CN104208977B - Organic working medium purifying and recycling system - Google Patents
Organic working medium purifying and recycling system Download PDFInfo
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- CN104208977B CN104208977B CN201410041068.4A CN201410041068A CN104208977B CN 104208977 B CN104208977 B CN 104208977B CN 201410041068 A CN201410041068 A CN 201410041068A CN 104208977 B CN104208977 B CN 104208977B
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Abstract
The invention provides a purification and recovery system of organic working medium, which comprises: the organic working medium utilization system is internally provided with an organic working medium for low-temperature waste heat power generation; the inlet of the vacuum pump is connected with the organic working medium utilization system through a pipeline; the inside of the packed tower is provided with a plurality of ceramic rings, a first tower opening of the packed tower, which is positioned at the bottom, is connected with an outlet of the vacuum pump through a pipeline, and a second tower opening of the packed tower, which is positioned at the bottom, is connected with the organic working medium utilization system through a pipeline; the inlet of the condenser is connected with a third tower opening positioned at the top of the packed tower through a pipeline, the pipeline connected with the outlet of the condenser is branched into a first pipeline and a second pipeline, the first pipeline is connected with a fourth tower opening positioned at the top of the packed tower through a first valve, and the condenser is connected with a vent pipe and a temperature detection device; and the first bottle mouth is connected with a second pipeline of the condenser through a second valve, and the second bottle mouth is connected with a pipeline connecting the organic working medium utilization system and the inlet of the vacuum pump through a balance gas pipe.
Description
Technical field
The present invention relates to a kind of purification-recovery system, particularly relate to a kind of purification-recovery system of organic working medium.
Background technology
The energy is the important substance basis that the mankind depend on for existence and development, and the height of energy use efficiency has become important development target, and in the current time, energy shortage is on the rise, and power saving is particularly outstanding.
Under these circumstances, how to utilize in production process and produce discarded energy and become important issue, such as in the prior art, waste heat not only for high temperature can make full use of, and can recycle 150 ° that produce in the industrial processes such as cement, iron and steel to 350 ° even low temperature exhaust heat of tens degree.Usually the low temperature exhaust heat recovery system utilizing organic working medium is used when reclaiming low temperature exhaust heat, it take low-boiling-point organic compound as working medium such as halogenated hydrocarbons (fluorohydrocarbon) etc., waste gas residual heat is reclaimed by evaporimeter, produce the organic working medium steam of certain temperature and pressure, promote decompressor, drive electrical generators generating or outputting power, then weary gas condensation within the condenser, export evaporimeter to by working medium pump, complete a circulation.
In the low temperature exhaust heat recovery system utilizing organic working medium, when needs parking maintenance, a large amount of working medium will be abandoned, expensive due to organic working medium, the working medium of abandoning causes very large waste, which enhance the cost of low temperature exhaust heat recovery system recovery waste heat, thus need device that the organic working medium in low temperature exhaust heat recovery system is reclaimed.And there is impurity in the organic working medium in low temperature exhaust heat recovery system, working medium of how purifying also becomes a kind of problem.But in the prior art, the equipment reclaiming organic working medium of can purifying like this need exploitation.
Summary of the invention
The object of the invention is to propose for the technological deficiency existed in prior art a kind ofly can purify and reclaim the purification-recovery system of organic working medium.
Following technical scheme is adopted for realizing object of the present invention.
The purification-recovery system of a kind of organic working medium of the present invention, has: organic working medium utilizes system, its inner remaining organic working medium had for low-temperature cogeneration; Vavuum pump, its entrance utilizes system to be connected via pipeline with described organic working medium; Packed tower, its inside has multiple porcelain ring, and the first tower mouth being positioned at bottom of described packed tower is connected with described vacuum delivery side of pump via pipeline, and the second tower mouth being positioned at bottom of described packed tower utilizes system to be connected via pipeline with described organic working medium; Condenser, its entrance is connected with the 3rd tower mouth being positioned at top of described packed tower via pipeline, the pipeline be connected with the outlet of described condenser is branched to the first pipeline and second pipe, described first pipeline is connected with the 4th tower mouth being positioned at top of described packed tower via the first valve, and is connected with blow-down pipe and temperature-detecting device on described condenser; Reclaim steel cylinder, its first bottleneck is connected via the second pipe of the second valve with described condenser, and its second bottleneck connects with the pipeline utilizing the entrance of system and described vavuum pump to be connected described organic working medium via balance tracheae.
