CN104177844A - Traditional Chinese medicine inner package material as well as preparation method and application thereof - Google Patents
Traditional Chinese medicine inner package material as well as preparation method and application thereof Download PDFInfo
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- CN104177844A CN104177844A CN201410415360.8A CN201410415360A CN104177844A CN 104177844 A CN104177844 A CN 104177844A CN 201410415360 A CN201410415360 A CN 201410415360A CN 104177844 A CN104177844 A CN 104177844A
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Abstract
The invention discloses a traditional Chinese medicine inner package material as well as a preparation method and application thereof. The traditional Chinese medicine inner package material comprises the following raw materials in percentage by weight: 55%-75% of paraffin, 15%-35% of rosin, 5%-15% of white vaselin, 0%-10% of beewax, 0.05%-0.4% of polyethylene and 3%-5% of castor oil, wherein the sum of all ingredients is 100%. The preparation method comprises the following steps: preparing ethylene wax and blending wax liquid. The traditional Chinese medicine inner package material is applied to preparation of a traditional Chinese medicine inner package wax shell. The prepared wax shell still adopts paraffin of a conventional wax shell as a main component, the preparation method still adopts a conventional process of hanging the wax shell, cutting, getting wood balls, airing and the like, a unique traditional Chinese medicine package preparation process reappears and is inherited, and the wax shell with moderate hardness and stable quality is obtained.
Description
Technical field
The invention belongs to field of packaging material, be specifically related to a kind of Chinese medicine inner packaging material and preparation method thereof and application.
Background technology
Traditional Chinese medicine pill is generally packed with wax shell, so that take care of and take, because of wax stable in properties, isolation performance is good, can prevent pill draw wet, damage by worms, the volatilization of oxidation and effective constituent, but affected by the factor such as area, season, affected by environment larger, in the easy deliquescing of hot summer weather environment, under cold environment, easily become fragile, add the shell preparation section of waxing numerous and diverse, the interfering factors of technique and quality is many, often, due to wax shell quality problems, have a strong impact on and produce and transport.
At present, use wax shell very rare as the medicine of honeyed bolus packaging, and materials have added other type material mostly, or adopt mechanical means wax shell processed, cannot pass on and innovate to improve to solve and have the series of problems causing due to the feature of wax shell itself, as the humiture environment along with different, the problem such as the quality club of wax shell changes, quality is unstable.Therefore, developing a kind of wax shell wrapping material that can address the above problem is very important.
Summary of the invention
The first object of the present invention is to provide a kind of Chinese medicine inner packaging material; The second object is to provide the preparation method of described Chinese medicine inner packaging material; The 3rd object is to provide the application of described Chinese medicine inner packaging material.
The first object of the present invention is achieved in that by the paraffin of weight percent 55 ~ 75%, 15 ~ 35% rosin, 5 ~ 15% white vaseline, 0 ~ 10% beeswax, 0.05 ~ 0.4% polyethylene and 3 ~ 5% Viscotrol C and forms, and each component sum is 100%.
The second object of the present invention is achieved in that the preparation, the wax liquid adaptation step that comprise ethylene waxes, specifically comprises:
The preparation of A, ethylene waxes: get the paraffin of weight percent 8 ~ 12% in starting paraffin in 90 ~ 130 DEG C of fusings, then divide the polyethylene particle that adds proportioning raw materials ratio for 1 ~ 3 time, at 90 ~ 130 DEG C, stir 5 ~ 10min until polyethylene dissolves completely, cooling to obtain ethylene waxes for subsequent use;
B, the allotment of wax liquid: will prepare the remaining paraffin of ethylene waxes in 90 ~ 130 DEG C of fusings, the ethylene waxes that adds A step to prepare, then add successively rosin, white vaseline, beeswax and the Viscotrol C of proportioning ratio, at 90 ~ 130 DEG C, refine 5 ~ 10min, filter the cooling target compound Chinese medicine inner packaging material that obtains.
The 3rd object of the present invention is achieved in that described Chinese medicine inner packaging material is in the application of preparing in Chinese medicine internal packing wax shell.
