CN104173227B - Gel skin care item preparation method and making apparatus based on glycerine and odium stearate - Google Patents
Gel skin care item preparation method and making apparatus based on glycerine and odium stearate Download PDFInfo
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- CN104173227B CN104173227B CN201410353203.9A CN201410353203A CN104173227B CN 104173227 B CN104173227 B CN 104173227B CN 201410353203 A CN201410353203 A CN 201410353203A CN 104173227 B CN104173227 B CN 104173227B
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Abstract
The invention discloses the gel skin care item preparation method based on glycerine and odium stearate supermolecule gelling system and making apparatus.48 50 parts of glycerine, 48 50 parts of deionized water, 0.3 2 parts of odium stearate are taken first, 60 DEG C~90 DEG C is heated to, mixes to form homogeneous system, and acquisition glycerine based supermolecular gel is as matrix gel after being cooled to room temperature；50 100 parts of matrix gel is then taken, 0 50 parts are well mixed with function ingredients, be heated to 60 DEG C~90 DEG C, stir, formed after homogeneous system and be incubated 5 minutes；Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.The beneficial effects of the invention are as follows high molecular polymer is substituted as gelling agent using inexpensive glycerine base gel, the gel skin care item for having moisturizing and skin effect concurrently are prepared.
Description
Technical field
The invention belongs to skin care technical field, it is related to the gel skin care item making side based on glycerine and odium stearate
Method and making apparatus.
Background technology
With the development of gel chemistries, gel skin care item are increasingly becoming the important member of medicinal cosmetic/skin care item.Current shield
The gelling agent used in skin product is mainly lac or water miscible high-molecular compound, such as xanthans, carrageenan, alginic acid
The natural gums such as sodium, gelatin, or sodium carboxymethylcellulose, carboxyethyl cellulose, hydroxy propyl cellulose rope, acrylate copolymer, third
The water soluble polymer of the synthesis such as olefin(e) acid ester copolymer.And the supermolecule gelling system based on organic molecule formation prepares gel
The also rare report of skin care/cosmetics.
The macromolecule gelling agent price used in contemporary skin care product is of a relatively high.With organic molecule glycerine and stearic acid
The gelling system that sodium is constructed is a kind of new supermolecular gel system, can obtain property stabilization, with low cost, with higher
Fusing point and the supermolecular gel of good mechanical (Chen Shuoping, Deng Jing, Fang Liang, the preparation method of glycerine base gel rubber material, China
Patent of invention, application number 201310378132.3), and glycerine (glycerine) has good moistening effect, is widely used in skin care
The design synthesis of product.It is contemplated that using glycerine-odium stearate supermolecular gel as matrix, adding appropriate water-solubility function
Stirred after component, oiliness function ingredients and surfactant congruent melting, can both have been obtained after cooling with moisturizing, skin care and other are medicinal
The new type gel skin care item of effect.
The content of the invention
It is an object of the invention to provide the gel skin care item system based on glycerine Yu odium stearate supermolecule gelling system
Make method, solve the problem of macromolecule gelling agent price used in contemporary skin care product is of a relatively high.
It is a further object to provide making apparatus.
The technical solution adopted in the present invention is to follow the steps below：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water,
0.3-2 parts of odium stearate；
Step 2：Will each composition mix after be heated to 60 DEG C~90 DEG C, stirring to homogeneous system is formed, be cooled to room temperature with
After can obtain translucent glycerine based supermolecular gel；
Step 3：50-100 parts of glycerine based supermolecular gel is taken, 0-50 parts are well mixed with function ingredients, are heated to 60
DEG C~90 DEG C, stir, formed after homogeneous system and be incubated 5 minutes；
Step 4：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
Further, the function ingredients include water-soluble water-solubility function component and are insoluble in the oiliness function of water
Component；Wherein water-soluble water-solubility function component includes vitamin C, allantoin, hyaluronic acid, parachlorometaxylenol etc.
One or more combination in water soluble compound, and the water-soluble extractive of various crude drugs such as Flos Osmanthi Fragrantis extract；No
Water-soluble oiliness function ingredients include jojoba oil, wheat-germ oil, saualane, tea tree ethereal oil, osmanthus essential oil, lavender
The one or more combination of essential oil.
Further, the heat sensitivity component in the function ingredients is stirred under the conditions of 60 DEG C.
Further, when added water insoluble oiliness function ingredients quality is more than the 1% of matrix gel, oily components
In be additionally added surfactant, and be well mixed in advance with oiliness function ingredients.
Further, the surfactant includes Tween 80, sorbester p17, glyceryl monostearate.