In the purification-recovery system of above-mentioned organic working medium, open vavuum pump, organic working medium utilizes the organic working medium with impurity in system and low temperature exhaust heat recovery system due to the suction of vavuum pump, enter to the first tower mouth being positioned at bottom of packed tower via vavuum pump, then rise in packed columns from the first tower mouth and enter condenser.Owing to there is blow-down pipe on condenser, so the initial stage of reclaiming in organic working medium, initial stage low boiling impurity can be discharged.In addition, condenser has temperature-detecting device and thermometer, like this can monitoring temperature, the evaporating temperature due to organic working medium is specified temp, so can determine whether that the steam of organic working medium enters condenser by monitoring temperature.In addition, branch into the first pipeline and second pipe with the outlet connecting pipe road of condenser, the first pipeline is connected with the tower mouth being positioned at top of packed tower, and second pipe is connected with recovery steel cylinder.Passing through temperature-detecting device, when judging that the steam of organic working medium enters condenser, open the valve being positioned at the first pipeline and the valve being positioned at second pipe respectively, the condensed organic working medium of small part is made to enter packed tower in addition, the organic working medium entering packed tower sprays on the porcelain ring installed in organic working medium, soaks porcelain ring.Organic working medium utilizes the institute of the organic working medium in system to comprise high boiling impurity such as gaseous state oil and lower boiling impurity such as air etc. with impurity, at such mist through packed tower, fully contact with for increasing surface area contacted porcelain ring, wherein lower boiling impurity can be discharged from the evacuated tube condenser in advance, organic working medium can be condensed through packed tower device condensation and be recycled to recovery steel cylinder, and high boiling impurity can liquefy because contacting with the organic working medium on porcelain ring flow back to organic working medium space via the second tower mouth be connected with the bottom of packed tower together with organic working medium, and then again entered recovery system by evaporating, carry out iterative cycles like this, carry out Recovery Purifying organic working medium.
According to the purification-recovery system of organic working medium of the present invention, organic working medium containing impurity is recovered to via packed tower and condenser and reclaims in steel cylinder, wherein lower boiling impurity is directly disposed to outside via the blow-down pipe be arranged on condenser, and the organic working medium device that is condensed is cooled to liquid state and is back to recovery steel cylinder.In addition, the organic working medium of the liquid state be recovered also sprays on the porcelain ring in packed tower via pipeline, high boiling like this impurity is back to organic working medium by the organic working medium liquefaction on porcelain ring and utilizes system together with organic working medium, and then the purification-recovery system by evaporating in organic working medium circulating, organic working medium can be purified like this and reclaim.
In the purification-recovery system of above-mentioned organic working medium, preferably utilize in described organic working medium between the entrance of system and described vavuum pump and be connected with pressure vacuum gauge, the pipeline of the arrival end of described vavuum pump is connected with the first tower mouth of described packed tower via the 3rd valve.
Thus, can judge that organic working medium utilizes the pressure in system according to Pressure gauge, under organic working medium utilizes the pressure in system to be greater than atmospheric situation, need not need to open vavuum pump, utilize the pressure in system just can discharge the organic working medium of band impurity by organic working medium, reclaim, be judged as being reduced to atmospheric pressure by Pressure gauge, organic working medium with impurity can not the situation of Self-discharged, opening vavuum pump extraction organic working medium utilizes the organic working medium of the band impurity of system to carry out purifying and reclaiming, certainly Pressure gauge can not be set in addition, organic working medium is utilized to utilize existing pressure-detecting device in system to detect.In addition, the pipeline of the arrival end of vavuum pump is directly connected with the first tower mouth of described packed tower via the 3rd valve, like this can under organic working medium utilize the pressure in system to be greater than atmospheric situation, open the 3rd valve and make organic working medium directly enter packed tower then to reclaim.
