CN104191319A - Method for grinding surfaces of boride ceramic materials - Google Patents
Method for grinding surfaces of boride ceramic materials Download PDFInfo
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- CN104191319A CN104191319A CN201410443022.5A CN201410443022A CN104191319A CN 104191319 A CN104191319 A CN 104191319A CN 201410443022 A CN201410443022 A CN 201410443022A CN 104191319 A CN104191319 A CN 104191319A
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- borides
- grinding
- surfacing
- polishing machine
- cleaning
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B1/00—Processes of grinding or polishing; Use of auxiliary equipment in connection with such processes
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Grinding And Polishing Of Tertiary Curved Surfaces And Surfaces With Complex Shapes (AREA)
- Ceramic Products (AREA)
Abstract
The invention provides a method for grinding surfaces of boride ceramic materials, and relates to a method for grinding the boride ceramic materials. The method aims to solve the problem that a traditional method for grinding the boride ceramic materials is low in grinding efficiency. The method includes the steps that (1) ultrasonic cleaning is conducted, and the cleaned boride ceramic materials are obtained; (2) surface heating and oxidization are conducted, and the boride ceramic materials obtained after surface oxidization is conducted are obtained; (3) grinding treatment is conducted on the boride ceramic materials obtained after surface oxidization is conducted through a polishing machine, and surface grinding of the boride ceramic materials is achieved. The method has the advantages that the grinding processing efficiency is improved by 50% to 300%, and the grinding material consumption is reduced by 20% to 60%. The method is mainly applied to surface grinding of the boride ceramic materials.
Description
Technical field
The present invention relates to a kind of method for grinding of borides.
Background technology
Along with the continuous lifting of aircraft performance, the crucial hot spot of aircraft also needs to meet the strict demand of aircraft to thermal protection system structural intergrity in can being competent at extreme Aerodynamic Heating environment military service, and this has proposed stern challenge to thermally protective materials.Superhigh temperature ceramic material is regarded as the very promising non-ablative-type protective coating structural material of one, and with ZrB
2, HfB
2for the borides of representative is superhigh temperature ceramic material main direction of studying.Borides has high fusing point, higher elevated temperature strength, excellent anti-oxidant ablation property and resist chemical performance.Due to its outstanding combination property, this year, borides was subject to extensive concern, and had obtained significant achievement in research.
The same with other ceramic materials, the intrinsic fragility of borides makes its effects on surface defect extremely responsive, and the blemish of reduced size can cause the strength of materials significantly to decline.And borides and structural member preparation, processing process in inevitably introduce a large amount of defects on surface, therefore very necessary to processing after material surface carry out grinding, polishing.But that the higher hardness (>20GPa) of borides makes that grinding is carried out in its surface is very difficult, abrasive material, equipment, grinding parameter are also proposed to higher requirement.Surfacing has become one of principal element of restriction borides extensive use.
The method for grinding of traditional borides is by utilizing the abrasive material higher than ceramic material hardness to realize the process of material surface friction, extruding, cutting, reaching the object that reduces material surface roughness.Whole grinding process is a pure mechanical process, and grinding efficiency is low.
Summary of the invention
There is the problem that grinding efficiency is low in the method for grinding that the present invention seeks to solve traditional borides, and a kind of method of borides surfacing is provided.
A method for borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking absolute ethyl alcohol as cleaning agent, borides is carried out to ultrasonic cleaning 5min～60min, obtain cleaning rear borides;
Two, surface heating oxidation: borides after cleaning is placed in to Muffle furnace, be heated to 400～1500 DEG C from room temperature, and be heating and thermal insulation 1min～120min at 400～1500 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine; taking abrasive material as diamond particles or boron carbide particles, grinding medium under 100 turn/min～1000 turn/min conditions, carry out grinding processing as water, polishing machine dish rotating speed, realize borides surfacing.
Advantage of the present invention: the method for grinding of traditional borides is by utilizing the abrasive material higher than ceramic material hardness to realize the process of material surface friction, extruding, cutting, reaching the object that reduces material surface roughness.Whole grinding process is a pure mechanical process, and grinding efficiency is low.The invention provides a kind of borides surface rapid stock-removal method, boride ceramics is placed under aerobic hot environment, utilize the chemical reaction at material surface place significantly to change surface component, pattern and basic materialization character thereof, the modification that realizes material surface by oxidation can improve the grindability of hard borides ceramic material greatly.Borides surfacing method of the present invention is compared with traditional surfacing method, and grinding speed has improved 50%～300%, reduces abrasive consumption 20%～60%.