A kind of preparation method of gel skin care item based on glycerine and odium stearate, is followed the steps below：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water,
0.3-2 parts of odium stearate, water-soluble 0-50 parts of water-solubility function component, the mass parts of water insoluble oiliness function ingredients
Number is no more than glycerine, deionized water, the 1% of three kinds of composition quality summations of odium stearate；
Step 2：60 DEG C~90 DEG C are heated to after each composition is mixed, 5 minutes are incubated after stirring to formation homogeneous system；
Step 3：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
Further, the function ingredients include water-soluble water-solubility function component and are insoluble in the oiliness function of water
Component；Wherein water-soluble water-solubility function component includes vitamin C, allantoin, hyaluronic acid, parachlorometaxylenol etc.
One or more combination in water soluble compound, and the water-soluble extractive of various crude drugs such as Flos Osmanthi Fragrantis extract；No
Water-soluble oiliness function ingredients include jojoba oil, wheat-germ oil, saualane, tea tree ethereal oil, osmanthus essential oil, lavender
The one or more combination of essential oil.
Further, the heat sensitivity component in the function ingredients is stirred under the conditions of 60 DEG C.
The equipment for making the gel skin care item based on glycerine odium stearate, including water-bath, water-bath are built-in with round bottom
Flask, round-bottomed flask bottom is provided with magnetic stir bar, and round-bottomed flask open communication has reflux condensing tube, and reflux condensing tube is provided with out
Mouth and entrance, here are water inlets, and the above is delivery port, and water-bath seat is on magnetic force heating stirrer.
The beneficial effects of the invention are as follows substituted with inexpensive glycerine base gel (glycerine and odium stearate gelling system)
High molecular polymer prepares the gel skin care item for having moisturizing and skin effect concurrently as gelling agent.
Brief description of the drawings
Fig. 1 is implementation figure of the present invention.
Embodiment
The present invention is described in detail with reference to the accompanying drawings and detailed description.
Present device is as shown in figure 1, including water-bath 1, water-bath 1 is built-in with round-bottomed flask 2, the bottom of round-bottomed flask 2
Provided with magnetic stir bar 3, the open communication of round-bottomed flask 2 has reflux condensing tube 4, and reflux condensing tube 4 is provided with outlet and entrance, below
It is water inlet, the above is delivery port, and water-bath 1 is on magnetic force heating stirrer 5；
Device in use, add material into round-bottomed flask 2 first, and reflux condensing tube 4 prevents moisture evaporation, magnetic agitation
Son 3 makes each component be well mixed for that can be opened after temperature rises to design temperature.Device in the present invention can be using burning
Cup replaces round-bottomed flask 2 and reflux condensing tube 4, and glass bar replaces magnetic stir bar 3, and (when being substituted using beaker, moisture can be waved
Hair is a small amount of, and proportioning is slightly influenceed, less demanding occasion is suitable only for).The type gel skin care item are prepared simply, and cost
Relative moderate.
Preparation method of the present invention：The present invention is on the basis of using glycerine/odium stearate gelling system as matrix, to add
The gel skin care item of other function ingredients synthesis.
Inventive gel skin care item preparation method is divided into following steps：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water,
0.3-2 parts of odium stearate；
Step 2：Will each composition mix after be heated to 60 DEG C~90 DEG C, stirring to homogeneous system is formed, be cooled to room temperature with
After can obtain translucent glycerine based supermolecular gel；
Step 3：50-100 parts of glycerine based supermolecular gel is taken, 0-50 parts are well mixed with function ingredients, are heated to 60
DEG C~90 DEG C, stir, formed after homogeneous system and be incubated 5 minutes；
Step 4：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
When added water insoluble oiliness function ingredients mass fraction is more than the 1% of matrix gel, in oily components
Appropriate surfactant is must be added to, surfactant includes but is not limited to Tween 80, sorbester p17, glyceryl monostearate
Deng, and be well mixed in advance with oiliness function ingredients.
Another preparation method of inventive gel skin care item is divided into following steps：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water,
0.3-2 parts of odium stearate, water-soluble 0-50 parts of water-solubility function component, the mass parts of water insoluble oiliness function ingredients
Number is no more than glycerine, deionized water, the 1% of three kinds of composition quality summations of odium stearate；
Step 2：60 DEG C~90 DEG C are heated to after each composition is mixed, 5 minutes are incubated after stirring to formation homogeneous system；
Step 3：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
In two kinds of preparation methods above：
Heat sensitivity component in function ingredients is stirred under the conditions of 60 DEG C.
Water-soluble water miscible function ingredients include but is not limited to vitamin C, allantoin, hyaluronic acid, chlorine
The water soluble compounds such as xylenols, and the various crude drugs such as Flos Osmanthi Fragrantis extract water-soluble extractive.