The wax shell packaging of large honeyed bolus is one of carrier of traditional Chinese medicine cultural heritage, its stable in properties, isolation performance is good, can prevent honeyed bolus draw wet, damage by worms, the volatilization of oxidation and effective ingredient.With the packaged large honeyed bolus of wax shell, place still fragrant odour of many decades, neither too hard, nor too soft, not perishable.
The wax shell that the present invention is prepared, its component has mainly still followed the paraffin composition of conventional waxes shell, and preparation method also defers to ancient method and hangs wax shell, cuts, gets wooden shot, the operation such as dries, and reappears and has passed on this unique drug packaging preparation process.
Wherein in wax shell component, also add a small amount of polyethylene, increased wax shell hardness and elasticity; Add rosin, increased film-forming properties and the hardness of wax shell, and there is the effect dispelling pathogenic wind and remove dampness; White vaseline has good ductility, oilness, prevents that wax shell is dry and cracked, is easy to be shaped; Viscotrol C has lubrication, and wax shell is easily peeled off, and the wax shell obtaining is complete, attractive in appearance; Beeswax has good plasticity-and viscosity, increases the suppleness of wax shell, makes its outward appearance exquisiteness, glossiness good.
Due to the problem that the feature of wax shell itself causes, as the humiture environment along with different, the quality club of wax shell changes, and by the cooperatively interacting and supplementing of above multiple components, and regulates each raw material usage ratio in prescription, also makes this problem improve.
Brief description of the drawings
Fig. 1 is wax shell internal diameter schematic diagram of the present invention (internal diameter R=25 mm ± 5% in figure);
Fig. 2 is wax shell overall schematic of the present invention;
In figure: l
1for otch infall length, be 12 ~ 17mm, l
2for otch infall width, be 4 ~ 8mm.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated, but never in any form the present invention is limited, and any conversion or the replacement done based on training centre of the present invention, all belong to protection scope of the present invention.
Chinese medicine inner packaging material of the present invention is made up of the paraffin of weight percent 55 ~ 75%, 15 ~ 35% rosin, 5 ~ 15% white vaseline, 0 ~ 10% beeswax, 0.05 ~ 0.4% polyethylene and 3 ~ 5% Viscotrol C, and each component sum is 100%.
Described Chinese medicine inner packaging material is made up of the paraffin of weight percent 55 ~ 75%, 15 ~ 35% rosin, 5 ~ 15% white vaseline, 0 ~ 10% beeswax, 0.05 ~ 0.4% polyethylene and 3 ~ 5% Viscotrol C, and each component sum is 100%.
The preparation method of Chinese medicine inner packaging material of the present invention, comprises and specifically comprises preparation, the wax liquid adaptation step of ethylene waxes:
The preparation of A, ethylene waxes: get the paraffin of weight percent 8 ~ 12% in starting paraffin in 90 ~ 130 DEG C of fusings, then divide the polyethylene particle that adds proportioning raw materials ratio for 1 ~ 3 time, at 90 ~ 130 DEG C, stir 5 ~ 10min until polyethylene dissolves completely, cooling to obtain ethylene waxes for subsequent use;
B, the allotment of wax liquid: will prepare the remaining paraffin of ethylene waxes in 90 ~ 130 DEG C of fusings, the ethylene waxes that adds A step to prepare, then add successively rosin, white vaseline, beeswax and the Viscotrol C of proportioning ratio, at 90 ~ 130 DEG C, refine 5 ~ 10min, filter the cooling target compound Chinese medicine inner packaging material that obtains.
Chinese medicine inner packaging material described in of the present invention being applied as is in the application of preparing in Chinese medicine internal packing wax shell.
The preparation method of described Chinese medicine internal packing wax shell comprises pre-treatment, shell processed, post-processing step, specifically comprises:
A, pre-treatment: get the Chinese medicine inner packaging material preparing, at 90 ~ 130 DEG C, melting obtains wax liquid;
B, shell processed: shell processed wax liquid is obtained to target compound Chinese medicine internal packing wax shell with casing equipment processed;
C, aftertreatment: wax shell is carried out to otch, dry moisture for subsequent use.