Brief description of the drawings
Fig. 1 is that test one obtains ZrB
2-SiC ceramic material surfaces shape appearance figure.
Detailed description of the invention
Detailed description of the invention one: present embodiment is a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking absolute ethyl alcohol as cleaning agent, borides is carried out to ultrasonic cleaning 5min～60min, obtain cleaning rear borides;
Two, surface heating oxidation: borides after cleaning is placed in to Muffle furnace, be heated to 400～1500 DEG C from room temperature, and be heating and thermal insulation 1min～120min at 400～1500 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine; taking abrasive material as diamond particles or boron carbide particles, grinding medium under 100 turn/min～1000 turn/min conditions, carry out grinding processing as water, polishing machine dish rotating speed, realize borides surfacing.
Present embodiment is a kind of borides surface rapid stock-removal method, boride ceramics is placed under aerobic hot environment, utilize the chemical reaction at material surface place significantly to change surface component, pattern and basic materialization character thereof, the modification that realizes material surface by oxidation can improve the grindability of hard borides ceramic material greatly.
Specifically, ZrB
2, HfB
2while oxidation between middle low-temperature short-time Deng borides, can generate at material surface the oxidation product of layer, and ceramic material inside is not affected.The oxidation product crystal grain of Surface Creation is more tiny, short texture, and the intrinsic hardness of the oxide generating is far below boride.After oxidation processes between this middle low-temperature short-time, improve greatly the grinding efficiency of borides, reduce the requirement to ceramic surface grinding process.
Detailed description of the invention two: the difference of present embodiment and detailed description of the invention one is: taking absolute ethyl alcohol as cleaning agent, borides is carried out to ultrasonic cleaning 20min～40min in step 1, obtain cleaning rear borides.Other are identical with detailed description of the invention one.
Detailed description of the invention three: one of present embodiment and detailed description of the invention one or two difference is: the volume ratio of the cleaning agent described in step 1 and borides is (4～10): 1.Other are identical with detailed description of the invention one or two.
Present embodiment determines that the volume ratio object of cleaning agent and borides is to ensure borides to clean up.
Detailed description of the invention four: one of present embodiment and detailed description of the invention one to three difference is: in step 1 borides be boride ceramics goods or containing boride ceramic structures.Other are identical with detailed description of the invention one to three.
Detailed description of the invention five: one of present embodiment and detailed description of the invention one to four difference is: in step 2, borides after cleaning is placed in to Muffle furnace, be heated to 600～1400 DEG C from room temperature, and be heating and thermal insulation 30min～90min at 600～1400 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation.Other are identical with detailed description of the invention one to four.
Detailed description of the invention six: one of present embodiment and detailed description of the invention one to five difference is: in step 3 by borides after surface oxidation on polishing machine; taking abrasive material as diamond particles or boron carbide particles, grinding medium under 200 turn/min～800 turn/min conditions, carry out grinding processing as water, polishing machine dish rotating speed, realize borides surfacing.Other are identical with detailed description of the invention one to five.
Detailed description of the invention seven: one of present embodiment and detailed description of the invention one to six difference is: the abrasive grain described in step 3 is of a size of 0.5 micron～10 microns.Other are identical with detailed description of the invention one to six.
Content of the present invention is not limited only to the content of the respective embodiments described above, and the combination of one of them or several detailed description of the invention equally also can realize the object of invention.
Adopt following verification experimental verification effect of the present invention
Test one: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 100mL absolute ethyl alcohol as cleaning agent to 30 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 800 DEG C from room temperature, and be heating and thermal insulation 30min at 800 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 10 microns.
Traditional method for grinding:
By 30 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Traditional method for grinding with test one compared with, ZrB
2-SiC ceramic does not directly carry out grinding through ultrasonic cleaning and surface heating oxidation, test one ZrB
2-SiC ceramic method for grinding removal rates is 37cm
2/ hour, and traditional method for grinding removal rates is 14cm
2/ hour, removal rates increase rate is 164%, estimates by boron carbide particles mass change before and after grinding, known boron carbide particles consumption saves 45%.