The oiliness function ingredients for being insoluble in water include but is not limited to jojoba oil, wheat-germ oil, saualane, Yi Jiqi
His plants essential oil such as tea tree ethereal oil, osmanthus essential oil, Lavender etc..
When added function ingredients be water-soluble water miscible function ingredients when, formation be illiquidity gel
The gel skin care item of type.Creams can not at this time be formed.When added function ingredients are water insoluble oily components, if oiliness
Component and glycerine base gel proportions are not more than 2: 8, then gained skin care item are Gel miles of illiquidity；If oily components and the third three
When alcohol-based gel ratio is between 2: 8 and 5: 5, gained skin care item are semimobile creams.
Specific embodiment is set forth below, and the present invention will be described：
Embodiment 1：One Gel miles of type gel skin care item containing tea tree elite can feed intake according to table 1 below formula：
Table 1
| Component | Material name | Mass fraction/% | Remarks |
| 1 | Glycerine | 50 | |
| 2 | Deionized water | 50 | |
| 3 | Odium stearate | 0.3 | |
| 4 | Parachlorometaxylenol | 0.2 |
| 5 | Tea tree ethereal oil | 0.3 | In 60 DEG C of additions |
Embodiment 2：One Gel miles of type gel skin care item containing sweet osmanthus elite can feed intake according to table 2 below formula：
Table 2
| Component | Material name | Mass fraction/% | Remarks |
| 1 | Glycerine | 48 | |
| 2 | Deionized water | 48 | |
| 3 | Odium stearate | 1 | |
| 4 | Flos Osmanthi Fragrantis extract | 2 | Can be in 60 DEG C of additions |
| 5 | Osmanthus essential oil | 1 | Can be in 60 DEG C of additions |
Embodiment 3：One Gel miles of type gel skin care item containing lavender elite can feed intake according to table 3 below formula：
Table 3
| Component | Material name | Mass fraction/% | Remarks |
| 1 | Glycerine base gel | 90 | |
| 2 | Jojoba oil | 7 | |
| 3 | Lavender | 1 | |
| 4 | Tween-80 | 0.6 | |
| 5 | Glyceryl monostearate | 1.4 |
Embodiment 4：One creams type gel skin care item containing sweet osmanthus elite can feed intake according to table 4 below formula：
Table 4
| Component | Material name | Mass fraction/% | Remarks |
| 1 | Glycerine base gel | 50 |
| 2 | Jojoba oil | 20 | |
| 3 | Wheat-germ oil | 19 | |
| 4 | Osmanthus essential oil | 1 | |
| 5 | Tween-80 | 3 | |
| 6 | Glyceryl monostearate | 7 |
Example 5：Glycerine 50g is weighed, deionized water 50g, odium stearate 0.3g, parachlorometaxylenol 0.2g is mixed,
It is heated to 90 DEG C and is stirred, be allowed to be formed after settled solution, be incubated 5 minutes at this temperature, cool to 60 DEG C, adds tea
Essential oil 0.3g is set, after stirring, 5 minutes is incubated, injects mould molding, you can obtain Gel miles of type for having sterilization and moisture-keeping functions concurrently
Gel skin care item.
Example 6：Glycerine 48g is weighed, deionized water 48g, odium stearate 1g mixing is heated to 80 DEG C and stirred,
It is allowed to be formed after settled solution, is incubated 5 minutes at this temperature, cool to 60 DEG C, adds solid-state Flos Osmanthi Fragrantis extract 2g, sweet osmanthus essence
Oily 1g, after stirring, is incubated 5 minutes, injects mould molding, can obtain after cooling with whitening, skin-moisturizing, skin effect
Gel miles of type gel skin care item of sweet osmanthus elite.
Example 7：Glycerine 50g is weighed first, and deionized water 49g, odium stearate 1g mixing is heated to 90 DEG C and stirred
Mix, be allowed to be formed after settled solution, be incubated 5 minutes at this temperature, inject mould molding, you can obtain with given shape
Translucent glycerine base gel.Jojoba oil 7g, Lavender 1g, the 0.6g of surface active agent tween -80 are then taken, it is stearic
Sour monoglyceride 1.4g, in 60 DEG C of heating for dissolving, after stirring, adds synthesized glycerine base gel 90g, keeps this temperature
System is melted, and is stirred continuously within 10 minutes, after homogeneous system to be formed, be incubated 5 minutes, inject mould molding, after cooling i.e.
The gel type gel skin care item for having moisturizing, moisturizing and whitening capability concurrently can be obtained.