Shell processed described in B step is that soaked wooden bead saturated or that poach is crossed is immersed to temperature is repeatedly in the wax liquid of 60 ~ 75 DEG C, reaches 2.4～3.1 g/ grains to wax thickness of the shell, drains the cooling target compound Chinese medicine internal packing wax shell that obtains after redundant paraffin power liquid.
The degree of depth immersing is for flooding wooden shot 1.5 ~ 3cm.
Described cooling be wax shell to be put into purified water cross water cooling.
Otch described in C step is to scratch a volution otch with cutter along the wooden shot middle part of dipping in after wax, and otch infall length is 12～17 mm, and width is 4～8 mm.
Described paraffin meets the regulation of " Chinese Pharmacopoeia two (2010 editions) ";
Described rosin meets the regulation of " first of Drug Standard of Ministry of Public Health of the Peoples Republic of China Chinese medicinal materials ";
Described polyethylene is this coloured particles, without black grain, and inclusion-free, its physical and chemical index meets the regulation of GB/T11115-2009, and hygienic requirements meets the regulation of GB9691.
Described white vaseline meets the regulation of " Chinese Pharmacopoeia two (2010 editions) ".
Described Viscotrol C meets the regulation of " Chinese Pharmacopoeia one (2010 editions) ".
Described beeswax meets the regulation of " Chinese Pharmacopoeia one (2010 editions) ".
The preparation method of Chinese medicine inner packaging material of the present invention, comprises the following steps:
1, the preparation of ethylene waxes
By appropriate heating paraffin fusing, divide and add polyethylene particle 2 times, constantly stir, until polyethylene dissolves completely, pour out, let cool for subsequent use.
2, wax liquid allotment
Production in accordance with regulations measures heating paraffin fusing, adds successively ethylene waxes, rosin, white vaseline, castor-oil plant wet goods material, refines approximately 5～10 minutes, is cooled to optimal temperature after filtration.
3, carry shell
3.1 soaked wooden bead saturated or that poach is crossed is immersed to temperature is repeatedly in the wax liquid of 60 DEG C～75 DEG C, immersion depth is advisable to flood about 1.5cm～3 cm of wooden shot, reach 2.4～3.1 g/ grains to wax thickness of the shell, drain redundant paraffin power liquid, put into immediately purified water and cross water cooling.
3.2 with scratching a volution otch, otch infall length approximately 12 mm～17 mm, wide approximately 4 mm～8 mm in the wooden shot middle part that dip in after wax on cutter edge.
3.3 open wax shell upper part, carefully wooden shot are taken out from bottom to top, obtain a complete wax shell, close incisions, and Stainless Steel Disc is put in tiling, and to dry moisture for subsequent use.
Wax shell prepared by the present invention need meet following specification of quality:
1, outward appearance
Surface should be smooth, otch is neat, and without perforation, yellow-white is to light yellow, becomes a globe with wax handle after closed.
2, wax chitin amount
Each wax chitin amount is 2.4 g～3.1 g/ grains.
3, opening/closing frequency
Each wax shell opening/closing frequency, should be greater than 3 times.
4, microbiological indicator
Microbiological indicator meets table 1 requirement.
The requirement of table 1 microorganism
| Project | Microbial limit |
| Bacterial count | ≤30000cfu/g |
| Mould, yeast count | ≤80cfu/g |
| Escherichia coli | Must not detect |
5, the method for inspection
5.1 condition for surveys
Each sample should be the wax shell of same batch.
5.2 outward appearance
Wax shell outward appearance is judged by vision, gets 10 wax shells, observes one by one at the bright place of available light.
5.3 wax chitin amounts
Get 10 wax shells, weigh its quality with the balance that precision is 0.1 g one by one.
5.4 opening/closing frequency
Get 10 wax shells, do one by one opening/closing frequency.Two hands are respectively held two semicircles of a wax shell, repeatedly do opening and closing action (unlatching, closure are once as a folding unit) taking the angle of 45 °～75 °, observe the connecting portion between two semicircular, completely rupture and be limited with connecting portion, record the opening/closing frequency of each wax shell.
5.5 microbial limit
Take wax shell 10 g, put into mortar, add 0.9 % aseptic sodium chloride solution 100 mL, mix, as the test liquid of 1:10, test by " Chinese Pharmacopoeia " 2010 editions annex X III C limit test of microbe methods.