Utilize SEM to obtain ZrB to testing one
2-SiC ceramic material characterizes, and as shown in Figure 1, Fig. 1 is that test one obtains ZrB
2-SiC ceramic material surfaces shape appearance figure, tests one by Fig. 1 and obtains ZrB
2after-SiC ceramic material is processed by heated oxide, can find that material surface generates a large amount of tiny ZrO
2crystal grain, its microstructure is loose not fine and close, and hardness is lower, is conducive to the grinding of material surface.
Test two: this test with the difference of test one is: in step 2, borides after cleaning is placed in to Muffle furnace, be heated to 1000 DEG C from room temperature, and be heating and thermal insulation 40min at 1000 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation.Other step and parameter are identical with test one.
Traditional method for grinding:
By 30 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Test two ZrB
2-SiC ceramic method for grinding removal rates is 40cm
2/ hour, and traditional method for grinding removal rates is 14cm
2/ hour, removal rates increase rate is 186%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 45%.
Test three: this test with test one difference and be: in step 3 by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 300 turn/min conditions, realizes borides surfacing; Abrasive grain described in step 3 is of a size of 2 microns.Other step and parameter are identical with test one.
Traditional method for grinding:
By 30 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 300 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 2 microns.
Test three ZrB
2-SiC ceramic method for grinding removal rates is 28cm
2/ hour, and traditional method for grinding removal rates is 12cm
2/ hour, removal rates increase rate is 133%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 40%.
Test four: this test with the difference of test one is: taking 45mL absolute ethyl alcohol as cleaning agent, 10 are of a size of in step 1
zrB
2-SiC ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides.Other step and parameter are identical with test one.
Traditional method for grinding:
10 are of a size of
zrB
2-SiC ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Test four ZrB
2-SiC ceramic method for grinding removal rates is 43cm
2/ hour, and traditional method for grinding removal rates is 18cm
2/ hour, removal rates increase rate is 139%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 41%.
Test five: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 18mL absolute ethyl alcohol as cleaning agent to 5 HfB that are of a size of 3mm × 4mm × 36mm
2ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 1400 DEG C from room temperature, and be heating and thermal insulation 5min at 1400 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 10 microns.
Traditional method for grinding:
By 5 HfB that are of a size of 3mm × 4mm × 36mm
2ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Test five HfB
2ceramic method for grinding removal rates is 30cm
2/ hour, and traditional method for grinding removal rates is 12cm
2/ hour, removal rates increase rate is 150%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 30%.
Test six: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 100mL absolute ethyl alcohol as cleaning agent to 30 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC-ZrC ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 800 DEG C from room temperature, and be heating and thermal insulation 30min at 800 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as diamond particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 1 micron.
Traditional method for grinding:
By 5 ZrB that are of a size of 3mm × 4mm × 36mm
2-SiC-ZrC ceramic is on polishing machine, and taking abrasive material as diamond particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 1 micron.
Test six ZrB
2-SiC-ZrC ceramic method for grinding removal rates is 32cm
2/ hour, and traditional method for grinding removal rates is 15cm
2/ hour, removal rates increase rate is 113%, estimates by diamond particles mass change before and after grinding, diamond particles consumption saves 37%.
Test seven: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 15mL absolute ethyl alcohol as cleaning agent to 1 ZrB that is of a size of 30mm × 30mm × 2mm
2-SiC-C ceramic carries out ultrasonic cleaning 30min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 800 DEG C from room temperature, and be heating and thermal insulation 10min at 800 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 10 microns.
Traditional method for grinding:
By 1 ZrB that is of a size of 30mm × 30mm × 2mm
2-SiC-C ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Test seven ZrB
2-SiC-C ceramic method for grinding removal rates is 55cm
2/ hour, and traditional method for grinding removal rates is 15cm
2/ hour, removal rates increase rate is 267%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 55%.
Test eight: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: 15 are of a size of taking 75mL absolute ethyl alcohol as cleaning agent
tiB
2ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 600 DEG C from room temperature, and be heating and thermal insulation 120min at 600 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 800 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 10 microns.
Traditional method for grinding:
15 are of a size of
tiB
2ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 800 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 10 microns.
Test eight TiB
2ceramic method for grinding removal rates is 80cm
2/ hour, and traditional method for grinding removal rates is 35cm
2/ hour, removal rates increase rate is 129%, estimates by boron carbide particles mass change before and after grinding, boron carbide particles consumption saves 33%.
Test nine: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 15mL absolute ethyl alcohol as cleaning agent to 20 HfB that are of a size of 2mm × 3mm × 16mm
2-SiC ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 900 DEG C from room temperature, and be heating and thermal insulation 30min at 900 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as diamond particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 5 microns.