In the purification-recovery system of above-mentioned organic working medium, first pipeline of preferred described condenser is also connected with the 3rd tower mouth of described packed tower via backflow visor, and the second pipe of described condenser is also connected with the first bottleneck reclaiming steel cylinder via organic working medium visor.Thus, can by backflow visor and organic working medium visor, observe the flow of ducted working medium, can suitably regulate each valve like this, the flow direction of the organic working medium of adjustment in the first pipeline and second pipe, make the organic working medium of small part spray the purification operation after carrying out to packed tower, most of organic working medium is recovered.
In the purification-recovery system of above-mentioned organic working medium, the described organic working medium of preferred connection utilizes system to be also connected with described balance tracheae via the 4th valve with the pipeline of the second tower mouth of described packed tower, and described organic working medium utilizes system to be also connected with the 5th tower mouth being positioned at top of described packed tower via the 5th valve.When only discharging the liquid impurities that organic working medium utilizes in system like this when not reclaiming organic working medium and utilizing the organic working medium in system, can isolated vacuum pump, organic working medium is made to utilize system to be directly connected with recovery steel cylinder, forming organic working medium utilizes system, recovery steel cylinder, packed tower to organic working medium to utilize the path of system, and liquid impurities is directly disposed to steel cylinder.
In the purification-recovery system of above-mentioned organic working medium, be preferably connected with the 6th valve in the downstream of described organic working medium visor, be connected with the 7th valve at the first bottleneck of described recovery steel cylinder.Like this in recovery ending phase, can reclaim remain in ducted organic working medium by closing the 6th valve open the 7th valve.
In the purification-recovery system of above-mentioned organic working medium, preferably on described recovery steel cylinder, connect electronic scale.Whether recovery flow and the organic working medium that can be measured the organic working medium reclaiming steel cylinder like this by electronic scale are filled.
In the purification-recovery system of above-mentioned organic working medium, the second pipe of preferred described condenser can be connected with multiple described recovery steel cylinder, and the second bottleneck of multiple described recovery steel cylinder connects with the pipeline utilizing the entrance of system and described vavuum pump to be connected described organic working medium via balance tracheae respectively.Can organic working medium be recycled in multiple recovery steel cylinder so simultaneously.
In the purification-recovery system of above-mentioned organic working medium, preferred described vavuum pump is oilless vacuum pump.Can avoid further like this in organic working medium, being mixed into impurity in the purification-recovery system of organic working medium.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of the purification-recovery system representing organic working medium of the present invention.
Detailed description of the invention
Below, the purification-recovery system of the organic working medium as embodiments of the invention is described based on accompanying drawing.
Fig. 1 is the schematic diagram of the purification-recovery system representing organic working medium of the present invention.
As shown in Figure 1, the purification-recovery system of organic working medium of the present invention has: organic working medium utilizes system 10, its inner remaining organic working medium had for low-temperature cogeneration; Vavuum pump 20, its entrance 21 utilizes system 10 to be connected via pipeline and organic working medium; Packed tower 30, its inside has multiple porcelain ring, and the first tower mouth 31 being positioned at bottom of packed tower 30 is connected with vacuum delivery side of pump 22 via pipeline, and the second tower mouth 32 being positioned at bottom of packed tower 30 utilizes system 10 to be connected via pipeline and organic working medium; Condenser 40, its entrance 41 is connected with the 3rd tower mouth 33 being positioned at top of packed tower 30 via pipeline, the pipeline be connected with the outlet 42 of condenser 40 is branched to the first pipeline 43 and second pipe 44, first pipeline 43 is connected with the 4th tower mouth 34 being positioned at top of packed tower 30 via the first valve 45, and on condenser 40, be connected with blow-down pipe 50 and temperature-detecting device TI; Reclaim steel cylinder 70, its first bottleneck 71 is connected with the second pipe 44 of condenser 40 via the second valve 46, and its second bottleneck 72 connects with pipeline organic working medium being utilized the entrance of system 10 and vavuum pump 20 to be connected via balance tracheae 80.