6, inspection rule
6.1 batching
Use pot flatly, same technique, the wax shell made from Primary batching system is one batch.
6.2 sampling
Early stage, mid-term, the later stage of preparing at wax shell sample respectively, randomly draw 40 at every turn.
6.3 decision rule
Decision rule is in table 1.
Decision rule
| Interventions Requested | Inspected number | Defective judgement |
| Outward appearance | 10 | Defective quantity >=4, this batch defective |
| Quality | 10 | Defective quantity >=4, this batch defective |
| Open and number of times | 10 | Defective quantity >=4, this batch defective |
| Microbial limit | 10 g | As long as occur that defective this batch of judgement is defective |
7, storage condition
Wax shell is positioned in Stainless Steel Disc, and temperature, below 26 DEG C, is ventilated, is dried place and deposit.Staging life, is no more than 8 days.
Embodiment 1
First take 237.6g heating paraffin fusing, then add 2.4g polyethylene, stir it is fully melted, become pour out after ethylene waxes cooling for subsequent use.
Paraffin 1.86kg is put into Stainless Steel Kettle heating and melting, then add successively ethylene waxes 0.24kg, rosin 0.51kg, polyethylene 2.4g, white vaseline 0.24kg, Viscotrol C 0.15kg, constantly stirs it is melted completely, refines after 5-10 minute and is cooled to 60 DEG C～75 DEG C.
Repeatedly immerse in wax liquid steeping water saturated wooden bead, reach 2.4～3.1g/ grain to wax thickness of the shell, drain redundant paraffin power liquid, put into immediately purified water cooling.With scratching a volution otch, otch infall length approximately 12 mm～17 mm, wide approximately 4 mm～8 mm in the wooden shot middle part that dip in after wax on cutter edge.Open wax shell upper part, carefully wooden shot is taken out from bottom to top, obtain a globe with wax handle, close incisions, puts into Stainless Steel Disc and dries moisture.
Through inspection, wax shell smooth surface, otch are neat, and without perforation, yellow-white is to light yellow, become a globe with wax handle after closed; Mean wax chitin amount is 2.6g; On average open with number of times and be greater than 3 times, in microbial limit, bacterial count is 20cfu/g, mould, yeast count < 10cfu/g, and escherichia coli does not detect, and meets quality control requirement.
Embodiment 2
First take 1.14kg heating paraffin fusing, then add 11.5g polyethylene, stir it is fully melted, become pour out after ethylene waxes cooling for subsequent use.
Paraffin 8.9kg is put into Stainless Steel Kettle heating and melting, then add successively ethylene waxes 1.15kg, rosin 2.45kg, white vaseline 1.15kg, Viscotrol C 0.72kg, constantly stirs it is melted completely, refines after 5-10 minute and is cooled to 60 DEG C～75 DEG C.
Repeatedly immerse in wax liquid steeping water saturated wooden bead, reach 2.4～3.1g/ grain to wax thickness of the shell, drain redundant paraffin power liquid, put into immediately purified water cooling.With scratching a volution otch, otch infall length approximately 12 mm～17 mm, wide approximately 4 mm～8 mm in the wooden shot middle part that dip in after wax on cutter edge.Open wax shell upper part, carefully wooden shot is taken out from bottom to top, obtain a globe with wax handle, close incisions, puts into Stainless Steel Disc and dries moisture.
Through inspection, wax shell smooth surface, otch are neat, and without perforation, yellow-white is to light yellow, become a globe with wax handle after closed; Mean wax chitin amount is 2.7g; On average open with number of times and be greater than 3 times, in microbial limit, bacterial count is 25cfu/g, mould, yeast count < 10cfu/g, and escherichia coli does not detect, and meets quality control requirement.
Embodiment 3---folding test:
Opening/closing frequency
Get 10 wax shells (getting respectively 5 wax shells from embodiment 1 and embodiment 2), do one by one opening/closing frequency.Two hands are respectively held two semicircles of a wax shell, repeatedly do opening and closing action (unlatching, closure are once as a folding unit) taking the angle of 45 °～75 °, observe the connecting portion between two semicircular, completely rupture and be limited with connecting portion, record the opening/closing frequency of each wax shell.
