WO2022027778A1 - High-efficiency reclaimed asphalt mixture and preparation process thereof - Google Patents

High-efficiency reclaimed asphalt mixture and preparation process thereof Download PDF

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Publication number
WO2022027778A1
WO2022027778A1 PCT/CN2020/114529 CN2020114529W WO2022027778A1 WO 2022027778 A1 WO2022027778 A1 WO 2022027778A1 CN 2020114529 W CN2020114529 W CN 2020114529W WO 2022027778 A1 WO2022027778 A1 WO 2022027778A1
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Prior art keywords
asphalt mixture
efficiency
parts
rap
drying cylinder
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PCT/CN2020/114529
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French (fr)
Chinese (zh)
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陈李峰
潘友强
李款
张志祥
关永胜
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江苏中路工程技术研究院有限公司
江苏中路交通科学技术有限公司
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Publication of WO2022027778A1 publication Critical patent/WO2022027778A1/en

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
    • C04B26/02Macromolecular compounds
    • C04B26/26Bituminous materials, e.g. tar, pitch
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/0075Uses not provided for elsewhere in C04B2111/00 for road construction

Definitions

  • the invention relates to an asphalt mixture, in particular to a high-efficiency asphalt regeneration mixture and a preparation process thereof.
  • the implementation process of asphalt pavement regeneration technology is to firstly excavate and mill the old asphalt pavement that needs to be renovated or discarded to obtain waste asphalt mixture, and then combine it with new aggregates, new asphalt (need to add regenerant if necessary) and other materials. Re-mix to form a recycled asphalt mixture with certain road performance, and the regenerated asphalt mixture can be used for laying the surface layer or base layer of the asphalt pavement.
  • the old material is firstly crushed, screened and classified, and its variability is effectively controlled; secondly, the mixing process of hot recycled mixture is similar to conventional The hot mix is carried out at a higher mixing temperature, so the old asphalt in the waste asphalt mixture is easier to fuse with the new asphalt and rejuvenating agent, and the regeneration effect of the old asphalt is good.
  • the produced factory-mixed hot recycled mixture has the best performance and is easy to control, and the uniformity of the mixture Well, it has the widest scope of application.
  • the designed thermal regeneration mixture has a low content of old materials, a low effective regeneration rate of the old materials, high content of new asphalt or regenerant to be added, and unstable quality of the recycled mixture.
  • the poor road performance of the recycled mixture reduces the economic advantage of the recycled mixture and seriously affects the industrialization and large-scale implementation of thermal regeneration technology.
  • the invention provides a high-efficiency recycled asphalt mixture and a preparation process thereof, which can break through key problems such as classification of recycled materials, special recycled asphalt, mixture design, production, and matching of construction equipment, etc.
  • the performance of the mixed material reaches the level of the new material, and the unit cost is lower than the target of the new material, so as to promote the industrialized utilization of road waste materials, improve the recycling efficiency of waste materials, consolidate the leading position of Jiangsu province in the level of highway construction and maintenance in the country, and promote highway construction and maintenance. High-quality development of the industry.
  • the purpose of the present invention is to provide a hot-mixed high-efficiency recycled asphalt mixture with high regeneration rate, low production cost, excellent high and low temperature and fatigue properties of the mixture and its preparation process.
  • a high-efficiency recycled asphalt mixture is characterized in that it comprises 1.0 to 3.0 parts by mass of special recycled asphalt and 100 parts of aggregate;
  • the 100 parts of aggregates include raw materials in the following proportions by mass: 0 to 30 parts of new aggregates with a particle size of 10mm to 25mm, 0 to 70 parts of RAP materials with a particle size of 10mm to 20mm, and a particle size of 5mm to 5mm. 0-80 parts of 10mm RAP material, 0-20 parts of RAP material with a particle size of 0mm-5mm, and 0-3 parts of mineral powder.
  • the new aggregate is limestone or basalt with a particle size of 10-25 mm.
  • the regenerated special asphalt is composed of matrix asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic oil regenerant, and stabilizer:
  • the mass percentages of the components of the base asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic oil regenerant, and stabilizer are as follows:
  • the styrene-containing modifier is one or both of styrene-butadiene-styrene triblock copolymer SBS and styrene-butadiene rubber SBR.
  • the multi-chain polyolefin type modifier is oxidized polyethylene wax, the melting point is 100-150°C, the viscosity at 140°C is 200-5000cps, and the acid value is 14-55mg KOH/g.
  • Described regenerant is a kind of in naphthenic oil or aromatic base oil
  • the rubber oil is one of naphthenic rubber oil and aromatic rubber oil.
  • the stabilizer is one of elemental sulfur, diaryl disulfide and nitro-substituted diaryl disulfide.
  • the preparation method of the regenerated special asphalt comprises the following steps:
  • step (2) Adding rubber oil to the asphalt obtained in step (1), stirring at 170-180°C for 0.5h-1h; then slowly adding stabilizer, stirring for 2-3h, then adding at 170-180°C
  • the regenerant is continuously stirred for 8h to 24h, and then the material is discharged and filled to obtain the product.
  • the present invention also provides a process for preparing high-efficiency regenerated asphalt mixture, which is characterized by comprising the following steps:
  • Step 1 The RAP material is planed, milled and crushed, and divided into three grades: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate, or 20-10mm RAP aggregate and 10-0mm RAP aggregate;
  • Step 2 heating the new aggregate and mineral powder in the first drying cylinder of the gas heating method
  • Step 3 Heat the third (or two) RAP material in the second drying cylinder of the gas heating method
  • Step 4 After measuring, put the new aggregate, mineral powder, and third-speed (or second-speed) RAP material into the mixing pot, and stir evenly;
  • Step 5 adding recycled special asphalt into the mixing pot and stirring evenly to obtain a high-efficiency recycled asphalt mixture.
  • planing, milling and crushing method in the step 1 is a milling machine + crushing and screening.
  • the heating method in the first drying cylinder is that the new aggregate is heated in the drying cylinder of the original stirring device, and the dried hot air is introduced into the drying cylinder, and the convection between the aggregate and the gas is realized in the drying cylinder. ; There is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator, which is conducive to the reuse of heat energy.
  • the heating temperature in the first drying cylinder is 170°C to 185°C.
  • the heating method in the second drying cylinder in the third step is to adopt a downstream heating method, and the dried hot air is introduced into the old asphalt mixture drying cylinder, and the convection of the mixture and the gas is realized in the drying cylinder; There is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator.
  • the recovered gas may have "blue smoke” and water vapor from heating. Therefore, before entering the hot gas generator, the water vapor is separated to ensure the drying of the gas, and the "blue smoke” produced is burned by reheating, which can not only prevent pollution, but also generate heat energy.
  • the heating temperature in the second drying cylinder is 120°C to 140°C.
  • the stirring equipment in the step 4 adopts intermittent forced stirring equipment.
  • the stirring device in the fourth step is a heating-type stirring device, so that the regenerated mixture can reach the discharge temperature uniformly.
  • the temperature of the recycled special asphalt in the step 5 is 165°C to 180°C.
  • the stirring temperature in the fifth step is 130°C to 150°C.
  • the asphalt used in the high-efficiency regenerated asphalt mixture provided by the present invention is a self-developed special cementing material for regeneration, which contains a multi-chain polyolefin modifier and a naphthenic oil regenerating agent, which can significantly improve the high and low temperature performance and regeneration performance of the asphalt.
  • the multi-chain polyolefin modifier and SBS copolymer can be combined into a new graft copolymer. This copolymer has high polarity and can form a uniform structure with no phase separation from the asphalt, effectively improving the stability of the asphalt. properties, high temperature rheology and temperature sensitivity.