Specifically, branch into vavuum pump connecting pipe with the valve downstream end of the pipeline utilizing the outlet of system 10 to be connected via valve and organic working medium and reclaim steel cylinder connecting pipe, vavuum pump connecting pipe is connected with the entrance 21 of vavuum pump 20 via valve, namely recovery steel cylinder connecting pipe balances tracheae 80 and is connected with recovery steel cylinder 70 via multiple valve, and the port of export of balance tracheae 80 stretches to the top of the recovery steel cylinder 20 of horizontal positioned.The outlet 22 of vavuum pump 20 is connected via the first tower mouth 31 of valve with the bottom of packed tower 30.In addition, the second tower mouth 32 of the bottom of packed tower 30 utilizes the middle and lower part of system to be connected via valve and organic working medium.In addition, be provided with multiple porcelain ring in packed tower 30, the 3rd tower mouth 33 at the top of packed tower 30 is connected via the entrance of pipeline with condenser 40.Condenser 40 is connected with blow-down pipe 50 and the thermometer TI as temperature-detecting device, the pipe branch be connected with the outlet 42 of condenser 40 is the first pipeline 43 and second pipe 44, first pipeline 43 is connected via the 4th tower mouth 34 of valve with the top of packed tower 30, second pipe 44 is connected with recovery steel cylinder 70 via valve, form reclaim line, the port of export of reclaim line stretches to the bottom of the recovery steel cylinder 20 of horizontal positioned.
In the purification-recovery system of above-mentioned organic working medium, open vavuum pump, organic working medium utilizes the organic working medium with impurity in system and low temperature exhaust heat recovery system due to the suction of vavuum pump, enter to the first tower mouth being positioned at bottom of packed tower via vavuum pump, then rise in packed columns from the first tower mouth and enter condenser.Owing to there is blow-down pipe on condenser, so the initial stage of reclaiming in organic working medium, the low boilers at initial stage can be discharged.In addition, condenser has temperature-detecting device such as thermometer, temperature sensor etc., like this can monitoring temperature, the evaporating temperature due to organic working medium is specified temp, so can determine whether that the steam of organic working medium enters condenser by monitoring temperature.In addition, branch into the first pipeline and second pipe with the outlet connecting pipe road of condenser, the first pipeline is connected with the tower mouth being positioned at top of packed tower, and second pipe is connected with recovery steel cylinder.Passing through temperature-detecting device, when judging that the steam of organic working medium enters condenser, open the valve being positioned at the first pipeline and the valve being positioned at second pipe respectively, the condensed organic working medium of small part is made to enter packed tower in addition, the organic working medium entering packed tower sprays on the porcelain ring installed in organic working medium, soaks porcelain ring.Organic working medium utilizes the institute of the organic working medium in system to comprise high boiling impurity such as gaseous state oil and lower boiling impurity such as air etc. with impurity, at such mist through packed tower, fully contact with for increasing surface area contacted porcelain ring, wherein lower boiling impurity can be discharged from the evacuated tube condenser in advance, organic working medium can be condensed through packed tower device condensation and be recycled to recovery steel cylinder, and high boiling impurity can liquefy because contacting with the organic working medium on porcelain ring and to fail to be convened for lack of a quorum machine working medium space via the second tower mouth be connected with the bottom of packed tower together with organic working medium, and then again entered recovery system by evaporating, carry out iterative cycles like this, carry out Recovery Purifying organic working medium.