Through test, the wax shell of preparing in above-mentioned raw materials ratio and technique, its opening/closing frequency all can meet and exceed 3 times, the reflection wax chitin amount that the method for inspection can be quick, easy.
Claims (9)
1. a Chinese medicine inner packaging material, it is characterized in that described Chinese medicine inner packaging material is made up of the paraffin of weight percent 55 ~ 75%, 15 ~ 35% rosin, 5 ~ 15% white vaseline, 0 ~ 10% beeswax, 0.05 ~ 0.4% polyethylene and 3 ~ 5% Viscotrol C, each component sum is 100%.
2. Chinese medicine inner packaging material according to claim 1, it is characterized in that described Chinese medicine inner packaging material is made up of the paraffin of weight percent 55 ~ 75%, 15 ~ 35% rosin, 5 ~ 15% white vaseline, 0 ~ 10% beeswax, 0.05 ~ 0.4% polyethylene and 3 ~ 5% Viscotrol C, each component sum is 100%.
3. a preparation method for the Chinese medicine inner packaging material described in claim 1 or 2, is characterized in that comprising specifically comprising preparation, the wax liquid adaptation step of ethylene waxes:
The preparation of A, ethylene waxes: get the paraffin of weight percent 8 ~ 12% in starting paraffin in 90 ~ 130 DEG C of fusings, then divide the polyethylene particle that adds proportioning raw materials ratio for 1 ~ 3 time, at 90 ~ 130 DEG C, stir 5 ~ 10min until polyethylene dissolves completely, cooling to obtain ethylene waxes for subsequent use;
B, the allotment of wax liquid: will prepare the remaining paraffin of ethylene waxes in 90 ~ 130 DEG C of fusings, the ethylene waxes that adds A step to prepare, then add successively rosin, white vaseline, beeswax and the Viscotrol C of proportioning ratio, at 90 ~ 130 DEG C, refine 5 ~ 10min, filter the cooling target compound Chinese medicine inner packaging material that obtains.
4. an application for the Chinese medicine inner packaging material described in claim 1 or 2, is characterized in that described Chinese medicine inner packaging material is in the application of preparing in Chinese medicine internal packing wax shell.
5. the application of Chinese medicine inner packaging material according to claim 4, is characterized in that the preparation method of described Chinese medicine internal packing wax shell comprises pre-treatment, shell processed, post-processing step, specifically comprises:
A, pre-treatment: get the Chinese medicine inner packaging material preparing, at 90 ~ 130 DEG C, melting obtains wax liquid;
B, shell processed: shell processed wax liquid is obtained to target compound Chinese medicine internal packing wax shell with casing equipment processed;
C, aftertreatment: wax shell is carried out to otch, dry moisture for subsequent use.
6. the application of Chinese medicine inner packaging material according to claim 5, it is characterized in that shell processed described in B step is that soaked wooden bead saturated or that poach is crossed is immersed to temperature is repeatedly in the wax liquid of 60 ~ 75 DEG C, reach 2.4～3.1 g/ grains to wax thickness of the shell, drain the cooling target compound Chinese medicine internal packing wax shell that obtains after redundant paraffin power liquid.
7. the application of Chinese medicine inner packaging material according to claim 6, is characterized in that the degree of depth immersing is for flooding wooden shot 1.5 ~ 3cm.
8. the application of Chinese medicine inner packaging material according to claim 6, it is characterized in that described cooling be wax shell to be put into purified water cross water cooling.
9. the application of Chinese medicine inner packaging material according to claim 5, is characterized in that the otch described in C step is to scratch a volution otch with cutter along the wooden shot middle part of dipping in after wax, and otch infall length is 12～17 mm, and width is 4～8 mm.
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| CN201410415360.8A CN104177844A (en) | 2014-08-22 | 2014-08-22 | Traditional Chinese medicine inner package material as well as preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108976823A (en) * | 2017-05-31 | 2018-12-11 | 抚顺恒益石化有限公司 | A kind of paraffin and preparation method thereof for Chinese patent drug plastic housing outer layer |
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Application publication date: 20141203 |