CN104153082B - Aloe antibiotic yarn - Google Patents
Aloe antibiotic yarn Download PDFInfo
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- CN104153082B CN104153082B CN201410414339.6A CN201410414339A CN104153082B CN 104153082 B CN104153082 B CN 104153082B CN 201410414339 A CN201410414339 A CN 201410414339A CN 104153082 B CN104153082 B CN 104153082B
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- aloe
- yarn
- antimicrobial agent
- silver zeolite
- antibiotic
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Abstract
Aloe antibiotic yarn, belongs to textile technology field, is made up of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent.The aloe antibiotic yarn that the present invention provides has concurrently antibacterial with pro-skin function, the most soft smooth, the pro-skin profit table of product, and outward appearance is beautiful affable, bright and plentiful, the most also there is good antibacterial bacteriostatic effect.Compared with tradition Aloe yarn, aloe antibiotic yarn excellent combination property, there is high market popularization value.
Description
Technical field
The invention belongs to textile technology field, particularly to a kind of aloe antibiotic yarn.
Background technology
nullAt present，Utilize yarn that aloe fibre makes or the equal existing procucts of yarn utilizing anti-bacterial fibre to make emerge，Chinese patent storehouse also has a lot of relevant record，Such as CN201210458080.6、CN201110355571.3、CN201320209391.9、CN201320172275.4、CN201320172290.9、CN201210227959.X、CN201010557918.8、CN201010557918.8、CN201110430892.5、CN01102267.1、CN201310378419.6 etc.，Respectively the manufacture method of Aloe yarn with antimicrobial yarn is described，But there are no the document report both being combined.
Aloe viscose rayon has biological activity, and the soft yarns of making is comfortable, skin-friendly good, but is easily corroded by antibacterial.The new type yarn using CN200410060290.5 patent to provide antibacterial viscose fiber blending therewith to make is the most soft, pro-skin profit table, but also possessed preferable antibacterial bacteriostatic effect, the application performance of yarn can be improved, be greatly expanded the application space of this type of yarn.
Summary of the invention
The invention aims to provide a kind of aloe antibiotic yarn.
Based on above-mentioned purpose, this invention takes following technical scheme: aloe antibiotic yarn, be made up of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent.
Above-mentioned aloe antibiotic yarn can be prepared by following two schemes, and one is:
Described aloe antibiotic yarn prepares via following methods: (1) takes Aloe extract and mixes with regenerated cellulose viscose, obtains Aloe viscose rayon through wet spinning；(2) take silver zeolite antimicrobial agent to mix with regenerated cellulose viscose, obtain antibacterial viscose fiber through wet spinning；(3) by step (1) gained Aloe viscose rayon and the antibacterial viscose fiber blending of step (2) gained and get final product.
Described Aloe extract calculates with dry and accounts for 1～50wt% in described Aloe viscose rayon.
In described antibacterial viscose fiber, the addition of silver zeolite antimicrobial agent is the 0.5～5wt% of regenerated cellulose.
Described Aloe viscose rayon accounts for the 1～99% of yarn gross weight, and antibacterial viscose fiber accounts for the 1～99% of yarn gross weight.
It two is:
Described aloe antibiotic yarn prepares via following methods: silver zeolite antimicrobial agent is evenly spread in the water added with Aloe extract by (1)；(2) separately take Aloe extract to mix homogeneously with regenerated cellulose viscose, then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Described step (1) adds 30～60 times of water dissolutioies particularly as follows: take 5～10 weight portion Aloe extracts, is subsequently adding the silver zeolite antimicrobial agent of 0.5～5 weight portions, utilizes high shear dispersion machine to shear dispersion 15～30min.
In described step (2), the addition of Aloe extract is 0～90 weight portions, and regenerated cellulose is 50～100 weight portions.
In described step (2), the addition of Aloe extract is 10～40 weight portions.
Particle diameter≤2.0 μm of described silver zeolite antimicrobial agent.
The aloe antibiotic yarn that the present invention provides has concurrently antibacterial with pro-skin function, the most soft smooth, the pro-skin profit table of product, and outward appearance is beautiful affable, bright and plentiful, the most also there is good antibacterial bacteriostatic effect.Compared with tradition Aloe yarn, aloe antibiotic yarn excellent combination property, there is high market popularization value.
