CN104194358B - A kind of warm mix regeneration asphalt and preparation method thereof - Google Patents
A kind of warm mix regeneration asphalt and preparation method thereof Download PDFInfo
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- CN104194358B CN104194358B CN201410425370.XA CN201410425370A CN104194358B CN 104194358 B CN104194358 B CN 104194358B CN 201410425370 A CN201410425370 A CN 201410425370A CN 104194358 B CN104194358 B CN 104194358B
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Abstract
The invention discloses a kind of warm mix regeneration asphalt, mixed and stirred and formed with compound warm mix regenerative agent by pitch, be combined the composite that warm mix regenerative agent is surfactant and oil regenerative agent.The warm mix regeneration asphalt of the present invention functional effect is good, pollution-free, cost is low, compound warm mix regenerative agent therein combines warm-mixing agent with regenerative agent, gives full play to its mass action.The invention also discloses a kind of preparation method of warm mix regeneration asphalt, its step is to be heated to pitch to mix and stir temperature；Compound warm mix regenerative agent is added in the pitch for having been heated to and mix and stir temperature and mixed and stirred.The preparation method of the warm mix regeneration asphalt of the present invention is simple, compound warm mix regenerative agent directly, is disposably added to uniform mixing in pitch, mixing and stirring temperature significantly reduces, and this not only reduces the discharge of pernicious gas, reduces cost, and it has good pavement performance.
Description
Technical field
The invention belongs to technical field of road engineering materials, it is related to the warm mix technology and regeneration techniques of pavement asphalt, specifically
It is related to a kind of warm mix regeneration asphalt and preparation method thereof.
Background technology
In recent years, the warm mix technology and regeneration techniques of pitch and asphalt as asphalt pavement construction new technology,
Increasingly it is taken seriously.
The regeneration techniques of bituminous paving, after being the pretreating process by old asphalt pavement by milling, recovery, screening, is adopted
Asphalt is mixed and stirred into again by a certain percentage with corresponding regeneration techniques and new pitch ground surface material, enables satisfaction one
Fixed pavement performance and with the technology of its surfacing again.Traditional Applied of Asphalt Pavement Recycle Technique is mainly hot recycling drip
Blue or green compound technology, heat regeneration asphalt mixture technology is that bitumen regenerant is added into old asphalt mixture and 150 are heated to
Carry out mixing and stirring regeneration with new pitch and mineral aggregate at a high temperature of DEG C -180 DEG C.Hot in-place recycling can recover the usability of aged asphalt
Can, but the secondary aging of old asphalt mixture is serious in regenerative process, causes that the pavement performance of asphalt is poor, and regeneration is mixed
It is low (within 20%) with rate.And cold recycled asphalt mixture pavement performance is poor, it is impossible to used in High Grade Bitumen Pavement.
Warm-mixed asphalt pavement technique is by adding warm-mixing agent in pitch, reducing the high-temperature viscosity of pitch to realize drip
Blue or green compound can be mixed and stirred at less than 150 DEG C, and its pavement performance is not less than the pavement performance of hot-mix asphalt mixture.
At present, the warm mix of pitch and asphalt and regeneration comprehensive application technology, i.e. warm mix regeneration asphalt and warm mix be again
Raw asphalt technology receives much concern, in order to effectively organically be combined asphalt pavement warm mixing technology with regeneration techniques
Get up, be badly in need of a kind of new compound warm mix regenerative agent of exploitation, for solving pitch and asphalt mixture warm-mixing technology and regeneration
The compatibility and the compatibility issues of material of technology, this is by as realizing that what pavement material energy-conserving and environment-protective and reclamation of old material utilized open
Invasive technology.
Publication No. discloses a kind of warm-mixed recycled asphalt mixture for CN102320765A patent of invention, and its composition is sulphur
Sulphur and bituminous cements.The warm-mixed recycled asphalt mixture of the invention is used as additive using sulphur, although price is relatively low, still
Mix and stir temperature still higher, secondary aging can be caused serious, regeneration ratio is relatively low, and pavement performance is affected.
The content of the invention
To solve problems of the prior art, the present invention provides a kind of warm mix regeneration asphalt, by pitch and compound temperature
Mix regenerative agent and mix and stir and form.The pitch is new pitch.Compound warm mix regenerative agent can directly, be disposably added to pitch
In, the warm mix of pitch and the regeneration of Bituminous concrete surface are realized, and then realize that the solid waste of ground surface material utilizes double with energy-saving and emission-reduction
Weight effect.
Bituminous cements includes new pitch and aged asphalt.The content of aged asphalt is the 10-40% of bituminous cements.
In any of the above-described scheme preferably, the compound warm mix regenerative agent is the composite wood of warm-mixing agent and regenerative agent
Material.During bituminous paving carries out warm mix with regeneration, asphalt road is caused due to warm mix technology and regeneration techniques phase separation
Face can not realize warm mix and the technical barrier of regeneration simultaneously, and the present invention adds one kind into pitch and can realize Bituminous concrete surface again simultaneously
The raw compound warm mix regenerative agent with pitch warm mix function, the compound warm mix regenerative agent is a kind of composite, can directly, once
It is added in pitch to property, realizes the warm mix of pitch and the regeneration of old asphalt mixture.