Example 8：Glycerine 50g is weighed first, and deionized water 48g, odium stearate 2g mixing is heated to 100 DEG C and is subject to
Stirring, is allowed to be formed after settled solution, is incubated 5 minutes at this temperature, injects mould molding, you can obtaining has given shape
Translucent glycerine base gel.Jojoba oil 20g is then taken, wheat-germ oil 19g, osmanthus essential oil 1g, surfactant is told
Temperature -80 3g, glyceryl monostearate 7g, after 70 DEG C dissolve by heating and stir, add synthesized glycerine base gel
50g, keeps this temperature to melt system in 10 minutes, and is stirred continuously, after homogeneous system to be formed, is incubated 5 minutes, injects mould
Shaping, can obtain the creams type gel skin care item for having moisturizing, moisturizing and whitening capability concurrently after cooling.
Claims (2)
1. the gel skin care item preparation method based on glycerine and odium stearate, it is characterised in that follow the steps below：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water, tristearin
Sour sodium 0.3-2 parts；
Step 2：Will each composition mix after be heated to 60 DEG C~90 DEG C, stirring is to homogeneous system is formed, and being cooled to after room temperature can
To obtain translucent glycerine based supermolecular gel；
Step 3：50-100 parts of glycerine based supermolecular gel is taken, 50 parts are well mixed with function ingredients, are heated to 60 DEG C~90
DEG C, stir, formed after homogeneous system and be incubated 5 minutes；Wherein, the heat sensitivity component in function ingredients is under the conditions of 60 DEG C
Stirring；
The function ingredients include water-soluble water-solubility function component and are insoluble in the oiliness function ingredients of water；Wherein may be used
Being dissolved in the water-solubility function component of water includes vitamin C, allantoin, hyaluronic acid, parachlorometaxylenol water soluble compound
And the one or more combination in Flos Osmanthi Fragrantis extract；Being insoluble in the oiliness function ingredients of water includes jojoba oil, wheat
Bud oil, saualane, tea tree ethereal oil, osmanthus essential oil, the one or more combination of Lavender；
When added water insoluble oiliness function ingredients quality is more than the 1% of matrix gel, table is additionally added in oily components
Face activating agent, and be well mixed in advance with oiliness function ingredients；
The surfactant includes Tween 80, sorbester p17, glyceryl monostearate；
Step 4：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
2. the gel skin care item preparation method based on glycerine and odium stearate, it is characterised in that follow the steps below：
Step 1：Prepare raw material, the mass fraction of each constituent is：48-50 parts of glycerine, 48-50 parts of deionized water, tristearin
Sour sodium 0.3-2 parts, water-soluble 50 parts of water-solubility function component, the mass fraction of water insoluble oiliness function ingredients is not
More than glycerine, deionized water, three kinds of composition quality summations of odium stearate 1%；Wherein, the heat sensitivity group in function ingredients
Divide and stirred under the conditions of 60 DEG C；
Water-soluble water-solubility function component includes vitamin C, allantoin, hyaluronic acid, parachlorometaxylenol water
One or more combination in soluble compound and Flos Osmanthi Fragrantis extract；The oiliness function ingredients for being insoluble in water are included suddenly
Bar oil, wheat-germ oil, saualane, tea tree ethereal oil, osmanthus essential oil, the one or more combination of Lavender suddenly；
Step 2：60 DEG C~90 DEG C are heated to after each composition is mixed, 5 minutes are incubated after stirring to formation homogeneous system；
Step 3：Mould molding is injected, is cooled to after room temperature, that is, forms gel skin care item.
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| CN201410353203.9A CN104173227B (en) | 2014-07-24 | 2014-07-24 | Gel skin care item preparation method and making apparatus based on glycerine and odium stearate |
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| CN104804795B (en) * | 2015-03-31 | 2018-07-03 | 桂林理工大学 | It is a kind of using waste cooking oil as solid alcohol of raw material and preparation method thereof and equipment |
| CN107320403A (en) * | 2017-08-29 | 2017-11-07 | 山东维赫生物科技有限公司 | A kind of Chloranthus glaber shower condensation |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010125543A2 (en) * | 2009-04-30 | 2010-11-04 | L'oreal | Cosmetic composition comprising a surfactant with hlb greater than or equal to 12 and a coated pigment |
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| US20050220832A1 (en) * | 2004-03-25 | 2005-10-06 | Richard Walton | Gels containing metallic soaps and coupling agents |
| CN1796519A (en) * | 2004-12-27 | 2006-07-05 | 葛海霖 | Solid wax candle with color flame and prepration method |
| CN103446962A (en) * | 2013-08-27 | 2013-12-18 | 桂林理工大学 | Preparation method of glycerin-based gel material |
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| WO2010125543A2 (en) * | 2009-04-30 | 2010-11-04 | L'oreal | Cosmetic composition comprising a surfactant with hlb greater than or equal to 12 and a coated pigment |
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