-50min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 750-800r/min, churning time 60-80min, and the temperature in control stirring tank is at 52-55 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2-3h, stirring velocity is 680-700r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
Like this, by technical scheme of the present invention, obtain a kind of quick-drying rub resistance, high temperature resistant primer, add the crocking resistance that Graphite Powder 99 improves priming paint in priming paint, multifunctional assistant AMP-95, the glossiness of priming paint can not only be improved, the PH stability that priming paint is extremely excellent can also be given, reduce corrosion, contribute to manufacturing low smell priming paint and being conducive to reducing priming paint cost, adding of iron oxide red not only improves the corrosion-resistant of priming paint and rustless property, and gives priming paint good outward appearance; Silicon powder add the chemical resistance further increasing priming paint; Barium sulfate add as a kind of heat-resistant filler, base-material can be made to thicken, compact in paint film, the lesion size of paint film can be reduced when hot-work, improve the physical and mechanical properties of paint film, the features such as organic fluorine modified acrylic acid resin primer had both remained the good alkali resistance of acrylic acid resin primer, protects look gloss retention, film is plentiful, have again that organic fluorine coating is weather-proof, resistant, corrosion-resistant and self-cleaning advantage.
The technical scheme that the present invention limits further is:
Aforesaid quick-drying rub resistance, high temperature resistant primer, priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 23%, iron oxide red: 5%, titanium dioxide: 12%, silicon powder: 10%, multifunctional assistant AMP-95:15%, Graphite Powder 99: 12%, polyoxyethylene glycol: 3%, surplus is that organic fluorine is acrylic resin modified.
Aforesaid quick-drying rub resistance, high temperature resistant primer, priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 25%, iron oxide red: 8%, titanium dioxide: 15%, silicon powder: 12%, multifunctional assistant AMP-95:18%, Graphite Powder 99: 15%, polyoxyethylene glycol: 8%, surplus is that organic fluorine is acrylic resin modified.
Aforesaid quick-drying rub resistance, high temperature resistant primer, priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 24%, iron oxide red: 7%, titanium dioxide: 13%, silicon powder: 11%, multifunctional assistant AMP-95:17%, Graphite Powder 99: 13%, polyoxyethylene glycol: 5%, surplus is that organic fluorine is acrylic resin modified.
The preparation method of aforesaid quick-drying rub resistance, high temperature resistant primer, this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 60 DEG C, setting stirring velocity 900r/min, churning time 2h, then put into iron oxide red to continue to stir, churning time is 1h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 860r/min, churning time 1h, adds multifunctional assistant AMP-95 and continues to stir 40min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 750r/min, churning time 60min, and the temperature in control stirring tank is at 52 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2h, stirring velocity is 680r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
The preparation method of aforesaid quick-drying rub resistance, high temperature resistant primer, this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 62 DEG C, setting stirring velocity 920r/min, churning time 3h, then put into iron oxide red to continue to stir, churning time is 2h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 870r/min, churning time 2h, adds multifunctional assistant AMP-95 and continues to stir 50min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 800r/min, churning time 80min, and the temperature in control stirring tank is at 55 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 3h, stirring velocity is 700r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
The preparation method of aforesaid quick-drying rub resistance, high temperature resistant primer, this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 61 DEG C, setting stirring velocity 910r/min, churning time 2.5h, then put into iron oxide red to continue to stir, churning time is 1.5h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 865r/min, churning time 1.5h, adds multifunctional assistant AMP-95 and continues to stir 48min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 780r/min, churning time 70min, and the temperature in control stirring tank is at 53 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2.8h, stirring velocity is 690r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
The invention has the beneficial effects as follows: obtain a kind of quick-drying rub resistance, high temperature resistant primer, the crocking resistance that Graphite Powder 99 improves priming paint is added in priming paint, multifunctional assistant AMP-95, the glossiness of priming paint can not only be improved, the PH stability that priming paint is extremely excellent can also be given, reduce corrosion, contribute to manufacturing low smell priming paint and being conducive to reducing priming paint cost, adding of iron oxide red not only improves the corrosion-resistant of priming paint and rustless property, and gives priming paint good outward appearance; Silicon powder add the chemical resistance further increasing priming paint; Barium sulfate add as a kind of heat-resistant filler, base-material can be made to thicken, compact in paint film, the lesion size of paint film can be reduced when hot-work, improve the physical and mechanical properties of paint film, the features such as organic fluorine modified acrylic acid resin primer had both remained the good alkali resistance of acrylic acid resin primer, protects look gloss retention, film is plentiful, have again that organic fluorine coating is weather-proof, resistant, corrosion-resistant and self-cleaning advantage.