Traditional method for grinding:
By 20 HfB that are of a size of 2mm × 3mm × 16mm
2-SiC ceramic is on polishing machine, and taking abrasive material as diamond particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 500 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 5 microns.
Test nine HfB
2-SiC ceramic method for grinding removal rates is 25cm
2/ hour, and traditional method for grinding removal rates is 10cm
2/ hour, removal rates increase rate is 150%, estimates by diamond particles mass change before and after grinding, diamond particles consumption saves 40%.
Test ten: a kind of method of borides surfacing, specifically completes according to the following steps:
One, ultrasonic cleaning: taking 300mL absolute ethyl alcohol as cleaning agent to 1 ZrB that is of a size of 20mm × 30mm × 60mm
2-MoSi
2-SiC ceramic carries out ultrasonic cleaning 20min, obtains cleaning rear borides;
Two, surface heating oxidation: by cleanings afterwards borides be placed in Muffle furnace, be heated to 1200 DEG C from room temperature, and be heating and thermal insulation 30min at 1200 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine, taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 200 turn/min conditions, realizes borides surfacing.
Abrasive grain described in this test procedure three is of a size of 5 microns.
Traditional method for grinding:
By 1 ZrB that is of a size of 20mm × 30mm × 60mm
2-MoSi
2-SiC ceramic is on polishing machine, and taking abrasive material as boron carbide particles, grinding medium carries out grinding processing as water, polishing machine dish rotating speed under 200 turn/min conditions, realizes borides surfacing, described abrasive grain is of a size of 5 microns.
Test ten ZrB
2-MoSi
2-SiC ceramic method for grinding removal rates is 15cm
2/ hour, and traditional method for grinding removal rates is 8cm
2/ hour, removal rates increase rate is 88%, estimates by diamond particles mass change before and after grinding, boron carbide particles consumption saves 20%.
Claims (7)
1. a method for borides surfacing, is characterized in that the method for borides surfacing completes according to the following steps:
One, ultrasonic cleaning: taking absolute ethyl alcohol as cleaning agent, borides is carried out to ultrasonic cleaning 5min～60min, obtain cleaning rear borides;
Two, surface heating oxidation: borides after cleaning is placed in to Muffle furnace, be heated to 400～1500 DEG C from room temperature, and be heating and thermal insulation 1min～120min at 400～1500 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation;
Three, grinding: by borides after surface oxidation on polishing machine; taking abrasive material as diamond particles or boron carbide particles, grinding medium under 100 turn/min～1000 turn/min conditions, carry out grinding processing as water, polishing machine dish rotating speed, realize borides surfacing.
2. the method for a kind of borides surfacing according to claim 1, is characterized in that taking absolute ethyl alcohol as cleaning agent, borides being carried out to ultrasonic cleaning 20min～40min in step 1, obtains cleaning rear borides.
3. the method for a kind of borides surfacing according to claim 1, the volume ratio that it is characterized in that the cleaning agent described in step 1 and borides is (4～10): 1.
4. the method for a kind of borides surfacing according to claim 1, it is characterized in that in step 1 borides be boride ceramics goods or containing boride ceramic structures.
5. the method for a kind of borides surfacing according to claim 1, it is characterized in that, in step 2, borides after cleaning is placed in to Muffle furnace, be heated to 600～1400 DEG C from room temperature, and be heating and thermal insulation 30min～90min at 600～1400 DEG C in temperature, be cooled to room temperature and obtain borides after surface oxidation.
6. the method for a kind of borides surfacing according to claim 1; it is characterized in that in step 3 borides after surface oxidation on polishing machine; taking abrasive material as diamond particles or boron carbide particles, grinding medium under 200 turn/min～800 turn/min conditions, carry out grinding processing as water, polishing machine dish rotating speed, realize borides surfacing.
7. the method for a kind of borides surfacing according to claim 1, is characterized in that the abrasive grain described in step 3 is of a size of 0.5 micron～10 microns.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN117245460A (en) * | 2023-11-15 | 2023-12-19 | 苏州博志金钻科技有限责任公司 | Surface treatment method and device for ceramic grinding sheet |
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| CN117245460B (en) * | 2023-11-15 | 2024-02-02 | 苏州博志金钻科技有限责任公司 | Surface treatment method and device for ceramic grinding sheet |
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| Publication number | Publication date |
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| CN104191319B (en) | 2016-08-17 |
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