The compound warm mix regenerative agent organically combines warm-mixing agent with regenerative agent, can realize that pitch and pitch are mixed
Close material and mix and stir the reduction of temperature and the regeneration of old asphalt mixture.Warm-mixing agent in the compound warm mix regenerative agent can reduce drip
Blue or green high-temperature viscosity, so as to realize that pitch and asphalt can be mixed and stirred at 100-140 DEG C, and then reduces pitch and pitch
Short ageing of the compound in work progress, improves the mixing and stirring of asphalt, consolidation effect, at the same realize energy-saving and emission-reduction and
Extend the service life of road.Regenerative agent in the compound warm mix regenerative agent can realize the regeneration of old asphalt mixture, its
Volume can reach 50%, and the utilization rate of old material is significantly improved, and then realize solid waste recycling and reduce green wood
The exploitation of material, preserves the ecological environment.
At present, generally use and be respectively added to warm-mixing agent and regenerative agent to use in pitch, the two is played respectively respectively
From effect, and the present invention combines warm-mixing agent and regenerative agent, forms a kind of composite, that is, is combined warm mix and regenerates
Agent, when in use, compound warm mix regenerative agent directly, is disposably come into operation, and plays mass action, better.
Compound warm mix regenerative agent is sticky state, atrament at normal temperatures.Compound warm mix regenerative agent need to be positioned over sealing
Aluminium vessel in preserve, be suitable for preserving for a long time at a temperature of 15-40 DEG C, be not suitable at too high or too low temperature protect
Deposit, otherwise can reduce the performance of compound warm mix regenerative agent, influence the performance of its warm mix and regeneration effect.
In any of the above-described scheme preferably, the warm-mixing agent is surfactant.Surfactant is at normal temperatures
Liquid, transparent, yellow substance.Surfactant is as the material that pitch warm mix is realized in compound warm mix regenerative agent, and it is in normal temperature
There is down good mobility.
In any of the above-described scheme preferably, the surfactant is fatty glyceride, fatty acid sorbitan, gathered
One or several kinds in sorb ester, sucrose ester.The chemical stability of such surfactant is more preferable, high temperature resistant and barotolerance
More preferably pitch warm mix can be adapted to and used.
In any of the above-described scheme preferably, the regenerative agent is oil regenerative agent.Oil regenerative agent is at normal temperatures
Viscous liquid state, dark yellow color substance.Oil regenerative agent is used as the material that Bituminous concrete surface regeneration is realized in compound warm mix regenerative agent.
In any of the above-described scheme preferably, the oil regenerative agent be bright stock when tapped oil, lubricating oil,
One or several kinds in machine oil, heavy oil.The oil regenerative agent that the present invention is used it is cheap, be readily available, it might even be possible to
Using the waste material of various oil plants, turn waste into wealth, greatly save cost.
The functional effect of the warm mix regeneration asphalt of the present invention is good, pollute that small, cost is low, and compound warm mix regenerative agent therein will
Warm-mixing agent combines with regenerative agent, forms composite, directly, disposably can be added in new pitch, fully
The mass action of compound warm mix regenerative agent is played, the warm mix regeneration asphalt thus prepared has good performance.
The present invention also provides a kind of preparation method of above-mentioned warm mix regeneration asphalt, comprises the following steps：
(1) pitch is heated to mixing and stirring temperature；
(2) compound warm mix regenerative agent is added in the pitch for having been heated to and mix and stir temperature and mixed and stirred；
The compound warm mix regenerative agent is the composite of warm-mixing agent and regenerative agent.The pitch is new pitch.
Preferably, the temperature of mixing and stirring is 100-140 DEG C.
In any of the above-described scheme preferably, the temperature of mixing and stirring is 110-130 DEG C.
In any of the above-described scheme preferably, the temperature of mixing and stirring is 120 DEG C.
Traditional heated tool butt-welding pitch, is to be mixed and stirred at a high temperature of 150-180 DEG C pitch with regenerative agent, temperature meeting
Cause secondary aging, regeneration ratio is relatively low, and the pavement performance of pitch can be also severely impacted, in addition, pitch is heated to so
High temperature, will consume substantial amounts of fuel oil, side by side the pernicious gas of amplification quantity, can cause serious environmental pollution.The present invention's
The preparation method of warm mix regeneration asphalt, can will mix and stir temperature and be reduced to 100-140 DEG C, this not only reduces the row of pernicious gas
Put, reduce cost, and prepared warm mix regeneration asphalt has good performance, and it is not less than the performance of hot asphalt.
In any of the above-described scheme preferably, the mixing time of compound the warm mix regenerative agent and pitch is 120-
180s.The present invention is by experimental results demonstrate in the range of this mixing time, being combined warm mix regenerative agent can be abundant with new pitch
Fusion is uniform.
In any of the above-described scheme preferably, the mixing time of compound the warm mix regenerative agent and pitch is 150s.
In any of the above-described scheme preferably, the preparation method of the compound warm mix regenerative agent comprises the following steps：
(1) surfactant is weighed according to a certain percentage with oil regenerative agent；
(2) surfactant and oil regenerative agent are fitted into mixing apparatus and mixed and stirred.
In any of the above-described scheme preferably, formed after the surfactant is mixed and stirred with the oil regenerative agent compound
Material, the composite is compound warm mix regenerative agent.
The synthesis ratio of surfactant and oil regenerative agent is PSurfactant：POil regenerative agent,
In formula, PSurfactantThe addition quality of-surfactant, g；
POil regenerative agentThe addition quality of-oil regenerative agent, g.
The calculating formula of the addition quality of surfactant is PSurfactant=(P1+P2) × A,
In formula, P1The quality of new pitch, g in-bituminous cements；
P2The quality of aged asphalt, g in-bituminous cements；
The addition quality of A-surfactant accounts for the percentage of bituminous cements gross mass, %.