Embodiment
The present invention is described in further detail below:
Embodiment 1
A kind of quick-drying rub resistance, high temperature resistant primer that the present embodiment provides, it is characterized in that: this priming paint is by bisphenol F-type epoxy resin, iron oxide red, titanium dioxide, silicon powder, multifunctional assistant AMP-95, Graphite Powder 99, polyoxyethylene glycol and organic fluorine is acrylic resin modified forms, its weight percent composition is: bisphenol F-type epoxy resin: 23%, iron oxide red: 5%, titanium dioxide: 12%, silicon powder: 10%, multifunctional assistant AMP-95:15%, Graphite Powder 99: 12%, polyoxyethylene glycol: 3%, surplus is that organic fluorine is acrylic resin modified; The preparation method of this quick-drying rub resistance, high temperature resistant primer carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 60 DEG C, setting stirring velocity 900r/min, churning time 2h, then put into iron oxide red to continue to stir, churning time is 1h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 860r/min, churning time 1h, adds multifunctional assistant AMP-95 and continues to stir 40min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 750r/min, churning time 60min, and the temperature in control stirring tank is at 52 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2h, stirring velocity is 680r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
Embodiment 2
A kind of quick-drying rub resistance, high temperature resistant primer that the present embodiment provides, it is characterized in that: this priming paint is by bisphenol F-type epoxy resin, iron oxide red, titanium dioxide, silicon powder, multifunctional assistant AMP-95, Graphite Powder 99, polyoxyethylene glycol and organic fluorine is acrylic resin modified forms, its weight percent composition is: bisphenol F-type epoxy resin: 25%, iron oxide red: 8%, titanium dioxide: 15%, silicon powder: 12%, multifunctional assistant AMP-95:18%, Graphite Powder 99: 15%, polyoxyethylene glycol: 8%, surplus is that organic fluorine is acrylic resin modified; The preparation method of this quick-drying rub resistance, high temperature resistant primer carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 62 DEG C, setting stirring velocity 920r/min, churning time 3h, then put into iron oxide red to continue to stir, churning time is 2h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 870r/min, churning time 2h, adds multifunctional assistant AMP-95 and continues to stir 50min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 800r/min, churning time 80min, and the temperature in control stirring tank is at 55 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 3h, stirring velocity is 700r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
Embodiment 3
A kind of quick-drying rub resistance, high temperature resistant primer that the present embodiment provides, it is characterized in that: this priming paint is by bisphenol F-type epoxy resin, iron oxide red, titanium dioxide, silicon powder, multifunctional assistant AMP-95, Graphite Powder 99, polyoxyethylene glycol and organic fluorine is acrylic resin modified forms, its weight percent composition is: bisphenol F-type epoxy resin: 24%, iron oxide red: 7%, titanium dioxide: 13%, silicon powder: 11%, multifunctional assistant AMP-95:17%, Graphite Powder 99: 13%, polyoxyethylene glycol: 5%, surplus is that organic fluorine is acrylic resin modified; The preparation method of this quick-drying rub resistance, high temperature resistant primer carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 61 DEG C, setting stirring velocity 910r/min, churning time 2.5h, then put into iron oxide red to continue to stir, churning time is 1.5h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 865r/min, churning time 1.5h, adds multifunctional assistant AMP-95 and continues to stir 48min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 780r/min, churning time 70min, and the temperature in control stirring tank is at 53 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2.8h, stirring velocity is 690r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
Following table is embodiment 1-3 quick-drying rub resistance, high temperature resistant primer performance detection data
Above embodiment is only and technological thought of the present invention is described, can not limit protection scope of the present invention with this, and every technological thought proposed according to the present invention, any change that technical scheme basis is done, all falls within scope.
Claims (8)
1. a quick-drying rub resistance, high temperature resistant primer, it is characterized in that: this priming paint is by bisphenol F-type epoxy resin, iron oxide red, titanium dioxide, silicon powder, multifunctional assistant AMP-95, Graphite Powder 99, polyoxyethylene glycol and organic fluorine is acrylic resin modified forms, its weight percent composition is: bisphenol F-type epoxy resin: 23-25%, iron oxide red: 5-8%, titanium dioxide: 12-15%, silicon powder: 10-12%, multifunctional assistant AMP-95:15-18%, Graphite Powder 99: 12-15%, polyoxyethylene glycol: 3-8%, surplus is that organic fluorine is acrylic resin modified.
2. quick-drying rub resistance according to claim 1, high temperature resistant primer, it is characterized in that: described priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 23%, iron oxide red: 5%, titanium dioxide: 12%, silicon powder: 10%, multifunctional assistant AMP-95:15%, Graphite Powder 99: 12%, polyoxyethylene glycol: 3%, surplus is that organic fluorine is acrylic resin modified.
3. quick-drying rub resistance according to claim 1, high temperature resistant primer, it is characterized in that: described priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 25%, iron oxide red: 8%, titanium dioxide: 15%, silicon powder: 12%, multifunctional assistant AMP-95:18%, Graphite Powder 99: 15%, polyoxyethylene glycol: 8%, surplus is that organic fluorine is acrylic resin modified.