According to the purification-recovery system of organic working medium of the present invention, organic working medium containing impurity is recovered to via packed tower and condenser and reclaims in steel cylinder, wherein lower boiling impurity is directly disposed to outside via the blow-down pipe be arranged on condenser, and the organic working medium device that is condensed is cooled to liquid state and is back to recovery steel cylinder.In addition, the organic working medium of the liquid state be recovered also sprays on the porcelain ring in packed tower via pipeline, high boiling like this impurity is back to organic working medium by the organic working medium liquefaction on porcelain ring and utilizes system together with organic working medium, and then the purification-recovery system by evaporating in organic working medium circulating, organic working medium can be purified like this and reclaim.
In addition, can be connected with pressure vacuum gauge PI between the entrance that organic working medium utilizes system 10 and vavuum pump 20, the pipeline of the arrival end of vavuum pump 20 is connected with the first tower mouth 31 of packed tower 30 via the 3rd valve 11.Specifically, branch out packed tower connecting pipe from the vavuum pump connecting pipe be connected with the entrance of vavuum pump 20, this packed tower connecting pipe is connected with the first tower mouth of packed tower via valve.
Thus, can judge that organic working medium utilizes the pressure in system according to Pressure gauge, under organic working medium utilizes the pressure in system to be greater than atmospheric situation, need not need to open vavuum pump, the organic working medium utilizing the pressure in system just can discharge band impurity by organic working medium reclaims, judging to be reduced to atmospheric pressure by Pressure gauge, organic working medium with impurity can not the situation of Self-discharged, opening vavuum pump extraction organic working medium utilizes the organic working medium of the band impurity of system to carry out purifying and reclaiming, certainly Pressure gauge can not be set in addition, organic working medium is utilized to utilize existing pressure-detecting device in system to detect.In addition, the pipeline of the arrival end of vavuum pump is directly connected with the first tower mouth of described packed tower via the 3rd valve, like this can under organic working medium utilize the pressure in system to be greater than atmospheric situation, open the 3rd valve and make organic working medium directly enter packed tower then to reclaim.
In addition, the first pipeline 43 of condenser 40 is also connected with the 3rd tower mouth 33 of packed tower 30 via backflow visor 47, and the second pipe 44 of condenser 40 is also connected with the first bottleneck 71 reclaiming steel cylinder 70 via organic working medium visor 48.
Thus, can by backflow visor and organic working medium visor, observe the flow of ducted working medium, can suitably regulate each valve like this, the flow direction of the organic working medium of adjustment in the first pipeline and second pipe, make the organic working medium of small part spray the purification operation after carrying out to packed tower, most of organic working medium is recovered.
In addition, connect organic working medium and utilize system 10 to be also connected with balance tracheae via the 4th valve 12 with the pipeline of the second tower mouth 32 of packed tower 30, organic working medium utilizes system 10 to be also connected with the 5th tower mouth 35 being positioned at top of packed tower 30 via the 5th valve 13.When only discharging the liquid impurities that organic working medium utilizes in system like this when not reclaiming organic working medium and utilizing the organic working medium in system, can isolated vacuum pump, organic working medium is made to utilize system to be directly connected with recovery steel cylinder, forming organic working medium utilizes system, recovery steel cylinder, packed tower to organic working medium to utilize the path of system, and liquid impurities is directly disposed to steel cylinder.
In addition, be connected with the 6th valve 73 in the downstream of organic working medium visor 47, be connected with the 7th valve 74 at the first bottleneck 71 reclaiming steel cylinder 70.Like this in recovery ending phase, can reclaim remain in ducted organic working medium by closing the 6th valve open the 7th valve.
In addition, recovery steel cylinder 70 connects electronic scale 90.Whether recovery flow and the organic working medium that can be measured the organic working medium reclaiming steel cylinder like this by electronic scale are filled.
In addition, the second pipe of condenser can be connected with multiple recovery steel cylinder, and the second bottleneck of multiple recovery steel cylinder connects with pipeline organic working medium being utilized the entrance of system and vavuum pump to be connected via balance tracheae respectively.Can organic working medium be recycled in multiple recovery steel cylinder so simultaneously.
In addition, vavuum pump can use oilless vacuum pump, can avoid further like this in organic working medium, being mixed into impurity in the purification-recovery system of organic working medium.
