CN104163457B - A kind of preparation method of monodisperse water soluble ferroferric oxide nano granules - Google Patents
A kind of preparation method of monodisperse water soluble ferroferric oxide nano granules Download PDFInfo
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- CN104163457B CN104163457B CN201410339575.6A CN201410339575A CN104163457B CN 104163457 B CN104163457 B CN 104163457B CN 201410339575 A CN201410339575 A CN 201410339575A CN 104163457 B CN104163457 B CN 104163457B
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- solution
- oxide nano
- ferroferric oxide
- nano granules
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- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000008187 granular material Substances 0.000 title claims abstract description 61
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims abstract description 76
- 238000003756 stirring Methods 0.000 claims abstract description 36
- 238000000034 method Methods 0.000 claims abstract description 27
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 34
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 30
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 17
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 16
- 238000006243 chemical reaction Methods 0.000 claims description 15
- 230000005291 magnetic effect Effects 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 8
- 238000013019 agitation Methods 0.000 claims description 8
- 229910052786 argon Inorganic materials 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000007789 gas Substances 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000000703 high-speed centrifugation Methods 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 8
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims description 8
- 238000003760 magnetic stirring Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000003960 organic solvent Substances 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- 230000001105 regulatory effect Effects 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- 239000002105 nanoparticle Substances 0.000 abstract description 12
- 238000000975 co-precipitation Methods 0.000 abstract description 10
- 238000001556 precipitation Methods 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000002904 solvent Substances 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 95
- 230000005415 magnetization Effects 0.000 description 5
- 239000013078 crystal Substances 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 239000002122 magnetic nanoparticle Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 229920002521 macromolecule Polymers 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000013543 active substance Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- -1 at 300K Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005308 ferrimagnetism Effects 0.000 description 1
- 230000005294 ferromagnetic effect Effects 0.000 description 1
- 239000011553 magnetic fluid Substances 0.000 description 1
- 230000005389 magnetism Effects 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000013110 organic ligand Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 229910052596 spinel Inorganic materials 0.000 description 1
- 239000011029 spinel Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
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Priority Applications (1)
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CN201410339575.6A CN104163457B (en) | 2014-07-17 | 2014-07-17 | A kind of preparation method of monodisperse water soluble ferroferric oxide nano granules |
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CN201410339575.6A CN104163457B (en) | 2014-07-17 | 2014-07-17 | A kind of preparation method of monodisperse water soluble ferroferric oxide nano granules |
Publications (2)
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CN104163457A CN104163457A (en) | 2014-11-26 |
CN104163457B true CN104163457B (en) | 2015-12-09 |
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CN201410339575.6A Active CN104163457B (en) | 2014-07-17 | 2014-07-17 | A kind of preparation method of monodisperse water soluble ferroferric oxide nano granules |
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CN (1) | CN104163457B (en) |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101870499A (en) * | 2010-06-03 | 2010-10-27 | 四川大学 | Ultrasonic vibration and in-situ coating preparation method of superparamagnetic ferroferric oxide nanoparticle |
CN103818971A (en) * | 2014-03-12 | 2014-05-28 | 厦门大学 | Preparation method for superparamagnetism ferrite nano particles |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101767836A (en) * | 2008-12-31 | 2010-07-07 | 陕西北美基因股份有限公司 | Method for preparing ferroferric oxide magnetic nanospheres |
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2014
- 2014-07-17 CN CN201410339575.6A patent/CN104163457B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101870499A (en) * | 2010-06-03 | 2010-10-27 | 四川大学 | Ultrasonic vibration and in-situ coating preparation method of superparamagnetic ferroferric oxide nanoparticle |
CN103818971A (en) * | 2014-03-12 | 2014-05-28 | 厦门大学 | Preparation method for superparamagnetism ferrite nano particles |
Non-Patent Citations (1)
Title |
---|
单分散Fe3O4纳米粉体的溶剂热合成及磁性;张敏等;《硅酸盐通报》;20110831;第30卷(第4期);摘要 * |
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CN104163457A (en) | 2014-11-26 |
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C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Guoyang Inventor before: Cheng Honglin |
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Effective date of registration: 20151028 Address after: 410 No., R & D building, Shishi hi tech Innovation Service Center, Quanzhou, Fujian, 362000 Applicant after: FUJIAN GANCHUANG PRECISION MACHINERY Co.,Ltd. Address before: Office building 215000 Yushan road Jiangsu city Suzhou province high tech Industrial Development Zone Industrial Park Building 4 Room 401. Applicant before: SUZHOU BOXUN INSTRUMENTS Co.,Ltd. |
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Effective date of registration: 20181127 Address after: 313023 No. 26 innovation road, Dai Xi District, Wuxing Economic Development Zone, Huzhou, Zhejiang Patentee after: HUZHOU YUFAN COSMETIC TECHNOLOGY CO.,LTD. Address before: 362000 R&D Building 410 -411, Shishi Hi-tech Entrepreneurship Service Center, Quanzhou City, Fujian Province Patentee before: FUJIAN GANCHUANG PRECISION MACHINERY Co.,Ltd. |
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Effective date of registration: 20221228 Address after: 276800 R & D building, No. 8, electronic information industrial park, Gaoxin seventh Road, high tech Zone, Rizhao City, Shandong Province Patentee after: Rizhao Xinrui Investment Promotion Development Co.,Ltd. Address before: 313023 No. 26 innovation road, Dai Xi District, Wuxing Economic Development Zone, Huzhou, Zhejiang Patentee before: HUZHOU YUFAN COSMETIC TECHNOLOGY CO.,LTD. |