4. quick-drying rub resistance according to claim 1, high temperature resistant primer, it is characterized in that: described priming paint by weight percentage composition is: bisphenol F-type epoxy resin: 24%, iron oxide red: 7%, titanium dioxide: 13%, silicon powder: 11%, multifunctional assistant AMP-95:17%, Graphite Powder 99: 13%, polyoxyethylene glycol: 5%, surplus is that organic fluorine is acrylic resin modified.
5. a preparation method for quick-drying rub resistance, high temperature resistant primer, is characterized in that: this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank is at 60-62 DEG C, setting stirring velocity 900-920r/min, churning time 2-3h, then put into iron oxide red to continue to stir, churning time is 1-2h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 860-870r/min, churning time 1-2h, adds multifunctional assistant AMP-95 and continues to stir 40-50min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 750-800r/min, churning time 60-80min, and the temperature in control stirring tank is at 52-55 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2-3h, stirring velocity is 680-700r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
6. the preparation method of quick-drying rub resistance according to claim 5, high temperature resistant primer, is characterized in that: this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank, at 60 DEG C, sets stirring velocity 900r/min, churning time 2h, then put into iron oxide red to continue to stir, churning time is 1h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 860r/min, churning time 1h, adds multifunctional assistant AMP-95 and continues to stir 40min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 750r/min, churning time 60min, and the temperature in control stirring tank is at 52 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2h, stirring velocity is 680r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
7. the preparation method of quick-drying rub resistance according to claim 5, high temperature resistant primer, is characterized in that: this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank, at 62 DEG C, sets stirring velocity 920r/min, churning time 3h, then put into iron oxide red to continue to stir, churning time is 2h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 870r/min, churning time 2h, adds multifunctional assistant AMP-95 and continues to stir 50min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 800r/min, churning time 80min, and the temperature in control stirring tank is at 55 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 3h, stirring velocity is 700r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
8. the preparation method of quick-drying rub resistance according to claim 5, high temperature resistant primer, is characterized in that: this preparation method carries out according to the following steps:
Step (1): first acrylic resin modified to bisphenol F-type epoxy resin and organic fluorine stirring tank of first putting into is mixed, temperature in control stirring tank, at 61 DEG C, sets stirring velocity 910r/min, churning time 2.5h, then put into iron oxide red to continue to stir, churning time is 1.5h;
Step (2): add titanium dioxide and silicon powder, setting stirring velocity is 865r/min, churning time 1.5h, adds multifunctional assistant AMP-95 and continues to stir 48min;
Step (3): then Graphite Powder 99 is added in stirring tank and stir, stirring velocity is 780r/min, churning time 70min, and the temperature in control stirring tank is at 53 DEG C;
Step (4): finally add polyoxyethylene glycol and stir 2.8h, stirring velocity is 690r/min, can obtain described quick-drying rub resistance, high temperature resistant primer.
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| CN104893458A (en) * | 2015-05-11 | 2015-09-09 | 广德县新杭镇聚源新型材料压膜厂 | Deodorization closestool cover coating with high adhesive force |
| CN105176269A (en) * | 2015-10-21 | 2015-12-23 | 苏州赛斯德工程设备有限公司 | Corrosion-resistant water-borne coating and preparation method thereof |
| CN106590101A (en) * | 2016-12-14 | 2017-04-26 | 苏州纽东精密制造科技有限公司 | High-temperature-resistant paint used for automobile chassis |
| CN106700830A (en) * | 2016-12-14 | 2017-05-24 | 苏州纽东精密制造科技有限公司 | Anti-corrosive primer for automobile chassis |
| CN106752800A (en) * | 2016-12-14 | 2017-05-31 | 苏州纽东精密制造科技有限公司 | A kind of car surface high-temperature resistant coating |
| CN106752614A (en) * | 2016-12-14 | 2017-05-31 | 苏州纽东精密制造科技有限公司 | A kind of automobile plastic anticorrosive paint and preparation method thereof |
| CN110819176A (en) * | 2019-11-18 | 2020-02-21 | 榆林学院 | Preparation method of anticorrosive and antiscale coating |
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| CN106590101A (en) * | 2016-12-14 | 2017-04-26 | 苏州纽东精密制造科技有限公司 | High-temperature-resistant paint used for automobile chassis |
| CN106700830A (en) * | 2016-12-14 | 2017-05-24 | 苏州纽东精密制造科技有限公司 | Anti-corrosive primer for automobile chassis |
| CN106752800A (en) * | 2016-12-14 | 2017-05-31 | 苏州纽东精密制造科技有限公司 | A kind of car surface high-temperature resistant coating |
| CN106752614A (en) * | 2016-12-14 | 2017-05-31 | 苏州纽东精密制造科技有限公司 | A kind of automobile plastic anticorrosive paint and preparation method thereof |
| CN110819176A (en) * | 2019-11-18 | 2020-02-21 | 榆林学院 | Preparation method of anticorrosive and antiscale coating |
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