The calculating formula of the addition quality of oil regenerative agent is POil regenerative agent=P2× B,
In formula, P2The quality of aged asphalt, g in-bituminous cements；
The addition quality of B-oil regenerative agent accounts for the percentage of aged asphalt quality in bituminous cements, and %, B can pass through
The grade experiment of the degree of aging of aged asphalt and target pitch is determined.
The addition quality of surfactant is the 0.3-0.6% of bituminous cements gross mass, preferably 0.5%.
The addition quality of oil regenerative agent is the 6.0-12.0% of aged asphalt quality in bituminous cements, preferably
8.5%.
In any of the above-described scheme preferably, the surfactant is fatty glyceride, fatty acid sorbitan, gathered
One or several kinds in sorb ester, sucrose ester.
In any of the above-described scheme preferably, the oil regenerative agent be bright stock when tapped oil, lubricating oil,
One or several kinds in machine oil, heavy oil.
In any of the above-described scheme preferably, the temperature of mixing and stirring of the surfactant and the oil regenerative agent is
40-60℃.The present invention is by experimental results demonstrate at a temperature of 40-60 DEG C, surfactant and oil regenerative agent are in
The state of free-flowing, good fluidity is conducive to the two to be sufficiently mixed, and uniformly, the compound warm mix regenerative agent of preparation is liquid,
With good mobility.When temperature drops to normal temperature, compound warm mix regenerative agent is changed into sticky state, due at 40-60 DEG C
At a temperature of, surfactant and oil regenerative agent have been adequately mixed uniformly, although so compound warm mix regenerative agent under normal temperature
Sticky state is presented, but it is very uniform, fine and smooth, exist without the uneven particulate material of size.
In any of the above-described scheme preferably, the mixing time of the surfactant and the oil regenerative agent is
90-150s.The present invention is by experimental results demonstrate in the range of this mixing time, two kinds of materials can be merged fully uniformly.It is preferred that
, 120s.
Surfactant and oil regenerative agent need to be sufficiently stirred in mixing apparatus.Mixing apparatus can use agitator,
Agitator needs to rotate at a high speed so that two materials are sufficiently stirred for, merge uniform.Optimum speed is 30 turns/min.
The present invention compound warm mix regenerative agent preparation method it is simple, preparation time is short, cost is low, preparation process is without dirt
Dye, will not be damaged to environment and the person.The present invention will indicate that activating agent is organically combined with oil regenerative agent, can realize drip
Blue or green and asphalt mixes and stirs the reduction of temperature and the regeneration of old asphalt mixture, while the compound warm mix regeneration of the present invention
The production preparation process of agent is pollution-free, fundamentally solves due to traditional pitch and asphalt that to mix and stir temperature high, old
The problems such as material utilization rate is low and causes environmental pollution and the wasting of resources.
The preparation method of the warm mix regeneration asphalt of the present invention is simple, and compound warm mix regenerative agent directly, is disposably added
Uniform mixing in pitch is added to, mixing and stirring temperature significantly reduces, this not only reduces the discharge of pernicious gas, reduces cost,
And it has good performance and pavement performance.
Asphalt production department is prepared warm mix regeneration asphalt using compound warm mix regenerative agent according to the preparation method of the present invention
After complete, the blending station of job site is conveyed to, and is saved with bituminous pitch storing tank, warm mix regeneration is then further prepared
Asphalt.
The present invention also provides a kind of warm-mixed recycled asphalt mixture, is mixed by warm mix regeneration asphalt, new mineral aggregate and Bituminous concrete surface
Material, which is mixed and stirred, to be formed, and the warm mix regeneration asphalt is mixed and stirred with above-mentioned compound warm mix regenerative agent by pitch and formed.The pitch is new
Pitch.Compound warm mix regenerative agent directly, is disposably added in pitch, warm mix regeneration asphalt is formed, then by warm mix again
Raw pitch directly, is disposably added in new mineral aggregate and old asphalt mixture, forms warm-mixed recycled asphalt mixture, wherein
The volume of old asphalt mixture is 0-50%.Determine to drip in warm-mixed recycled asphalt mixture by Bitumen Mix Design
The consumption of blue or green cementitious matter is 4.7-5.3%.Aged asphalt in old asphalt mixture accounts for the 4.7-5.3% of old asphalt mixture.
Preferably, the compound warm mix regenerative agent is the composite of warm-mixing agent and regenerative agent.
In any of the above-described scheme preferably, the warm-mixing agent is surfactant, and the regenerative agent regenerates for oil
Agent.
In any of the above-described scheme preferably, the surfactant is fatty glyceride, fatty acid sorbitan, gathered
One or several kinds in sorb ester, sucrose ester.
In any of the above-described scheme preferably, the oil regenerative agent be bright stock when tapped oil, lubricating oil,
One or several kinds in machine oil, heavy oil.
The warm-mixed recycled asphalt mixture of the present invention takes full advantage of old asphalt mixture, and the volume of old asphalt mixture can
50% is reached, compound warm mix regenerative agent therein combines warm-mixing agent with regenerative agent, form composite, can be direct
Ground, disposably it is added in pitch, forms warm mix regeneration asphalt, then warm mix regeneration asphalt is mixed with new mineral aggregate and Bituminous concrete surface
Material is mixed and stirred, and has given full play to the mass action of compound warm mix regenerative agent, and the warm-mixed recycled asphalt mixture thus prepared has good
Good pavement performance.The warm mix of the achievable pitch of the present invention and the regeneration of old asphalt mixture, and then realize ground surface material
Solid waste utilize and energy-saving and emission-reduction double effectses.