  • the naphthenic oil regenerant used in the present invention has good compatibility, has good dispersibility for insoluble sulfides, and has remarkable reconciliation and regeneration performance for asphalt components. And it has good stability, no pollution and no toxicity, which can reduce environmental pollution during use and improve the protection of the environment.
  • the high-efficiency recycled asphalt mixture provided by the present invention aims at the disadvantages of the existing recycled mixture design, which is the first volume design and then the mixture performance verification.
  • the Asphalt Mixture Design Method (LPC) which forms a performance balance-based method for the preparation of recycled asphalt mixtures.
  • LPC Asphalt Mixture Design Method
  • the proportioning design the gradation of the recycled asphalt mixture can be adjusted freely. Even the densely mixed mixture with extremely small porosity can ensure its high temperature performance due to the effect of the recycled special asphalt.
  • the invention integrates the French high-modulus asphalt mixture design method (LPC) and the American asphalt mixture design method based on performance balance (BMD), and strives for more space for the synergistic improvement of the fatigue resistance and low temperature performance of the recycled asphalt mixture , fully guarantee the overall improvement of the overall performance of the recycled mixture.
  • LPC French high-modulus asphalt mixture design method
  • BMD performance balance
  • High-efficiency recycled asphalt mixture including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 45 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material and 5 parts of RAP material with a particle size of 0 mm to 5 mm.
  • the high-efficiency recycled asphalt mixture is SMA-13 type asphalt mixture.
  • the new aggregate added to the high-efficiency regenerated asphalt mixture is basalt with a particle size of 10 mm to 20 mm.
  • the RAP material added to the high-efficiency recycled asphalt mixture is the SMA-13 waste asphalt mixture recovered by milling.
  • the preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
  • Step 1 Planing, milling and crushing the SMA-13 waste asphalt mixture into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
  • Step 2 heating 20 parts of new aggregates of 10mm to 20mm in the first drying cylinder of the gas heating method, and the heating temperature is 170°C;
  • Step 3 Put 45 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 130 °C;
  • Step 4 Put the new aggregate and the third-speed RAP material into the mixing pot and stir evenly;
  • Step 5 Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 1#, and the stirring temperature is 140°C.
  • the test results in Table 1 show that the high temperature performance of 1# recycled asphalt mixture is excellent, the stability is increased from 7.8kN to 12.54kN, and the dynamic stability is increased from 4238 times/mm to 9545 times/mm.
  • the low temperature crack resistance of the mixture is basically restored, and the maximum bending and tensile strain at low temperature is increased from 1972 ⁇ to 2299 ⁇ .
  • the improvement of high and low temperature performance shows that the regeneration effect of 1# recycled asphalt mixture is good.
  • the high-efficiency recycled asphalt mixture includes, in parts by weight: 2.2 parts of recycled special asphalt, 60 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and RAP with a particle size of 0mm to 5mm 10 servings.
  • the high-efficiency regenerated asphalt mixture is AC-20 type fully regenerated asphalt mixture.
  • the RAP material added to the high-efficiency recycled asphalt mixture is the AC-20 type waste asphalt mixture recovered by milling.
  • the preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
  • Step 1 Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
  • Step 2 put 45 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 °C;
  • Step 3 Put the third gear RAP material into the mixing pot and stir evenly;
  • Step 5 Add 175°C regenerated special asphalt into the mixing pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 2#, and the stirring temperature is 140°C.
  • the test results in Table 2 show that the high temperature performance of the 2# recycled asphalt mixture has been improved, the stability has increased from 5.6kN to 8.72kN, and the dynamic stability has increased from 4500 times/mm to 6387 times/mm.
  • the low temperature is slightly improved, and the maximum bending and tensile strain at low temperature is increased from 1412 ⁇ to 1514 ⁇ .
  • the 2# recycled asphalt mixture implemented this time is a fully recycled asphalt mixture, and its regeneration effect is slightly improved.
  • High-efficiency recycled asphalt mixture including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 45 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material and 5 parts of RAP material with a particle size of 0 mm to 5 mm.
  • the high-efficiency regenerated asphalt mixture is AC-20 type asphalt mixture.
  • the new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10 mm to 20 mm.
  • the RAP material added to the high-efficiency recycled asphalt mixture is AC-20 waste and old asphalt mixture recovered by milling.
  • the preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
  • Step 1 Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
  • Step 2 heating 20 parts of new aggregates of 10mm to 20mm in the first drying cylinder of the gas heating method, and the heating temperature is 170°C;
  • Step 3 Put 45 parts of RAP material with a particle size of 10mm-20mm, 30 parts of RAP material with a particle size of 5mm-10mm, and 5 parts of RAP material with a particle size of 0mm-5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 °C;
  • Step 4 Put the new aggregate and the third-speed RAP material into the mixing pot and stir evenly;
  • Step 5 Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 3#, and the stirring temperature is 140°C.
  • Test items unit High-efficiency recycled mixture 3# test results
  • the test results in Table 3 show that the 3# recycled asphalt mixture has excellent high temperature performance, the stability is increased from 5.6kN to 8.43kN, and the dynamic stability is increased from 4500 times/mm to 8750 times/mm.
  • the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412 ⁇ to 1887 ⁇ .
  • the improvement of high and low temperature performance shows that the regeneration effect of 3# recycled asphalt mixture is good.
  • High-efficiency recycled asphalt mixture including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 44 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material, 5 parts of RAP material with a particle size of 0mm to 5mm, and 1 part of mineral powder.
  • the high-efficiency recycled asphalt mixture is AC-20 type asphalt mixture.
  • the new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10 mm to 20 mm.
  • the RAP material added to the high-efficiency recycled asphalt mixture is AC-20 waste and old asphalt mixture recovered by milling.
  • the preparation method of high-efficiency recycled asphalt mixture is characterized in that, specifically comprises the following steps:
  • Step 1 Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
  • Step 2 heating 20 parts of 10mm-20mm new aggregate and 1 part of mineral powder in the first drying cylinder of the gas heating method, and the heating temperature is 170 ° C;
  • Step 3 Put 44 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 °C;
  • Step 4 Put the new aggregate, mineral powder and RAP material in the third gear into the mixing pot and stir evenly;
  • Step 5 Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency recycled asphalt mixture 4#, and the stirring temperature is 140°C.
  • Test items unit High-efficiency recycled mixture 4# test results
  • the test results in Table 4 show that the high temperature performance of 4# recycled asphalt mixture is excellent, the stability is increased from 5.6kN to 8.55kN, and the dynamic stability is increased from 4500 times/mm to 9844 times/mm.
  • the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412 ⁇ to 1821 ⁇ .
  • the improvement of high and low temperature performance shows that the regeneration effect of 4# recycled asphalt mixture is good.
  • High-efficiency recycled asphalt mixture including by weight: 2 parts of recycled special asphalt, 25 parts of new aggregate with particle size of 10mm-15mm, 22 parts of RAP material with particle size of 10mm-20mm, particle size of 0mm-10mm 53 servings of RAP material.
  • the high-efficiency recycled asphalt mixture is AC-13 type asphalt mixture.
  • the new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10mm-15mm.
  • the RAP material added to the high-efficiency recycled asphalt mixture is AC-13 waste and old asphalt mixture recovered by milling.
  • the preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
  • Step 1 Plan, mill and crush the AC-13 waste asphalt mixture, and divide it into two blocks of 20-10mm RAP aggregate and 10-0mm RAP aggregate;
  • Step 2 heating 25 parts of new aggregates of 10mm to 15mm in the first drying cylinder of the gas heating method, and the heating temperature is 180°C;
  • Step 3 heating 22 parts of RAP material with a particle size of 10mm to 20mm and 53 parts of RAP material with a particle size of 0mm to 10mm in the second drying cylinder of the gas heating method, and the heating temperature is 135 ° C;
  • Step 4 Put the new aggregate and RAP material in two blocks into the mixing pot and stir evenly;
  • Step 5 Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 5#, and the stirring temperature is 140°C.