The aloe antibiotic yarn of the present invention can be realized with antibacterial viscose fiber blending by (scheme one) existing Aloe viscose rayon, also (scheme two) spinning can be carried out with regenerated cellulose, Aloe extract and silver zeolite antimicrobial agent after raw material mixing, first give monofilament (fiber) dual-use function, the most again by silk spun yarn.
For scheme one, its preparation method is simple, and enterprise outsourcing Aloe viscose rayon and antibacterial viscose fiber can carry out blending respectively, just can obtain finished product, it is not necessary to increase new equipment, it is easy to be widely popularized.
But but there is following defect in this scheme: either silver zeolite antimicrobial agent or Aloe extract, the addition in monofilament is all limited；Aloe extract addition is excessive, can affect the intensity of fiber, and if silver zeolite antimicrobial agent addition is excessive, also easily cause stress concentration point, thus affect yarn strength.Assume the addition capping value of silver zeolite antimicrobial agent in antibacterial viscose fiber, i.e. 5wt%, as a example by the Aloe viscose rayon blending rate with each 50wt% of antibacterial viscose fiber, in scribbled, the average addition of silver zeolite antimicrobial agent only has 2.5wt%, can not reach best antimicrobial effect.If continuing to increase the silver zeolite antimicrobial agent in monofilament, its intensity can be made again to have a greatly reduced quality.Also it is such for Aloe extract.In other words, in mixed yarn, the maximum addition of silver zeolite antimicrobial agent and Aloe extract is rather limited.
By contrast, second scheme can overcome drawbacks described above, and the addition for silver zeolite antimicrobial agent and Aloe extract provides bigger selection space.Simultaneously, owing in Aloe extract, moieties has Natural surfactant, therefore, regard Aloe extract as a kind of necessary raw material on the premise of, it is also possible to by its surface activity effect, effectively reduce ultra-fine silver zeolite antimicrobial agent powder granule agglomeration in viscose glue, significantly improve the spinnability of this functional fibre, reduce lousiness rate, improve fiber row yielding, it is also possible to significantly improve the strength of fiber or even yarn.
In the present invention, Aloe extract used all adds with Aloe extraction solution form, and its addition is all in terms of dry.The extraction of Aloe extraction solution can refer to following procedure: Aloe → thin skin takes glue → making beating homogenizing → separation and carries old → Aloe extract.
The preparation of regenerated cellulose viscose can refer to following procedure: pulp → alkali soaks, squeezes, pulverizes → aging → yellow → dissolving.
Spinning can use RING SPINNING, SEILE textile, vortex spinning or method for open-end rotor spinning to carry out.
RING SPINNING manufacturing process is: blowing room-comb and parallel cotton fibers prior to spinning-pre-drawing-bar also rolls up-combing-slubbing drafting-two road drafting-rove-spun yarn-winder.
SEILE textile manufacturing process is: the parallel feeding of coarse sand-drawing-off simultaneously-output single thread yarn-twist on twist.
Vortex spinning manufacturing process is: Blowing carding-three road T drafting-vortex spinning.
Air spinning manufacturing process is: blowing room-comb and parallel cotton fibers prior to spinning-pre-drawing-bar also rolls up-combing-slubbing drafting-two road drafting-air-jet spinning.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described.
Embodiment 1
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take Aloe extract to mix with regenerated cellulose viscose, obtain Aloe viscose rayon through wet spinning；Aloe extract calculates with dry and accounts for 30wt% in Aloe viscose rayon.
(2) take silver zeolite antimicrobial agent (particle diameter 1.0～2.0 μm) to mix with regenerated cellulose viscose, obtain antibacterial viscose fiber through wet spinning；The addition of silver zeolite antimicrobial agent is the 2.5wt% of regenerated cellulose.
(3) by step (1) gained Aloe viscose rayon and the antibacterial viscose fiber blending of step (2) gained and get final product.
Described Aloe viscose rayon accounts for the 50% of yarn gross weight, and antibacterial viscose fiber accounts for the 50% of yarn gross weight.
Embodiment 2
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take Aloe extract to mix with regenerated cellulose viscose, obtain Aloe viscose rayon through wet spinning；Aloe extract calculates with dry and accounts for 20wt% in Aloe viscose rayon.
(2) take silver zeolite antimicrobial agent (particle diameter 1.0～2.0 μm) to mix with regenerated cellulose viscose, obtain antibacterial viscose fiber through wet spinning；The addition of silver zeolite antimicrobial agent is the 3wt% of regenerated cellulose.