The present invention also provides a kind of preparation method of above-mentioned warm-mixed recycled asphalt mixture, comprises the following steps：
(1) warm mix regeneration asphalt is prepared；
(2) warm mix regeneration asphalt is mixed and stirred at a certain temperature with new mineral aggregate and old asphalt mixture；
The warm mix regeneration asphalt is mixed and stirred with compound warm mix regenerative agent by pitch and formed.The pitch is new pitch.
The temperature of mixing and stirring of the warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture is 100-140 DEG C.
In any of the above-described scheme preferably, the warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture are mixed and stirred
Temperature is 110-130 DEG C.
In any of the above-described scheme preferably, the warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture are mixed and stirred
Time is 80-100s.
In any of the above-described scheme preferably, the warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture are mixed and stirred
Time is 90s.
The preparation method of the warm-mixed recycled asphalt mixture of the present invention is simple, will with the addition of the warm mix of compound warm mix regenerative agent
Regeneration asphalt and new mineral aggregate and old asphalt mixture uniform mixing, mixing and stirring temperature significantly reduces, and greatly reduces harmful gas
The discharge of body, reduces cost, and the utilization rate of old asphalt mixture is significantly improved, and the volume of old asphalt mixture can reach 50%,
Prepared warm-mixed recycled asphalt mixture has good pavement performance simultaneously.
Embodiment
In order to be further understood that the content of the invention of the present invention, the present invention is elaborated below in conjunction with specific embodiment.
Embodiment one：
A kind of warm mix regeneration asphalt, is mixed and stirred with compound warm mix regenerative agent by pitch and formed.The pitch is new pitch.Drip
The quality of blue or green cementitious matter is 10000g, and wherein the content of new pitch is 70%, i.e. 7000g, and the content of aged asphalt is 30%, i.e.,
3000g.Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is fatty glyceride, normal temperature
It is yellow, transparent, liquid down；It is dark yellow, viscous fluid under tapped oil when oil regenerative agent is bright stock, normal temperature
State material.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) tapped oil during by fatty glyceride with bright stock is weighed according to a certain percentage.
The addition of fatty glyceride is the 0.5% of bituminous cements quality, i.e. PFatty glyceride=(P1+P2) × A=
10000 × 0.5%=50g；When experiment measures aged asphalt and is regenerated to the pitch with new pitch same levels, oil regenerative agent
Addition is the 8.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 8.5%=255g, so, fatty acid glycerine
The ratio of ester and tapped oil is 1：5.1.
(2) tapped oil when fatty glyceride and bright stock is fitted into agitator and mixed and stirred to uniform shape
State.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 40 DEG C, the mixing time is 150s, make fatty glyceride with
Tapped oil is sufficiently stirred for, merges uniform.The compound warm mix regenerative agent prepared is at normal temperatures black, the material of sticky state, its
Performance is as shown in Table 1.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 120 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 120 DEG C of pitch
With to uniform state, the mixing time is 150s.
The performance of the warm mix regeneration asphalt of preparation is as shown in Table 2.
Embodiment two：
A kind of warm mix regeneration asphalt, is mixed and stirred with compound warm mix regenerative agent by pitch and formed.The pitch is new pitch.Drip
The quality of blue or green cementitious matter is 10000g, and wherein the content of new pitch is 60%, i.e. 6000g, and the content of aged asphalt is 40%, i.e.,
4000g.Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is fatty acid sorbitan, normal temperature
It is yellow, transparent, liquid down；Oil regenerative agent is heavy oil, is dark yellow, viscous liquid state material under normal temperature.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) fatty acid sorbitan is weighed according to a certain percentage with heavy oil.
The addition of fatty acid sorbitan is the 0.6% of bituminous cements quality, i.e. PFatty acid sorbitan=(P1+P2) × A=
10000 × 0.6%=60g；When experiment measures aged asphalt and is regenerated to the pitch with new pitch same levels, oil regenerative agent
Addition is the 10% of aged asphalt quality, i.e. PHeavy oil=P2× B=4000 × 10%=400g, so, fatty acid sorbitan with
The ratio of heavy oil is 1：6.7.
(2) fatty acid sorbitan and heavy oil are fitted into agitator and mixed and stirred to uniform state.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 45 DEG C, the mixing time is 135s, make fatty acid sorbitan with
Heavy oil is sufficiently stirred for, merges uniform.The compound warm mix regenerative agent prepared is black, the material of sticky state, its property at normal temperatures
Can be as shown in Table 1.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 110 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 110 DEG C of pitch
With to uniform state, the mixing time is 165s.
The performance of the warm mix regeneration asphalt of preparation is as shown in Table 2.
Embodiment three：
A kind of warm mix regeneration asphalt, is mixed and stirred with compound warm mix regenerative agent by pitch and formed.The pitch is new pitch.Drip
The quality of blue or green cementitious matter is 10000g, and wherein the content of new pitch is 80%, i.e. 8000g, and the content of aged asphalt is 20%, i.e.,
2000g.Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is
Yellow, transparent, liquid；Oil regenerative agent is lubricating oil, is dark yellow, viscous liquid state material under normal temperature.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) polysorbate is weighed according to a certain percentage with lubricating oil.
The addition of polysorbate is the 0.3% of bituminous cements quality, i.e. PPolysorbate=(P1+P2) × A=10000 ×
0.3%=30g；When experiment measures aged asphalt and is regenerated to the pitch with new pitch same levels, the addition of oil regenerative agent
For the 6.0% of aged asphalt quality, i.e. PLubricating oil=P2× B=2000 × 6.0%=120g, so, polysorbate and lubricating oil
Ratio be 1：4.0.