In addition, multiple valve can be connected on balance tracheae.And the valve that can connect in the bottom of organic working medium accommodation space for discharging raffinate.
Above the purification-recovery system of the organic working medium of the preferred embodiment of the present invention is illustrated, but the present invention is not limited to above-mentioned concrete embodiment, only otherwise depart from the scope of claim, can various distortion or change be carried out.Present invention resides in the various distortion in the scope of claim and change.
Claims (8)
1. a purification-recovery system for organic working medium, is characterized in that, has:
Organic working medium utilizes system, its inner remaining organic working medium had for low-temperature cogeneration;
Vavuum pump, its entrance utilizes system to be connected via pipeline with described organic working medium;
Packed tower, its inside has multiple porcelain ring, and the first tower mouth being positioned at bottom of described packed tower is connected with described vacuum delivery side of pump via pipeline, and the second tower mouth being positioned at bottom of described packed tower utilizes system to be connected via pipeline with described organic working medium;
Condenser, its entrance is connected with the 3rd tower mouth being positioned at top of described packed tower via pipeline, the pipeline be connected with the outlet of described condenser is branched to the first pipeline and second pipe, described first pipeline is connected with the 4th tower mouth being positioned at top of described packed tower via the first valve, and is connected with blow-down pipe and temperature-detecting device on described condenser;
Reclaim steel cylinder, its first bottleneck is connected via the second pipe of the second valve with described condenser, and its second bottleneck connects with the pipeline utilizing the entrance of system and described vavuum pump to be connected described organic working medium via balance tracheae.
2. the purification-recovery system of organic working medium according to claim 1, is characterized in that,
Utilize in described organic working medium between the entrance of system and described vavuum pump and be connected with pressure vacuum gauge, the pipeline of the arrival end of described vavuum pump is connected with the first tower mouth of described packed tower via the 3rd valve.
3. the purification-recovery system of organic working medium according to claim 2, is characterized in that,
First pipeline of described condenser is also connected with the 3rd tower mouth of described packed tower via backflow visor, and the second pipe of described condenser is also connected with the first bottleneck reclaiming steel cylinder via organic working medium visor.
4. the purification-recovery system of organic working medium according to claim 3, it is characterized in that, connecting described organic working medium utilizes system to be also connected with described balance tracheae via the 4th valve with the pipeline of the second tower mouth of described packed tower, and described organic working medium utilizes system to be also connected with the 5th tower mouth being positioned at top of described packed tower via the 5th valve.
5. the purification-recovery system of organic working medium according to claim 3, is characterized in that, is connected with the 6th valve in the downstream of described organic working medium visor, is connected with the 7th valve at the first bottleneck of described recovery steel cylinder.
6. the purification-recovery system of organic working medium according to any one of claim 1 to 3, is characterized in that, described recovery steel cylinder connects electronic scale.
7. the purification-recovery system of organic working medium according to any one of claim 1 to 3, it is characterized in that, the second pipe of described condenser can be connected with multiple described recovery steel cylinder, and the second bottleneck of multiple described recovery steel cylinder connects with the pipeline utilizing the entrance of system and described vavuum pump to be connected described organic working medium via balance tracheae respectively.
8. the purification-recovery system of organic working medium according to any one of claim 1 to 3, is characterized in that, described vavuum pump is oilless vacuum pump.
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| CN201410041068.4A CN104208977B (en) | 2014-01-28 | 2014-01-28 | Organic working medium purifying and recycling system |
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| CN201410041068.4A CN104208977B (en) | 2014-01-28 | 2014-01-28 | Organic working medium purifying and recycling system |
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Effective date of registration: 20220427 Address after: No. 113 podium building, 1st floor, No. 69, Zizhuyuan Road, Haidian District, Beijing 100089 Patentee after: Beijing Huasheng Zhiqing new energy Co.,Ltd. Address before: No. 9, North Fourth Ring West Road, Haidian District, Beijing 100088 2014 Patentee before: BEIJING HUASHENG HUANNENG SCIENCE & TECHNOLOGY CO.,LTD. |