(3) by step (1) gained Aloe viscose rayon and the antibacterial viscose fiber blending of step (2) gained and get final product.
Described Aloe viscose rayon accounts for the 60% of yarn gross weight, and antibacterial viscose fiber accounts for the 40% of yarn gross weight.
Embodiment 3
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take Aloe extract to mix with regenerated cellulose viscose, obtain Aloe viscose rayon through wet spinning；Aloe extract calculates with dry and accounts for 1wt% in Aloe viscose rayon.
(2) take silver zeolite antimicrobial agent (particle diameter 0.5～1.0 μm) to mix with regenerated cellulose viscose, obtain antibacterial viscose fiber through wet spinning；The addition of silver zeolite antimicrobial agent is the 5wt% of regenerated cellulose.
(3) by step (1) gained Aloe viscose rayon and the antibacterial viscose fiber blending of step (2) gained and get final product.
Described Aloe viscose rayon accounts for the 99% of yarn gross weight, and antibacterial viscose fiber accounts for the 1% of yarn gross weight.
Embodiment 4
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take Aloe extract to mix with regenerated cellulose viscose, obtain Aloe viscose rayon through wet spinning；Aloe extract calculates with dry and accounts for 50wt% in Aloe viscose rayon.
(2) take silver zeolite antimicrobial agent (particle diameter 0.5～1.0 μm) to mix with regenerated cellulose viscose, obtain antibacterial viscose fiber through wet spinning；The addition of silver zeolite antimicrobial agent is the 0.5wt% of regenerated cellulose.
(3) by step (1) gained Aloe viscose rayon and the antibacterial viscose fiber blending of step (2) gained and get final product.
Described Aloe viscose rayon accounts for the 1% of yarn gross weight, and antibacterial viscose fiber accounts for the 99% of yarn gross weight.
Embodiment 5
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 7 weight portion Aloe extracts and add 40 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 0.2～0.5 μm) of 2.5 weight portions, utilize high shear dispersion machine to shear dispersion 20min.Stand 15min to observe without sedimentation.
(2) separately take 35 weight portion Aloe extracts to mix homogeneously with viscose (containing 100 weight portion regenerated celluloses), then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 6
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 5 weight portion Aloe extracts and add 50 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 0.2～0.5 μm) of 3 weight portions, utilize high shear dispersion machine to shear dispersion 30min.Stand 15min to observe without sedimentation.
(2) separately take 20 weight portion Aloe extracts to mix homogeneously with viscose (containing 100 weight portion regenerated celluloses), then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 7
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 5 weight portion Aloe extracts and add 30 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 0.5～1.0 μm) of 0.5 weight portion, utilize high shear dispersion machine to shear dispersion 15min.Stand 15min to observe without sedimentation.
(2) step (1) gained mixed liquor injected in viscose (containing 100 weight portion regenerated celluloses) and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 8
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 10 weight portion Aloe extracts and add 60 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 0.2～0.5 μm) of 5 weight portions, utilize high shear dispersion machine to shear dispersion 30min.Stand 15min to observe without sedimentation.
(2) separately take 90 weight portion Aloe extracts to mix homogeneously with viscose (containing 100 weight portion regenerated celluloses), then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 9
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 5.6 weight portion Aloe extracts and add 50 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 1.0～2.0 μm) of 1.25 weight portions, utilize high shear dispersion machine to shear dispersion 30min.Stand 15min to observe without sedimentation.
(2) separately take 12 weight portion Aloe extracts to mix homogeneously with viscose (containing 100 weight portion regenerated celluloses), then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 10
Aloe antibiotic yarn, is made up via following methods of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent:
(1) take 5.1 weight portion Aloe extracts and add 50 times of water dissolutioies, be subsequently adding the silver zeolite antimicrobial agent (particle diameter 1.0～2.0 μm) of 1.5 weight portions, utilize high shear dispersion machine to shear dispersion 30min.Stand 15min to observe without sedimentation.
(2) separately take 6 weight portion Aloe extracts to mix homogeneously with viscose (containing 100 weight portion regenerated celluloses), then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；
(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
Embodiment 11
With reference to the carrier trace qualitative method in the Anti-microbial Performance Tests method of textile industry standard FZ/T01021-92 fabric, the yarn samples of embodiment 1,2,9,10 is carried out antibiotic rate mensuration, and measuring sample antibiotic rate after 20 conventional wash, result is as shown in table 1.