(2) polysorbate and lubricating oil are fitted into agitator and mixed and stirred to uniform state.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 50 DEG C, the mixing time is 120s, makes polysorbate and lubrication
Oil is sufficiently stirred for, merges uniform.The compound warm mix regenerative agent prepared is black, the material of sticky state, its performance at normal temperatures
As shown in Table 1.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 130 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 130 DEG C of pitch
With to uniform state, the mixing time is 135s.
The performance of the warm mix regeneration asphalt of preparation is as shown in Table 2.
Example IV：
A kind of warm mix regeneration asphalt, is mixed and stirred with compound warm mix regenerative agent by pitch and formed.The pitch is new pitch.Drip
The quality of blue or green cementitious matter is 10000g, and wherein the content of new pitch is 90%, i.e. 9000g, and the content of aged asphalt is 10%, i.e.,
1000g.Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is fatty glyceride and sucrose
It is yellow, transparent, liquid under ester, normal temperature；Oil regenerative agent is lubricating oil and machine oil, is dark yellow, viscous fluid under normal temperature
State material.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) mixture of the mixture of fatty glyceride and sucrose ester and lubricating oil and machine oil is claimed according to a certain percentage
Take.
The addition of the mixture of fatty glyceride and sucrose ester is the 0.3% of bituminous cements quality, i.e.,
PFatty glyceride+sucrose ester=(P1+P2) × A=10000 × 0.3%=30g；Experiment measure aged asphalt be regenerated to it is identical with new pitch
During the pitch of grade, the addition of oil regenerative agent is the 10% of aged asphalt quality, i.e. PLubricating oil+machine oil=P2× B=1000 ×
10%=100g, so, the ratio of the mixture of the mixture and lubricating oil and machine oil of fatty glyceride and sucrose ester is 1：
3.3。
(2) mixture of the mixture of fatty glyceride and sucrose ester and lubricating oil and machine oil is fitted into agitator
Row is mixed and stirred to uniform state.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 55 DEG C, the mixing time is 105s, make fatty glyceride and
Sucrose ester is sufficiently stirred for lubricating oil and machine oil, merges uniform.The compound warm mix regenerative agent prepared is at normal temperatures black, sticky
The material of state, its performance is as shown in Table 1.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 140 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 140 DEG C of pitch
With to uniform state, the mixing time is 120s.
The performance of the warm mix regeneration asphalt of preparation is as shown in Table 2.
Embodiment five：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.45% of bituminous cements quality,
That is PFatty glyceride=(P1+P2) × A=10000 × 0.45%=45g；Experiment measure aged asphalt be regenerated to it is mutually equal with new pitch
During the pitch of level, the addition of oil regenerative agent is the 6.0% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 6.0%
=180g, so, the ratio of fatty glyceride and tapped oil is 1：4.0.Fatty glyceride and tapped oil mix and stir temperature
For 60 DEG C, the mixing time is 90s.
When preparing warm mix regeneration asphalt, pitch is heated to 100 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 180s is mixed and stirred.
Embodiment six：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.55% of bituminous cements quality,
That is PFatty glyceride=(P1+P2) × A=10000 × 0.55%=55g；Experiment measure aged asphalt be regenerated to it is mutually equal with new pitch
During the pitch of level, the addition of oil regenerative agent is the 7.0% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 7.0%
=210g, so, the ratio of fatty glyceride and tapped oil is 1：3.8.Fatty glyceride and tapped oil mix and stir temperature
For 60 DEG C, the mixing time is 110s.
When preparing warm mix regeneration asphalt, pitch is heated to 115 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 170s is mixed and stirred.
Embodiment seven：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.5% of bituminous cements quality, i.e.,
PFatty glyceride=(P1+P2) × A=10000 × 0.5%=50g；Experiment measures aged asphalt and is regenerated to and new pitch same levels
Pitch when, the addition of oil regenerative agent is the 8.0% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 8.0%=
240g, so, the ratio of fatty glyceride and tapped oil is 1：4.8.The temperature of mixing and stirring of fatty glyceride and tapped oil is
60 DEG C, the mixing time is 125s.
When preparing warm mix regeneration asphalt, pitch is heated to 125 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 160s is mixed and stirred.
Embodiment eight：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.4% of bituminous cements quality, i.e.,
PFatty glyceride=(P1+P2) × A=10000 × 0.4%=40g；Experiment measures aged asphalt and is regenerated to and new pitch same levels
Pitch when, the addition of oil regenerative agent is the 6.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 6.5%=
195g, so, the ratio of fatty glyceride and tapped oil is 1：4.9.The temperature of mixing and stirring of fatty glyceride and tapped oil is
55 DEG C, the mixing time is 100s.
When preparing warm mix regeneration asphalt, pitch is heated to 135 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 140s is mixed and stirred.
Embodiment nine：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.6% of bituminous cements quality, i.e.,
PFatty glyceride=(P1+P2) × A=10000 × 0.6%=60g；Experiment measures aged asphalt and is regenerated to and new pitch same levels
Pitch when, the addition of oil regenerative agent is the 8.0% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 8.0%=
240g, so, the ratio of fatty glyceride and tapped oil is 1：4.0.The temperature of mixing and stirring of fatty glyceride and tapped oil is
50 DEG C, the mixing time is 125s.
When preparing warm mix regeneration asphalt, pitch is heated to 105 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 180s is mixed and stirred.
Embodiment ten：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.5% of bituminous cements quality, i.e.,
PFatty glyceride=(P1+P2) × A=10000 × 0.5%=50g；Experiment measures aged asphalt and is regenerated to and new pitch same levels
Pitch when, the addition of oil regenerative agent is the 7.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 7.5%=
225g, so, the ratio of fatty glyceride and tapped oil is 1：4.5.The temperature of mixing and stirring of fatty glyceride and tapped oil is
40 DEG C, the mixing time is 145s.
When preparing warm mix regeneration asphalt, pitch is heated to 120 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 160s is mixed and stirred.