  • Test items unit High-efficiency recycled mixture 5# test results
  • the test results in Table 5 show that the 5# recycled asphalt mixture has excellent high temperature performance, the stability is increased from 5.6kN to 10.51kN, and the dynamic stability is increased from 4500 times/mm to 6058 times/mm.
  • the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412 ⁇ to 2405 ⁇ .
  • the improvement of high and low temperature performance shows that the regeneration effect of 5# recycled asphalt mixture is good.

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  • Ceramic Engineering (AREA)
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Abstract

Disclosed is a high-efficiency reclaimed asphalt mixture, comprising in terms of parts by mass a reclaimed dedicated asphalt and 100 parts of a core material. The 100 parts of the core material comprise the following raw materials in terms of parts by mass: 0-30 parts of a newly aggregated material of which the particle size is 10 mm to 25 mm, 0-70 parts of a RAP material of which the particle size is 10 mm to 20 mm, 0-80 parts of a RAP material of which the particle size is 5 mm to 10 mm, 0-20 parts of a RAP material of which the particle size is 0 mm to 5 mm, and 0-3 parts of a mineral powder. Also provided in the present invention is a preparation process for the high-efficiency reclaimed asphalt mixture. In the product high-efficiency reclaimed asphalt mixture of the present invention, the blending ratio of the RAP materials can be 70% or more, mixing entirely in a reclamation plant can be attained at best, and this is applicable in various grades of road surfaces.

Description

一种高效再生沥青混合料及其制备工艺A kind of high-efficiency recycled asphalt mixture and its preparation process 技术领域technical field
本发明涉及一种沥青混合料,具体涉及一种高效沥青再生混合料及其制备工艺。The invention relates to an asphalt mixture, in particular to a high-efficiency asphalt regeneration mixture and a preparation process thereof.
背景技术Background technique
我国公路发展正从建养并重向养护时代转变,道路养护每年产生数亿立方的废旧材料,需要进行处置和利用,造成巨大的生态环境压力。如果将废旧材料作为垃圾废弃填埋,会占用巨大的堆放空间。如果将废旧沥青混合料进行简单机械处理作为路基垫层,不能充分发挥废旧沥青混合料的功用,造成严重的资源浪费。因此回收这个废旧材料再利用会节省大量成本,具有重要的经济和社会价值。my country's highway development is changing from an era of equal emphasis on construction and maintenance to the era of maintenance. Road maintenance produces hundreds of millions of cubic meters of waste materials every year, which need to be disposed of and utilized, causing huge pressure on the ecological environment. If waste materials are disposed of as waste in landfills, it will take up a huge amount of storage space. If the waste asphalt mixture is simply mechanically treated as the subgrade cushion, the function of the waste asphalt mixture cannot be fully exerted, resulting in a serious waste of resources. Therefore, recycling this waste material for reuse will save a lot of cost and have important economic and social value.
沥青路面再生技术的实施过程是,将需要翻修或者废弃的旧沥青路面,首先经过翻挖铣刨获得废旧沥青混合料,随后和新集料、新沥青(必要时还需添加再生剂)等材料重新拌和,形成具有一定路用性能的再生沥青混合料,再生后的沥青混合料可用于铺筑沥青路面的面层或基层。The implementation process of asphalt pavement regeneration technology is to firstly excavate and mill the old asphalt pavement that needs to be renovated or discarded to obtain waste asphalt mixture, and then combine it with new aggregates, new asphalt (need to add regenerant if necessary) and other materials. Re-mix to form a recycled asphalt mixture with certain road performance, and the regenerated asphalt mixture can be used for laying the surface layer or base layer of the asphalt pavement.
在所有的沥青路面再生技术中,厂拌热再生混合料在生产过程中,旧料首先经过破碎、筛分分档,其变异性得到有效的控制;其次热再生混合料的拌和过程类似于常规热拌混合料,在较高的拌和温度下进行,因此废旧沥青混合料中的旧沥青更容易和新沥青、再生剂发生融合,旧沥青的再生效果好。经过废旧沥青混合料预处理及精确计量、旧沥青再生、新集料及新沥青按需配置等多步骤控制,所生产的厂拌热再生混合料性能最优,且易于控制,混合料的均匀性好,适用范围最广,不仅可以被用于道路的中、下面层及基层,经过合理设计并检验的厂拌热再生混合料还可被用于道路的上面层。缺点是废旧沥青混合料需要运输至拌和厂,额外增加了粒料的转运费用,而且废旧沥青混合料的掺量较冷再生技术低,一般为10%-30%,成为抑制该技术广泛应用的瓶颈。但是2010年以来,随着法国超级再生技术的研究,80%以上,甚至100%再生掺量的技术已经应用于工程实践,因此本项目将工厂化、产业化、高效能热再生作为主要研究方向。Among all asphalt pavement recycling technologies, in the production process of factory-mixed hot recycled mixture, the old material is firstly crushed, screened and classified, and its variability is effectively controlled; secondly, the mixing process of hot recycled mixture is similar to conventional The hot mix is carried out at a higher mixing temperature, so the old asphalt in the waste asphalt mixture is easier to fuse with the new asphalt and rejuvenating agent, and the regeneration effect of the old asphalt is good. After multi-step control of waste asphalt mixture pretreatment and accurate metering, old asphalt regeneration, new aggregate and new asphalt configuration on demand, the produced factory-mixed hot recycled mixture has the best performance and is easy to control, and the uniformity of the mixture Well, it has the widest scope of application. It can not only be used in the middle and lower layers of the road and the base layer, but also can be used in the upper layer of the road after a reasonable design and inspection. The disadvantage is that the waste asphalt mixture needs to be transported to the mixing plant, which increases the transportation cost of the pellets, and the content of the waste asphalt mixture is lower than that of the cold recycling technology, generally 10%-30%, which has become an obstacle to the widespread application of this technology. bottleneck. However, since 2010, with the research of super regeneration technology in France, more than 80%, or even 100% of the regeneration dosage technology has been applied to engineering practice. Therefore, this project takes factoryization, industrialization, and high-efficiency thermal regeneration as the main research direction. .
国内外研究人员对再生混合料设计施工技术开展了大量的研究,并取得了相应的研究成果,但是由于研究者所采用试验材料、试验设备等的不同,造成研究结论不统一,甚至相互矛盾,同时由于不精细化的试验及设计方法,导致所设计的热再生混合料中旧料掺量低,旧料有效再生率低,所需添加新沥青或再生剂含量高,再生混合料质量不稳定,再生混合料路用性能差,降低了再生混合料的经济优势,严重影响热再生技术产业化、规模化的实施。本发明提供的一种高效再生沥青混合料及其制备工艺,能够突破再生材料分类、再生专用沥青、混合料设计、生产、施工装备匹配性等关键问题,实现铣刨料用量达到70%以上,再生混合料性能达到新料水平,单位造价低于新料的目标,从而推动公路废旧材料的产业化利用,提升废旧材料的再生利用效能,巩固江苏省公路建养水平在全国的领先地位,促进公路行业的高质量发展。Researchers at home and abroad have carried out a lot of research on the design and construction technology of recycled mixtures, and have achieved corresponding research results. However, due to the differences in the test materials and test equipment used by the researchers, the research conclusions are inconsistent and even contradict each other. At the same time, due to the unrefined test and design method, the designed thermal regeneration mixture has a low content of old materials, a low effective regeneration rate of the old materials, high content of new asphalt or regenerant to be added, and unstable quality of the recycled mixture. , The poor road performance of the recycled mixture reduces the economic advantage of the recycled mixture and seriously affects the industrialization and large-scale implementation of thermal regeneration technology. The invention provides a high-efficiency recycled asphalt mixture and a preparation process thereof, which can break through key problems such as classification of recycled materials, special recycled asphalt, mixture design, production, and matching of construction equipment, etc. The performance of the mixed material reaches the level of the new material, and the unit cost is lower than the target of the new material, so as to promote the industrialized utilization of road waste materials, improve the recycling efficiency of waste materials, consolidate the leading position of Jiangsu Province in the level of highway construction and maintenance in the country, and promote highway construction and maintenance. High-quality development of the industry.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种高再生率厂拌、生产成本低、混合料高低温及疲劳性能优异的热拌高效再生沥青混合料及其制备工艺。The purpose of the present invention is to provide a hot-mixed high-efficiency recycled asphalt mixture with high regeneration rate, low production cost, excellent high and low temperature and fatigue properties of the mixture and its preparation process.
为实现上述发明目的,本发明采用的具体技术方案是:In order to realize the above-mentioned purpose of the invention, the concrete technical scheme adopted in the present invention is:
一种高效再生沥青混合料,其特征在于,包含质量份为1.0~3.0份的再生专用沥青和100份的骨料;A high-efficiency recycled asphalt mixture is characterized in that it comprises 1.0 to 3.0 parts by mass of special recycled asphalt and 100 parts of aggregate;
所述的100份骨料包含以下质量份配比的原料:粒径为10mm~25mm的新集料0~30份,粒径为10mm~20mm的RAP料0~70份,粒径为5mm~10mm的RAP料0~80份,粒径为0mm~5mm的RAP料0~20份,矿粉0~3份。The 100 parts of aggregates include raw materials in the following proportions by mass: 0 to 30 parts of new aggregates with a particle size of 10mm to 25mm, 0 to 70 parts of RAP materials with a particle size of 10mm to 20mm, and a particle size of 5mm to 5mm. 0-80 parts of 10mm RAP material, 0-20 parts of RAP material with a particle size of 0mm-5mm, and 0-3 parts of mineral powder.
优选的,所述的新集料为粒径10~25mm石灰岩或玄武岩。Preferably, the new aggregate is limestone or basalt with a particle size of 10-25 mm.
所述再生专用沥青由基质沥青、含苯乙烯类改性剂、多链聚烯烃类改性剂、橡胶油、环烷基油再生剂、稳定剂组成:The regenerated special asphalt is composed of matrix asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic oil regenerant, and stabilizer:
所述的基质沥青、含苯乙烯类改性剂、多链聚烯烃类改性剂、橡胶油、环烷基油再生剂、稳定剂各组分质量百分比如下:The mass percentages of the components of the base asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic oil regenerant, and stabilizer are as follows:
Figure PCTCN2020114529-appb-000001
Figure PCTCN2020114529-appb-000001
所述的含苯乙烯类改性剂为苯乙烯-丁二烯-苯乙烯三嵌段共聚物SBS、丁苯橡胶SBR的一种或两种。The styrene-containing modifier is one or both of styrene-butadiene-styrene triblock copolymer SBS and styrene-butadiene rubber SBR.
所述的多链聚烯烃类改性剂为氧化聚乙烯蜡,其熔滴点为100~150℃、140℃黏度为200~5000cps、酸值为14~55mg KOH/g。The multi-chain polyolefin type modifier is oxidized polyethylene wax, the melting point is 100-150°C, the viscosity at 140°C is 200-5000cps, and the acid value is 14-55mg KOH/g.
所述的再生剂为环烷基油或芳香基油中的一种Described regenerant is a kind of in naphthenic oil or aromatic base oil
所述橡胶油为环烷基橡胶油和芳香基橡胶油中的一种。The rubber oil is one of naphthenic rubber oil and aromatic rubber oil.
所述稳定剂为单质硫、二芳基二硫化物、硝基取代二芳基二硫化物中的一种。The stabilizer is one of elemental sulfur, diaryl disulfide and nitro-substituted diaryl disulfide.
所述再生专用沥青的制备方法,包括以下步骤:The preparation method of the regenerated special asphalt comprises the following steps:
(1)在反应釜中将基质沥青加热至165~180℃,待到温度稳定后加入含苯乙烯类改性剂,搅拌0.5~1h至其均匀,将搅拌均匀的沥青通过胶体磨进行高速剪切,剪切功率为20~40t/h;剪切完毕后,搅拌0.5h~1h;然后加入多链聚烯烃类改性剂,继续搅拌0.5~1h;(1) Heat the base asphalt to 165-180°C in the reaction kettle, add styrene-containing modifier after the temperature is stable, stir for 0.5-1 h until it is uniform, and pass the uniformly stirred asphalt to high-speed shearing through a colloid mill. Cut, the shearing power is 20~40t/h; after the shearing is completed, stir for 0.5h~1h; then add the multi-chain polyolefin modifier, and continue to stir for 0.5~1h;
(2)向步骤(1)所得到的沥青中加入橡胶油,在170~180℃温度下搅拌0.5h~1h;然后缓慢加入稳定剂,搅拌2~3h后,在170~180℃温度下加入再生剂继续搅拌8h~24h,之后出料灌装,即得到产品。(2) Adding rubber oil to the asphalt obtained in step (1), stirring at 170-180°C for 0.5h-1h; then slowly adding stabilizer, stirring for 2-3h, then adding at 170-180°C The regenerant is continuously stirred for 8h to 24h, and then the material is discharged and filled to obtain the product.
本发明还提供一种高效再生沥青混合料制备工艺,其特征在于包括以下步骤:The present invention also provides a process for preparing high-efficiency regenerated asphalt mixture, which is characterized by comprising the following steps:
步骤一:RAP料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡,或20~10mmRAP集料、10~0mmRAP集料两档;Step 1: The RAP material is planed, milled and crushed, and divided into three grades: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate, or 20-10mm RAP aggregate and 10-0mm RAP aggregate;
步骤二:将新集料、矿粉在气加热法的第一烘干筒中加热;Step 2: heating the new aggregate and mineral powder in the first drying cylinder of the gas heating method;
步骤三:将三挡(或两档)RAP料在气加热法的第二烘干筒中加热;Step 3: Heat the third (or two) RAP material in the second drying cylinder of the gas heating method;
步骤四:经过计量后分别将新集料、矿粉、三挡(或两档)RAP料投入搅拌锅,搅拌均匀;Step 4: After measuring, put the new aggregate, mineral powder, and third-speed (or second-speed) RAP material into the mixing pot, and stir evenly;
步骤五,搅拌锅中加入再生专用沥青搅拌均匀后得到高效再生沥青混合料。Step 5, adding recycled special asphalt into the mixing pot and stirring evenly to obtain a high-efficiency recycled asphalt mixture.
进一步的,所述的步骤一中的刨铣破碎方式为铣刨机+破碎筛分。Further, the planing, milling and crushing method in the step 1 is a milling machine + crushing and screening.
进一步的,所述的步骤二中第一烘干筒中的加热方式为新集料在原有搅拌设备的烘干筒中加热,将干燥的热气导入干燥筒,在干燥筒内实现集料与气体的对流;在干燥筒的另一端有一个引风机,将加热后的气体抽回热发生器,有利于热能再利用。Further, in the step 2, the heating method in the first drying cylinder is that the new aggregate is heated in the drying cylinder of the original stirring device, and the dried hot air is introduced into the drying cylinder, and the convection between the aggregate and the gas is realized in the drying cylinder. ; There is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator, which is conducive to the reuse of heat energy.
进一步的,所述的步骤二中第一烘干筒中的加热温度为170℃~185℃。Further, in the second step, the heating temperature in the first drying cylinder is 170°C to 185°C.