Embodiment 11：
A kind of warm mix regeneration asphalt, it is identical with embodiment one, unlike：
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.55% of bituminous cements quality,
That is PFatty glyceride=(P1+P2) × A=10000 × 0.55%=55g；Experiment measure aged asphalt be regenerated to it is mutually equal with new pitch
During the pitch of level, the addition of oil regenerative agent is the 8.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 8.5%
=255g, so, the ratio of fatty glyceride and tapped oil is 1：4.6.Fatty glyceride and tapped oil mix and stir temperature
For 45 DEG C, the mixing time is 115s.
When preparing warm mix regeneration asphalt, pitch is heated to 115 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 145s is mixed and stirred.
Embodiment 12：
A kind of warm-mixed recycled asphalt mixture, is mixed and stirred and is formed by warm mix regeneration asphalt, new mineral aggregate and old asphalt mixture, institute
State warm mix regeneration asphalt and mixed and stirred by pitch with compound warm mix regenerative agent and formed.The pitch is new pitch.
Prepare 2 × 105G warm-mixed recycled asphalt mixtures.The volume of old asphalt mixture is 30%, i.e., 6 × 104G, wherein
Aged asphalt content is the quality P of 5.0%, i.e. aged asphalt in old material2=3000g.Pass through Bitumen Mix Design
The consumption for determining bituminous cements in warm-mixed recycled asphalt mixture is that the quality of 4.8%, i.e. bituminous cements is 9600g.Drip
Blue or green cementitious matter includes new pitch and aged asphalt, the quality P of new pitch1=9600-3000=6600g.
Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is fatty glyceride, often
Lower temperature is yellow, transparent, liquid；Tapped oil when oil regenerative agent is bright stock is dark yellow under normal temperature, sticky
Liquid.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) tapped oil during by fatty glyceride with bright stock is weighed according to a certain percentage.
The addition of fatty glyceride is the 0.5% of bituminous cements quality, i.e. PFatty glyceride=(P1+P2) × A=
9600 × 0.5%=48g；When experiment measures aged asphalt and is regenerated to the pitch with new pitch same levels, oil regenerative agent
Addition is the 8.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3000 × 8.5%=255g, so, fatty acid glycerine
The ratio of ester and tapped oil is 1：5.3.
(2) tapped oil when fatty glyceride and bright stock is fitted into agitator and mixed and stirred to uniform shape
State.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 40 DEG C, the mixing time is 150s, make fatty glyceride with
Tapped oil is sufficiently stirred for, merges uniform.The compound warm mix regenerative agent prepared is black, the material of sticky state at normal temperatures.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 120 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 120 DEG C of pitch
With to uniform state, the mixing time is 150s.
Prepare above-mentioned warm-mixed recycled asphalt mixture：By the above-mentioned warm mix regeneration asphalt prepared and new mineral aggregate and old drip
Blue or green compound is mixed and stirred, and mixes and stirs temperature for 120 DEG C, the mixing time is 100s, uniform mixing.The warm mix regeneration drip of preparation
As shown in Table 3, pavement performance is as shown in Table 4 for the compaction capacity of blue or green compound.
Embodiment 13：
A kind of warm-mixed recycled asphalt mixture, is mixed and stirred and is formed by warm mix regeneration asphalt, new mineral aggregate and old asphalt mixture, institute
State warm mix regeneration asphalt and mixed and stirred by pitch with compound warm mix regenerative agent and formed.The pitch is new pitch.
Prepare 2 × 105G warm-mixed recycled asphalt mixtures.The volume of old asphalt mixture is 50%, i.e., 1 × 105G, wherein
Aged asphalt content is the quality P of 4.7%, i.e. aged asphalt in old material2=4700g.Pass through Bitumen Mix Design
The consumption for determining bituminous cements in warm-mixed recycled asphalt mixture is that the quality of 5.0%, i.e. bituminous cements is 10000g.Drip
Blue or green cementitious matter includes new pitch and aged asphalt, the quality P of new pitch1=10000-4700=5300g.
Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Under surfactant is polysorbate, normal temperature
For yellow, transparent, liquid；Oil regenerative agent is machine oil, is dark yellow, viscous liquid state material under normal temperature.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) polysorbate is weighed according to a certain percentage with machine oil.
The addition of polysorbate is the 0.6% of bituminous cements quality, i.e. PPolysorbate=(P1+P2) × A=10000 ×
0.6%=60g；When experiment measures aged asphalt and is regenerated to the pitch with new pitch same levels, the addition of oil regenerative agent
For the 6.0% of aged asphalt quality, i.e. PMachine oil=P2× B=4700 × 6.0%=282g, so, the ratio of polysorbate and machine oil
Example is 1：4.7.
(2) polysorbate and machine oil are fitted into agitator and mixed and stirred to uniform state.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 50 DEG C, the mixing time is 120s, makes polysorbate and machine oil
It is sufficiently stirred for, merges uniform.The compound warm mix regenerative agent prepared is black, the material of sticky state at normal temperatures.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 140 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 140 DEG C of pitch
With to uniform state, the mixing time is 120s.
Prepare above-mentioned warm-mixed recycled asphalt mixture：By the above-mentioned warm mix regeneration asphalt prepared and new mineral aggregate and old drip
Blue or green compound is mixed and stirred, and mixes and stirs temperature for 100 DEG C, the mixing time is 95s, uniform mixing.The warm mix regeneration drip of preparation
As shown in Table 3, pavement performance is as shown in Table 4 for the compaction capacity of blue or green compound.