进一步的,所述的步骤三中第二烘干筒中的加热方式为采用顺流式加热方式,将干燥的热气导入旧沥青混合料干燥筒,在干燥筒内实现混合料与气体的对流;在干燥筒的另一端有一个引风机,将加热后的气体抽回热发生器。该回收气体可能带有“蓝烟”和加热产生的水蒸汽。因此,在进入热气发生器之前,将水蒸汽分离掉,以保证气体的干燥,同时将产生的“蓝烟”通过再加热燃烧掉,既可防止污染,又可产生热能。Further, the heating method in the second drying cylinder in the third step is to adopt a downstream heating method, and the dried hot air is introduced into the old asphalt mixture drying cylinder, and the convection of the mixture and the gas is realized in the drying cylinder; There is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator. The recovered gas may have "blue smoke" and water vapor from heating. Therefore, before entering the hot gas generator, the water vapor is separated to ensure the drying of the gas, and the "blue smoke" produced is burned by reheating, which can not only prevent pollution, but also generate heat energy.
进一步的,所述的步骤三中第二烘干筒中的加热温度为120℃~140℃。Further, in the third step, the heating temperature in the second drying cylinder is 120°C to 140°C.
进一步的,所述的步骤四中的搅拌设备采用间歇式强制搅拌设备。Further, the stirring equipment in the step 4 adopts intermittent forced stirring equipment.
进一步的,所述的步骤四中的搅拌设备为加热型搅拌设备,使得再生混合料能均匀地达到出料温度。Further, the stirring device in the fourth step is a heating-type stirring device, so that the regenerated mixture can reach the discharge temperature uniformly.
进一步的,所述的步骤五中的再生专用沥青温度为165℃~180℃。Further, the temperature of the recycled special asphalt in the step 5 is 165°C to 180°C.
进一步的,所述的步骤五中的搅拌温度为130℃~150℃。Further, the stirring temperature in the fifth step is 130°C to 150°C.
本发明提供的一种高效再生沥青混合料及其制备工艺具有以下有益效果:A high-efficiency regenerated asphalt mixture and a preparation process thereof provided by the present invention have the following beneficial effects:
本发明提供的高效再生沥青混合料使用的沥青是自主开发的再生专用胶结料,里面包含多链聚烯烃类改性剂和环烷基油再生剂能够显著提高沥青的高低温性能和再生性能。多链聚烯烃类改性剂与SBS共聚物能够结合成新的接枝共聚物,这种共聚物的极性很高,能与沥青形成分相不分离的均匀结构,有效地改善沥青的稳定性、高温流变性和温度敏感性。本发明使用的环烷基油再生剂相容性好,对不溶性硫化物有很好的分散性,其对于沥青组分的调和再生性能显著。并且其稳定性好,无污染、无毒,能够减少使用过程中的环境污染,提高对环境的保护。The asphalt used in the high-efficiency regenerated asphalt mixture provided by the present invention is a self-developed special cementing material for regeneration, which contains a multi-chain polyolefin modifier and a naphthenic oil regenerating agent, which can significantly improve the high and low temperature performance and regeneration performance of the asphalt. The multi-chain polyolefin modifier and SBS copolymer can be combined into a new graft copolymer. This copolymer has high polarity and can form a uniform structure with no phase separation from the asphalt, effectively improving the stability of the asphalt. properties, high temperature rheology and temperature sensitivity. The naphthenic oil regenerant used in the present invention has good compatibility, has good dispersibility for insoluble sulfides, and has remarkable reconciliation and regeneration performance for asphalt components. And it has good stability, no pollution and no toxicity, which can reduce environmental pollution during use and improve the protection of the environment.
其次本发明提供的高效再生沥青混合料针对现有再生混合料设计中先体积设计、后混合料性能验证的弊病,通过综合美国基于性能平衡的沥青混合料设计方法(BMD)和法国高模量沥青混合料设计方法(LPC),形成基于性能平衡的再生沥青混合料制备方法。配比设计中,再生沥青混合料的级配调节自由,即使是空隙率极小的密集配混合料,由于再生专用沥青的作用,也能够保证其高温性能。本发明综合了法国高模量沥青混合料设计方法(LPC)和美国基于性能平衡的沥青混合料设计方法(BMD),为再生沥青混合料抗疲劳性能及低温性能的协同提升争取更大的空间,充分保障再生混合料整体性能的全面提升。Secondly, the high-efficiency recycled asphalt mixture provided by the present invention aims at the disadvantages of the existing recycled mixture design, which is the first volume design and then the mixture performance verification. The Asphalt Mixture Design Method (LPC), which forms a performance balance-based method for the preparation of recycled asphalt mixtures. In the proportioning design, the gradation of the recycled asphalt mixture can be adjusted freely. Even the densely mixed mixture with extremely small porosity can ensure its high temperature performance due to the effect of the recycled special asphalt. The invention integrates the French high-modulus asphalt mixture design method (LPC) and the American asphalt mixture design method based on performance balance (BMD), and strives for more space for the synergistic improvement of the fatigue resistance and low temperature performance of the recycled asphalt mixture , fully guarantee the overall improvement of the overall performance of the recycled mixture.
具体实施方式detailed description
下面,通过具体实施例对本发明的技术方案进行详细说明。Hereinafter, the technical solutions of the present invention will be described in detail through specific embodiments.
实施例1Example 1
高效再生沥青混合料,按重量份计包括:再生专用沥青2份,粒径为10mm~20mm的新集料20份,粒径为10mm~20mm的RAP料45份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份。High-efficiency recycled asphalt mixture, including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 45 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material and 5 parts of RAP material with a particle size of 0 mm to 5 mm.
所述的高效再生沥青混合料为SMA-13型沥青混合料。The high-efficiency recycled asphalt mixture is SMA-13 type asphalt mixture.
所述的高效再生沥青混合料中添加的新集料为粒径为10mm~20mm的玄武岩。The new aggregate added to the high-efficiency regenerated asphalt mixture is basalt with a particle size of 10 mm to 20 mm.
所述的高效再生沥青混合料中添加的RAP料为铣刨回收的SMA-13废旧沥青混合料。The RAP material added to the high-efficiency recycled asphalt mixture is the SMA-13 waste asphalt mixture recovered by milling.
高效再生沥青混合料的制备方法,其特征在于,具体包括以下步骤:The preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
步骤一:将SMA-13废旧沥青混合料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡;Step 1: Planing, milling and crushing the SMA-13 waste asphalt mixture into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
步骤二:将10mm~20mm的新集料20份在气加热法的第一烘干筒中加热,加热温度为170℃;Step 2: heating 20 parts of new aggregates of 10mm to 20mm in the first drying cylinder of the gas heating method, and the heating temperature is 170°C;
步骤三:将粒径为10mm~20mm的RAP料45份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份三挡RAP料在气加热法的第二烘干筒中加热,加热温度为130℃;Step 3: Put 45 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 130 ℃;
步骤四:将新集料、三挡RAP料投入搅拌锅,搅拌均匀;Step 4: Put the new aggregate and the third-speed RAP material into the mixing pot and stir evenly;
步骤五,搅拌锅中加入175℃再生专用沥青搅拌均匀后得到高效再生沥青混合料1#,搅拌温度140℃。Step 5: Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 1#, and the stirring temperature is 140°C.
取高效再生沥青混合料1#进行稳定度、流值、动稳定度和低温小梁测定,检测结果见表1。Take the high-efficiency recycled asphalt mixture 1# to measure the stability, flow value, dynamic stability and low temperature trabecular. The test results are shown in Table 1.
表1 1#高效再生沥青混合料检测结果Table 1 Test results of 1# high-efficiency recycled asphalt mixture
Figure PCTCN2020114529-appb-000002
Figure PCTCN2020114529-appb-000002
表1检测结果表明,1#再生沥青混合料的高温性能优异,稳定度由7.8kN提升至12.54kN,动稳定度由4238次/mm提升至9545次/mm。低温方面基本恢复混合料的低温抗裂性能,低温最大弯拉应变由1972με提升至2299με。高低温性能的提升说明1#再生沥青混合料再生效果良好。The test results in Table 1 show that the high temperature performance of 1# recycled asphalt mixture is excellent, the stability is increased from 7.8kN to 12.54kN, and the dynamic stability is increased from 4238 times/mm to 9545 times/mm. In terms of low temperature, the low temperature crack resistance of the mixture is basically restored, and the maximum bending and tensile strain at low temperature is increased from 1972 με to 2299 με. The improvement of high and low temperature performance shows that the regeneration effect of 1# recycled asphalt mixture is good.
实施例2Example 2
高效再生沥青混合料,按重量份计包括:再生专用沥青2.2份,粒径为10mm~20mm的RAP料60份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料10份。The high-efficiency recycled asphalt mixture includes, in parts by weight: 2.2 parts of recycled special asphalt, 60 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and RAP with a particle size of 0mm to 5mm 10 servings.
所述的高效再生沥青混合料为AC-20型全再生沥青混合料。The high-efficiency regenerated asphalt mixture is AC-20 type fully regenerated asphalt mixture.
所述的高效再生沥青混合料中添加的RAP料为铣刨回收的AC-20型废旧沥青混合料。The RAP material added to the high-efficiency recycled asphalt mixture is the AC-20 type waste asphalt mixture recovered by milling.
高效再生沥青混合料的制备方法,其特征在于,具体包括以下步骤:The preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
步骤一:将AC-20废旧沥青混合料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡;Step 1: Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
步骤二:将粒径为10mm~20mm的RAP料45份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份三挡RAP料在气加热法的第二烘干筒中加热,加热温度为140℃;Step 2: put 45 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 ℃;
步骤三:将三挡RAP料投入搅拌锅,搅拌均匀;Step 3: Put the third gear RAP material into the mixing pot and stir evenly;
步骤五,搅拌锅中加入175℃再生专用沥青搅拌均匀后得到高效再生沥青混合料2#,搅拌温度140℃。Step 5: Add 175°C regenerated special asphalt into the mixing pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 2#, and the stirring temperature is 140°C.
取高效再生沥青混合料2#进行稳定度、流值、动稳定度和低温小梁测定,检测结果见表2。Take the high-efficiency recycled asphalt mixture 2# to measure the stability, flow value, dynamic stability and low temperature trabecular. The test results are shown in Table 2.
表2 2#高效再生沥青混合料检测结果Table 2 Test results of 2# high-efficiency recycled asphalt mixture
Figure PCTCN2020114529-appb-000003
Figure PCTCN2020114529-appb-000003
表2检测结果表明,2#再生沥青混合料的高温性能均有所提升,稳定度由5.6kN提升至8.72kN,动稳定度由4500次/mm提升至6387次/mm。低温方面略有提升,低温最大弯拉应变由1412με提升至1514με。本次实施的2#再生沥青混合料为全再生沥青混合料,其再生效果略有提升。The test results in Table 2 show that the high temperature performance of the 2# recycled asphalt mixture has been improved, the stability has increased from 5.6kN to 8.72kN, and the dynamic stability has increased from 4500 times/mm to 6387 times/mm. The low temperature is slightly improved, and the maximum bending and tensile strain at low temperature is increased from 1412με to 1514με. The 2# recycled asphalt mixture implemented this time is a fully recycled asphalt mixture, and its regeneration effect is slightly improved.
实施例3Example 3
高效再生沥青混合料,按重量份计包括:再生专用沥青2份,粒径为10mm~20mm的新集料20份,粒径为10mm~20mm的RAP料45份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份。High-efficiency recycled asphalt mixture, including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 45 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material and 5 parts of RAP material with a particle size of 0 mm to 5 mm.
所述的高效再生沥青混合料为AC-20型沥青混合料。The high-efficiency regenerated asphalt mixture is AC-20 type asphalt mixture.
所述的高效再生沥青混合料中添加的新集料为粒径为10mm~20mm的石灰岩。The new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10 mm to 20 mm.
所述的高效再生沥青混合料中添加的RAP料为铣刨回收的AC-20废旧沥青混合料。The RAP material added to the high-efficiency recycled asphalt mixture is AC-20 waste and old asphalt mixture recovered by milling.
高效再生沥青混合料的制备方法,其特征在于,具体包括以下步骤:The preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
步骤一:将AC-20废旧沥青混合料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡;Step 1: Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
步骤二:将10mm~20mm的新集料20份在气加热法的第一烘干筒中加热,加热温度为170℃;Step 2: heating 20 parts of new aggregates of 10mm to 20mm in the first drying cylinder of the gas heating method, and the heating temperature is 170°C;
步骤三:将粒径为10mm~20mm的RAP料45份,粒径为5mm~10mm的RAP料30份, 粒径为0mm~5mm的RAP料5份三挡RAP料在气加热法的第二烘干筒中加热,加热温度为140℃;Step 3: Put 45 parts of RAP material with a particle size of 10mm-20mm, 30 parts of RAP material with a particle size of 5mm-10mm, and 5 parts of RAP material with a particle size of 0mm-5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 ℃;
步骤四:将新集料、三挡RAP料投入搅拌锅,搅拌均匀;Step 4: Put the new aggregate and the third-speed RAP material into the mixing pot and stir evenly;
步骤五,搅拌锅中加入175℃再生专用沥青搅拌均匀后得到高效再生沥青混合料3#,搅拌温度140℃。Step 5: Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 3#, and the stirring temperature is 140°C.
取高效再生沥青混合料3#进行稳定度、流值、动稳定度和低温小梁测定,检测结果见表3。Take high-efficiency recycled asphalt mixture 3# to measure the stability, flow value, dynamic stability and low temperature trabecular. The test results are shown in Table 3.
表3 3#高效再生沥青混合料检测结果Table 3 Test results of 3# high-efficiency recycled asphalt mixture
检测项目Test items 单位unit 高效再生混合料3#检测结果High-efficiency recycled mixture 3# test results 原AC路面检测结果Original AC road test results
稳定度stability kNkN 8.438.43 5.605.60
流值flow value 0.1mm0.1mm 45.245.2 44.544.5
低温最大弯拉应变Maximum bending strain at low temperature μεμε 18871887 14121412
动稳定度Dynamic stability 次/mmtimes/mm 87508750 45004500
表3检测结果表明,3#再生沥青混合料的高温性能优异,稳定度由5.6kN提升至8.43kN,动稳定度由4500次/mm提升至8750次/mm。低温方面基本恢复混合料的低温抗裂性能,低温最大弯拉应变由1412με提升至1887με。高低温性能的提升说明3#再生沥青混合料再生效果良好。The test results in Table 3 show that the 3# recycled asphalt mixture has excellent high temperature performance, the stability is increased from 5.6kN to 8.43kN, and the dynamic stability is increased from 4500 times/mm to 8750 times/mm. In terms of low temperature, the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412 με to 1887 με. The improvement of high and low temperature performance shows that the regeneration effect of 3# recycled asphalt mixture is good.
实施例4Example 4
高效再生沥青混合料,按重量份计包括:再生专用沥青2份,粒径为10mm~20mm的新集料20份,粒径为10mm~20mm的RAP料44份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份,矿粉1份。High-efficiency recycled asphalt mixture, including by weight: 2 parts of recycled special asphalt, 20 parts of new aggregates with a particle size of 10mm to 20mm, 44 parts of RAP material with a particle size of 10mm to 20mm, and a particle size of 5mm to 10mm. 30 parts of RAP material, 5 parts of RAP material with a particle size of 0mm to 5mm, and 1 part of mineral powder.
所述的高效再生沥青混合料为AC-20型沥青混合料。The high-efficiency recycled asphalt mixture is AC-20 type asphalt mixture.
所述的高效再生沥青混合料中添加的新集料为粒径为10mm~20mm的石灰岩。The new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10 mm to 20 mm.