Embodiment 14：
A kind of warm-mixed recycled asphalt mixture, is mixed and stirred and is formed by warm mix regeneration asphalt, new mineral aggregate and old asphalt mixture, institute
State warm mix regeneration asphalt and mixed and stirred by pitch with compound warm mix regenerative agent and formed.The pitch is new pitch.
Prepare 2 × 105G warm-mixed recycled asphalt mixtures.The volume of old asphalt mixture is 40%, i.e., 8 × 104G, wherein
Aged asphalt content is the quality P of 4.8%, i.e. aged asphalt in old material2=3840g.Pass through Bitumen Mix Design
The consumption for determining bituminous cements in warm-mixed recycled asphalt mixture is that the quality of 5.1%, i.e. bituminous cements is 10200g.Drip
Blue or green cementitious matter includes new pitch and aged asphalt, the quality P of new pitch1=10200-3840=6360g.
Compound warm mix regenerative agent includes surfactant and oil regenerative agent.Surfactant is fatty glyceride and poly-
It is yellow, transparent, liquid under sorb ester, normal temperature；Oil regenerative agent is heavy oil and lubricating oil, is dark yellow under normal temperature, glutinous
Thick liquid.
Above-mentioned compound warm mix regenerative agent is prepared, is comprised the following steps：
(1) by the mixture of the mixture of fatty glyceride and polysorbate and heavy oil and lubricating oil according to a certain percentage
Weigh.
The addition of fatty glyceride and polysorbate is the 0.4% of bituminous cements quality, i.e. PFatty glyceride+poly- sorb is smooth
=(P1+P2) × A=10200 × 0.4%=40.8g；Experiment measures aged asphalt and is regenerated to pitch with new pitch same levels
When, the addition of oil regenerative agent is the 7.0% of aged asphalt quality, i.e. PHeavy oil+lubricating oil=P2× B=3840 × 7.0%=
268.8g, so, the ratio of the mixture of the mixture and heavy oil and lubricating oil of fatty glyceride and polysorbate is 1：
6.6。
(2) mixture of the mixture of fatty glyceride and polysorbate and heavy oil and lubricating oil is fitted into agitator
Mixed and stirred to uniform state.
The rotating speed of agitator is 30 turns/min, mixes and stirs temperature for 55 DEG C, the mixing time is 110s, make fatty glyceride and
Polysorbate is sufficiently stirred for heavy oil and lubricating oil, merges uniform.The compound warm mix regenerative agent prepared is at normal temperatures black, sticked
The material of thick state.
Above-mentioned warm mix regeneration asphalt is prepared, is comprised the following steps：
(1) above-mentioned pitch is heated to 130 DEG C and mixes and stirs temperature, be at flow regime.
(2) the compound warm mix regenerative agent of above-mentioned preparation is directly appended to have been heated to and mixed rapidly in 130 DEG C of pitch
With to uniform state, the mixing time is 130s.
Prepare above-mentioned warm-mixed recycled asphalt mixture：By the above-mentioned warm mix regeneration asphalt prepared and new mineral aggregate and old drip
Blue or green compound is mixed and stirred, and mixes and stirs temperature for 140 DEG C, the mixing time is 80s, uniform mixing.The warm mix regeneration drip of preparation
As shown in Table 3, pavement performance is as shown in Table 4 for the compaction capacity of blue or green compound.
Embodiment 15：
A kind of warm-mixed recycled asphalt mixture, it is identical with embodiment 12, unlike：
Prepare 2 × 105G warm-mixed recycled asphalt mixtures.The volume of old asphalt mixture is 45%, i.e., 9 × 104G, wherein
The content of aged asphalt is the quality P of 4.9%, i.e. aged asphalt in old material2=4410g.Set by Bituminous Mixture Ratio
Meter determines that the quality that the consumption of bituminous cements in warm-mixed recycled asphalt mixture is 5.2%, i.e. bituminous cements is 10400g.
Bituminous cements includes new pitch and aged asphalt, the quality P of new pitch1=10400-4410=5990g.
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.45% of bituminous cements quality,
That is PFatty glyceride=(P1+P2) × A=10400 × 0.45%=46.8g；Experiment measure aged asphalt be regenerated to it is identical with new pitch
During the pitch of grade, the addition of oil regenerative agent is the 6.5% of aged asphalt quality, i.e. PTapped oil=P2× B=4410 ×
6.5%=286.65g, so, the ratio of fatty glyceride and tapped oil is 1：6.1.Fatty glyceride and tapped oil
Temperature is mixed and stirred for 52 DEG C, the mixing time is 100s.
When preparing warm mix regeneration asphalt, pitch is heated to 115 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 140s is mixed and stirred.
When preparing warm-mixed recycled asphalt mixture, warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture mix and stir temperature
Spend for 125 DEG C, the mixing time is 90s.
Embodiment 16：
A kind of warm-mixed recycled asphalt mixture, it is identical with embodiment 12, unlike：
Prepare 2 × 105G warm-mixed recycled asphalt mixtures.The volume of old asphalt mixture is 35%, i.e., 7 × 104G, wherein
The content of aged asphalt is the quality P of 5.2%, i.e. aged asphalt in old material2=3640g.Set by Bituminous Mixture Ratio
Meter determines that the quality that the consumption of bituminous cements in warm-mixed recycled asphalt mixture is 4.9%, i.e. bituminous cements is 9800g.
Bituminous cements includes new pitch and aged asphalt, the quality P of new pitch1=9800-3640=6160g.