所述的高效再生沥青混合料中添加的RAP料为铣刨回收的AC-20废旧沥青混合料。The RAP material added to the high-efficiency recycled asphalt mixture is AC-20 waste and old asphalt mixture recovered by milling.
高效再生沥青混合料的制备方法,其特征在于,具体包括以下步骤:The preparation method of high-efficiency recycled asphalt mixture is characterized in that, specifically comprises the following steps:
步骤一:将AC-20废旧沥青混合料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡;Step 1: Plan, mill and crush the AC-20 waste asphalt mixture, and divide it into three blocks: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate;
步骤二:将10mm~20mm的新集料20份和矿粉1份在气加热法的第一烘干筒中加热,加热温度为170℃;Step 2: heating 20 parts of 10mm-20mm new aggregate and 1 part of mineral powder in the first drying cylinder of the gas heating method, and the heating temperature is 170 ° C;
步骤三:将粒径为10mm~20mm的RAP料44份,粒径为5mm~10mm的RAP料30份,粒径为0mm~5mm的RAP料5份三挡RAP料在气加热法的第二烘干筒中加热,加热温度为140℃;Step 3: Put 44 parts of RAP material with a particle size of 10mm to 20mm, 30 parts of RAP material with a particle size of 5mm to 10mm, and 5 parts of RAP material with a particle size of 0mm to 5mm in the second stage of the gas heating method. Heating in the drying cylinder, the heating temperature is 140 ℃;
步骤四:将新集料、矿粉、三挡RAP料投入搅拌锅,搅拌均匀;Step 4: Put the new aggregate, mineral powder and RAP material in the third gear into the mixing pot and stir evenly;
步骤五,搅拌锅中加入175℃再生专用沥青搅拌均匀后得到高效再生沥青混合料4#,搅拌温度140℃。Step 5: Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency recycled asphalt mixture 4#, and the stirring temperature is 140°C.
取高效再生沥青混合料4#进行稳定度、流值、动稳定度和低温小梁测定,检测结果见表4。Take the high-efficiency recycled asphalt mixture 4# to measure the stability, flow value, dynamic stability and low temperature trabecular. The test results are shown in Table 4.
表4 4#高效再生沥青混合料检测结果Table 4 Test results of 4# high-efficiency recycled asphalt mixture
检测项目Test items 单位unit 高效再生混合料4#检测结果High-efficiency recycled mixture 4# test results 原AC路面检测结果Original AC road test results
稳定度stability kNkN 8.558.55 5.605.60
流值flow value 0.1mm0.1mm 23.423.4 44.544.5
低温最大弯拉应变Maximum bending strain at low temperature μεμε 18211821 14121412
动稳定度Dynamic stability 次/mmtimes/mm 98449844 45004500
表4检测结果表明,4#再生沥青混合料的高温性能优异,稳定度由5.6kN提升至8.55kN,动稳定度由4500次/mm提升至9844次/mm。低温方面基本恢复混合料的低温抗裂性能,低温最大弯拉应变由1412με提升至1821με。高低温性能的提升说明4#再生沥青混合料再生效果良好。The test results in Table 4 show that the high temperature performance of 4# recycled asphalt mixture is excellent, the stability is increased from 5.6kN to 8.55kN, and the dynamic stability is increased from 4500 times/mm to 9844 times/mm. In terms of low temperature, the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412 με to 1821 με. The improvement of high and low temperature performance shows that the regeneration effect of 4# recycled asphalt mixture is good.
实施例5Example 5
高效再生沥青混合料,按重量份计包括:再生专用沥青2份,粒径为10mm~15mm的新集料25份,粒径为10mm~20mm的RAP料22份,粒径为0mm~10mm的RAP料53份。High-efficiency recycled asphalt mixture, including by weight: 2 parts of recycled special asphalt, 25 parts of new aggregate with particle size of 10mm-15mm, 22 parts of RAP material with particle size of 10mm-20mm, particle size of 0mm-10mm 53 servings of RAP material.
所述的高效再生沥青混合料为AC-13型沥青混合料。The high-efficiency recycled asphalt mixture is AC-13 type asphalt mixture.
所述的高效再生沥青混合料中添加的新集料为粒径为10mm~15mm的石灰岩。The new aggregate added to the high-efficiency regenerated asphalt mixture is limestone with a particle size of 10mm-15mm.
所述的高效再生沥青混合料中添加的RAP料为铣刨回收的AC-13废旧沥青混合料。The RAP material added to the high-efficiency recycled asphalt mixture is AC-13 waste and old asphalt mixture recovered by milling.
高效再生沥青混合料的制备方法,其特征在于,具体包括以下步骤:The preparation method of high-efficiency regenerated asphalt mixture is characterized in that, specifically comprises the following steps:
步骤一:将AC-13废旧沥青混合料进行刨铣破碎,分为20~10mmRAP集料、10~0mmRAP集料两挡;Step 1: Plan, mill and crush the AC-13 waste asphalt mixture, and divide it into two blocks of 20-10mm RAP aggregate and 10-0mm RAP aggregate;
步骤二:将10mm~15mm的新集料25份在气加热法的第一烘干筒中加热,加热温度为180℃;Step 2: heating 25 parts of new aggregates of 10mm to 15mm in the first drying cylinder of the gas heating method, and the heating temperature is 180°C;
步骤三:将粒径为10mm~20mm的RAP料22份,粒径为0mm~10mm的RAP料53份两挡RAP料在气加热法的第二烘干筒中加热,加热温度为135℃;Step 3: heating 22 parts of RAP material with a particle size of 10mm to 20mm and 53 parts of RAP material with a particle size of 0mm to 10mm in the second drying cylinder of the gas heating method, and the heating temperature is 135 ° C;
步骤四:将新集料、两挡RAP料投入搅拌锅,搅拌均匀;Step 4: Put the new aggregate and RAP material in two blocks into the mixing pot and stir evenly;
步骤五,搅拌锅中加入175℃再生专用沥青搅拌均匀后得到高效再生沥青混合料5#,搅拌温度140℃。Step 5: Add 175°C regenerated special asphalt into the stirring pot and stir evenly to obtain high-efficiency regenerated asphalt mixture 5#, and the stirring temperature is 140°C.
取高效再生沥青混合料5#进行稳定度、流值、动稳定度和低温小梁测定,检测结果见表5。Take high-efficiency recycled asphalt mixture 5# for stability, flow value, dynamic stability and low-temperature trabecular measurement. The test results are shown in Table 5.
表5 5#高效再生沥青混合料检测结果Table 5 Test results of 5# high-efficiency recycled asphalt mixture
检测项目Test items 单位unit 高效再生混合料5#检测结果High-efficiency recycled mixture 5# test results 原AC路面检测结果Original AC road test results
稳定度stability kNkN 10.5110.51 5.605.60
流值flow value 0.1mm0.1mm 37.637.6 44.544.5
低温最大弯拉应变Maximum bending strain at low temperature μεμε 24052405 14121412
动稳定度Dynamic stability 次/mmtimes/mm 60586058 45004500
表5检测结果表明,5#再生沥青混合料的高温性能优异,稳定度由5.6kN提升至10.51kN,动稳定度由4500次/mm提升至6058次/mm。低温方面基本恢复混合料的低温抗裂性能,低温最大弯拉应变由1412με提升至2405με。高低温性能的提升说明5#再生沥青混合料再生效 果良好。The test results in Table 5 show that the 5# recycled asphalt mixture has excellent high temperature performance, the stability is increased from 5.6kN to 10.51kN, and the dynamic stability is increased from 4500 times/mm to 6058 times/mm. In terms of low temperature, the low temperature crack resistance of the mixture is basically restored, and the maximum flexural tensile strain at low temperature is increased from 1412με to 2405με. The improvement of high and low temperature performance shows that the regeneration effect of 5# recycled asphalt mixture is good.
采用以上所述,仅为本发明比较理想的实施方案,但本发明的适用范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭示的技术范围内,根据本发明的技术方案构思,加以同等的替换和改变,都应涵盖在本发明的保护范围内。The above description is only an ideal embodiment of the present invention, but the scope of application of the present invention is not limited to this. Concepts, equivalent replacements and changes should be included within the protection scope of the present invention.

Claims (13)

  1. 一种高效再生沥青混合料,其特征在于,所述高效再生沥青混合料包含质量份为1.0~3.0份的再生专用沥青和100份的骨料;A high-efficiency recycled asphalt mixture, characterized in that the high-efficiency recycled asphalt mixture comprises 1.0 to 3.0 parts by mass of special recycled asphalt and 100 parts of aggregate;
    所述的100份骨料包含以下质量份配比的原料:粒径为10mm~25mm的新集料0~30份,粒径为10mm~20mm的RAP料0~70份,粒径为5mm~10mm的RAP料0~80份,粒径为0mm~5mm的RAP料0~20份,矿粉0~3份。The 100 parts of aggregates include raw materials in the following proportions by mass: 0 to 30 parts of new aggregates with a particle size of 10mm to 25mm, 0 to 70 parts of RAP materials with a particle size of 10mm to 20mm, and a particle size of 5mm to 5mm. 0-80 parts of 10mm RAP material, 0-20 parts of RAP material with a particle size of 0mm-5mm, and 0-3 parts of mineral powder.
  2. 根据权利要求1所述的一种高效再生沥青混合料,其特征在于,所述再生专用沥青由基质沥青、含苯乙烯类改性剂、多链聚烯烃类改性剂、橡胶油、环烷基油再生剂、稳定剂组成:The high-efficiency regenerated asphalt mixture according to claim 1, wherein the regenerated special asphalt is composed of matrix asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic Composition of base oil regenerant and stabilizer:
    所述的基质沥青、含苯乙烯类改性剂、多链聚烯烃类改性剂、橡胶油、环烷基油再生剂、稳定剂各组分质量百分比如下:The mass percentages of the components of the base asphalt, styrene-containing modifier, multi-chain polyolefin modifier, rubber oil, naphthenic oil regenerant, and stabilizer are as follows:
    Figure PCTCN2020114529-appb-100001
    Figure PCTCN2020114529-appb-100001
  3. 根据权利要求1所述的一种高效再生沥青混合料,其特征在于:所述的新集料为粒径10~25mm石灰岩或玄武岩。The high-efficiency recycled asphalt mixture according to claim 1, wherein the new aggregate is limestone or basalt with a particle size of 10-25 mm.
  4. 一种高效再生沥青混合料制备工艺,其特征在于,所述制备工艺包括以下步骤:A preparation process for high-efficiency regenerated asphalt mixture, characterized in that, the preparation process comprises the following steps:
    步骤一:RAP料进行刨铣破碎,分为20~10mmRAP集料、10~5mmRAP集料、小于5mmRAP集料三挡,或20~10mmRAP集料、10~0mmRAP集料两档;Step 1: The RAP material is planed, milled and crushed, and divided into three grades: 20-10mm RAP aggregate, 10-5mm RAP aggregate, and less than 5mm RAP aggregate, or 20-10mm RAP aggregate and 10-0mm RAP aggregate;
    步骤二:将新集料、矿粉在气加热法的第一烘干筒中加热;Step 2: heating the new aggregate and mineral powder in the first drying cylinder of the gas heating method;
    步骤三:将三挡(或两档)RAP料在气加热法的第二烘干筒中加热;Step 3: Heat the third (or two) RAP material in the second drying cylinder of the gas heating method;
    步骤四:经过计量后分别将新集料、矿粉、三挡(或两档)RAP料投入搅拌锅,搅拌均匀;Step 4: After measuring, put the new aggregate, mineral powder, and third-speed (or second-speed) RAP material into the mixing pot, and stir evenly;
    步骤五,搅拌锅中加入再生专用沥青搅拌均匀后得到高效再生沥青混合料。Step 5, adding recycled special asphalt into the mixing pot and stirring evenly to obtain a high-efficiency recycled asphalt mixture.
  5. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤一中的刨铣破碎方式为耙松+破碎筛分和铣刨机+破碎筛分中的一种。The preparation process of a kind of high-efficiency regenerated asphalt mixture according to claim 4, it is characterized in that: the planing, milling and crushing method in the step 1 is raking+crushing and screening and milling machine+crushing and screening. A sort of.
  6. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤二中第一烘干筒中的加热方式为新集料在原有搅拌设备的烘干筒中加热,将干燥的热气导入干燥筒,在干燥筒内实现集料与气体的对流;在干燥筒的另一端有一个引风机,将加热后的气体抽回热发生器,有利于热能再利用。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, characterized in that: in the step 2, the heating method in the first drying cylinder is that the new aggregate is heated in the drying cylinder of the original stirring equipment, The dry hot air is introduced into the drying cylinder, and the convection between the aggregate and the gas is realized in the drying cylinder; there is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator, which is conducive to the reuse of heat energy.
  7. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤二中第一烘干筒中的加热温度为170℃~185℃。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, wherein the heating temperature in the first drying cylinder in the second step is 170°C to 185°C.
  8. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤三中第二烘干筒中的加热方式为采用顺流式加热方式,将干燥的热气导入旧沥青混合料干燥筒,在干燥筒内实现混合料与气体的对流;在干燥筒的另一端有一个引风机,将加热后的气体抽回热发生器。该回收气体可能带有“蓝烟”和加热产生的水蒸汽。因此,在进入热气 发生器之前,将水蒸汽分离掉,以保证气体的干燥,同时将产生的“蓝烟”通过再加热燃烧掉,既可防止污染,又可产生热能。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, wherein the heating method in the second drying cylinder in the third step is to adopt a downstream heating method, and the dry hot air is introduced into the old The asphalt mixture drying cylinder realizes the convection between the mixture and the gas in the drying cylinder; there is an induced draft fan at the other end of the drying cylinder, which draws the heated gas back to the heat generator. The recovered gas may have "blue smoke" and water vapor from heating. Therefore, before entering the hot gas generator, the water vapor is separated to ensure the drying of the gas, and at the same time, the "blue smoke" produced is burned off by reheating, which can not only prevent pollution, but also generate heat energy.
  9. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤三中第二烘干筒中的加热温度为120℃~140℃。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, wherein the heating temperature in the second drying cylinder in the third step is 120°C to 140°C.
  10. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤四中的搅拌设备采用间歇式强制搅拌设备。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, characterized in that: the stirring equipment in the step 4 adopts intermittent forced stirring equipment.
  11. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤四中的搅拌设备为加热型搅拌设备,使得再生混合料能均匀地达到出料温度。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, characterized in that: the stirring equipment in the step 4 is a heating type stirring equipment, so that the regenerated mixture can reach the discharge temperature uniformly.
  12. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤五中的再生专用沥青温度为165℃~180℃。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, wherein the temperature of the regenerated special asphalt in the step 5 is 165°C to 180°C.
  13. 根据权利要求4所述的一种高效再生沥青混合料的制备工艺,其特征在于:所述的步骤五中的搅拌温度为130℃~150℃。The preparation process of a high-efficiency regenerated asphalt mixture according to claim 4, wherein the stirring temperature in the step 5 is 130°C to 150°C.
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CN115594440A (en) * 2022-09-14 2023-01-13 华北水利水电大学(Cn) Polyurethane modified cold-recycling mixture and preparation method thereof
CN115849766A (en) * 2022-09-23 2023-03-28 保利长大工程有限公司 Processing technology of mixing ratio of regenerant in hot mix plant recycled asphalt
CN116283066B (en) * 2023-01-06 2023-12-26 黑龙江大学 High-performance asphalt mixture prepared from chicken graphite tailings in AC-16 grading manner and preparation method of asphalt mixture
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