When preparing compound warm mix regenerative agent, the addition of fatty glyceride is the 0.4% of bituminous cements quality, i.e.,
PFatty glyceride=(P1+P2) × A=9800 × 0.4%=39.2g；Experiment measures aged asphalt and is regenerated to and new pitch same levels
Pitch when, the addition of oil regenerative agent is the 7.5% of aged asphalt quality, i.e. PTapped oil=P2× B=3640 × 7.5%=
273g, so, the ratio of fatty glyceride and tapped oil is 1：7.0.The temperature of mixing and stirring of fatty glyceride and tapped oil is
48 DEG C, the mixing time is 140s.
When preparing warm mix regeneration asphalt, pitch is heated to 105 DEG C and mixes and stirs temperature, and compound warm mix regenerative agent is directly added
Into pitch, 160s is mixed and stirred.
When preparing warm-mixed recycled asphalt mixture, warm mix regeneration asphalt and new mineral aggregate and old asphalt mixture mix and stir temperature
Spend for 115 DEG C, the mixing time is 93s.
Table one：The performance of compound warm mix regenerative agent
Table two：The performance of warm mix regeneration asphalt
Table three：AC-13 warm-mixed recycled asphalt mixture compaction capacities
Table four：AC-13 warm-mixed recycled asphalt mixture pavement performances
It will be apparent to those skilled in the art that warm mix regeneration asphalt of the present invention and preparation method thereof includes the invention described above
The content of the invention of specification and any combination of embodiment part, as space is limited and to make specification concisely without inciting somebody to action
Each scheme that these combinations are constituted is described one by one.Within the spirit and principles of the invention, any modification for being made, equally replace
Change, improve, should be included in the scope of the protection.
Claims (7)
1. a kind of warm mix regeneration asphalt, it is characterised in that：The warm mix regeneration asphalt is mixed and stirred by pitch with compound warm mix regenerative agent
Form, the compound warm mix regenerative agent is the composite of warm-mixing agent and regenerative agent, and the warm-mixing agent is surfactant, described
Regenerative agent is oil regenerative agent；The surfactant is fatty glyceride, fatty acid sorbitan, polysorbate, sucrose ester
In one or several kinds, tapped oil, lubricating oil, machine oil when the oil regenerative agent is bright stock, one in heavy oil
Plant or several；Warm mix regeneration temperature is 100-110 DEG C.
2. the preparation method of warm mix regeneration asphalt as claimed in claim 1, comprises the following steps：
Pitch is heated to mix and stir temperature；
Compound warm mix regenerative agent is added in the pitch for having been heated to and mix and stir temperature and mixed and stirred；
Wherein, the preparation method for being combined warm mix regenerative agent is as follows：Surfactant is claimed according to a certain percentage with oil regenerative agent
Take, then surfactant and oil regenerative agent are fitted into mixing apparatus mixed and stirred；
It is characterized in that：The compound warm mix regenerative agent is the composite of warm-mixing agent and regenerative agent；The surfactant adds
Plus the calculation formula of quality is PSurfactant=（P1+P2）× A, the calculation formula of the oil regenerative agent addition quality is POil regenerative agent=
P2× B,
Wherein, P1The quality of new pitch, g in-bituminous cements；
P2The quality of aged asphalt, g in-bituminous cements；
The addition quality of A-surfactant accounts for the percentage of bituminous cements gross mass, %；
The addition quality of B-oil regenerative agent accounts for the percentage of aged asphalt quality in bituminous cements, %；
The addition quality of the surfactant is the 0.3-0.6% of bituminous cements gross mass, the addition of the oil regenerative agent
Quality is the 6.0-12.0% of aged asphalt quality in bituminous cements.
3. the preparation method of warm mix regeneration asphalt as claimed in claim 2, it is characterised in that：The compound warm mix regenerative agent with
The mixing time of pitch is 120-180s.
4. the preparation method of warm mix regeneration asphalt as claimed in claim 3, it is characterised in that：The compound warm mix regenerative agent with
The mixing time of pitch is 150s.
5. the preparation method of warm mix regeneration asphalt as claimed in claim 2, it is characterised in that：The surfactant with it is described
Oil regenerative agent forms composite after mixing and stirring, and the composite is compound warm mix regenerative agent.
6. the preparation method of warm mix regeneration asphalt as claimed in claim 2, it is characterised in that：The surfactant with it is described
The temperature of mixing and stirring of oil regenerative agent is 40-60 DEG C.
7. the preparation method of warm mix regeneration asphalt as claimed in claim 2, it is characterised in that：The surfactant with it is described
The mixing time of oil regenerative agent is 90-150s.
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| CN105255205B (en) * | 2015-10-21 | 2017-08-25 | 王立志 | A kind of low-temp recovery asphalt and preparation method thereof |
| CN105670316B (en) * | 2016-02-04 | 2018-06-08 | 武汉成世通环保沥青工程有限公司 | Common mid temperature pitch of high solids content and preparation method thereof |
| CN109233306A (en) * | 2018-07-11 | 2019-01-18 | 北京建筑大学 | A kind of pitch warm mix modifying regenerant and preparation method thereof |
| CN110499035A (en) * | 2019-09-27 | 2019-11-26 | 郑州航空工业管理学院 | A kind of warm mix flame-retardant pitch and preparation method thereof |
| CN110964336A (en) * | 2019-11-29 | 2020-04-07 | 东莞广泰公路材料科技有限公司 | Recycled asphalt mixture |
| CN112062495A (en) * | 2020-09-17 | 2020-12-11 | 西南交通大学 | Warm-mix regenerant and preparation method of warm-mix regenerated asphalt |
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