The antibiotic rate measurement result of table 1 sample segment
As it can be seen from table 1 when Aloe extract in yarn, silver zeolite antimicrobial agent content close to time, its anti-microbial property is also very close to；Product with reference to scheme two preparation is slightly better than scheme one, but difference is inconspicuous.
Prepare the yarn samples of same size with reference to embodiment 1,2,9,10, be labeled as 1#, 2#, 9#, 10# sample successively；Respectively 1# and 9#, 2# and 10# sample being carried out hot strength contrast test according to GB/T3916-2013, measurement result shows that 9# sample is substantially better than 1# sample, and 10# sample is substantially better than 2# sample.
Claims (5)
1. aloe antibiotic yarn, it is characterised in that be made up of regenerated cellulose, Aloe extract, silver zeolite antimicrobial agent；Prepare via following methods: silver zeolite antimicrobial agent is evenly spread in the water added with Aloe extract by (1)；(2) separately take Aloe extract to mix homogeneously with regenerated cellulose viscose, then step (1) gained mixed liquor injected wherein and carry out wet spinning, obtaining aloe antibiotic fiber；(3) the aloe antibiotic fiber utilizing step (2) spins, and obtains aloe antibiotic yarn.
2. aloe antibiotic yarn as claimed in claim 1, it is characterized in that, described step (1) adds 30～60 times of water dissolutioies particularly as follows: take 5～10 weight portion Aloe extracts, is subsequently adding the silver zeolite antimicrobial agent of 0.5～5 weight portions, utilizes high shear dispersion machine to shear dispersion 15～30min.
3. aloe antibiotic yarn as claimed in claim 1 or 2, it is characterised in that in described step (2), the addition of Aloe extract is 0～90 weight portions, and regenerated cellulose is 100 weight portions.
4. aloe antibiotic yarn as claimed in claim 1 or 2, it is characterised in that in described step (2), the addition of Aloe extract is 10～40 weight portions.
5. aloe antibiotic yarn as claimed in claim 1 or 2, it is characterised in that particle diameter≤2.0 μm of described silver zeolite antimicrobial agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410414339.6A CN104153082B (en) | 2014-05-07 | 2014-08-21 | Aloe antibiotic yarn |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2014101900623 | 2014-05-07 | ||
| CN201410190062.3 | 2014-05-07 | ||
| CN201410190062 | 2014-05-07 | ||
| CN201410414339.6A CN104153082B (en) | 2014-05-07 | 2014-08-21 | Aloe antibiotic yarn |
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| CN104153082A CN104153082A (en) | 2014-11-19 |
| CN104153082B true CN104153082B (en) | 2016-08-03 |
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| CN201410414339.6A Expired - Fee Related CN104153082B (en) | 2014-05-07 | 2014-08-21 | Aloe antibiotic yarn |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104988616A (en) * | 2015-05-28 | 2015-10-21 | 安徽省含山县顺天纺织有限公司 | Blending reprocessed cotton yarn capable of emitting anions and being good for health, and preparation method thereof. |
| CN104988618A (en) * | 2015-05-29 | 2015-10-21 | 安徽省含山县顺天纺织有限公司 | Stretch-proofing mekralon blending reprocessed cotton yarn and preparation method thereof |
| CN104963048A (en) * | 2015-05-29 | 2015-10-07 | 安徽省含山县顺天纺织有限公司 | Blending regeneration cotton yarn with ray proof efficacy and preparation method thereof |
| CN105040207A (en) * | 2015-05-29 | 2015-11-11 | 安徽省含山县顺天纺织有限公司 | Industrial polypropylene fiber regenerated cotton blended yarn with flame retardance and preparing method thereof |
| CN107699973A (en) * | 2016-08-24 | 2018-02-16 | 桐乡守敬应用技术研究院有限公司 | A kind of preparation method of antibacterial aloe fiber |
| CN108049204A (en) * | 2017-12-19 | 2018-05-18 | 常熟市沪联印染有限公司 | A kind of antibiotic health care fiber type fabric dyeing |
| CN109338540A (en) * | 2018-11-28 | 2019-02-15 | 湖北中天科技有限公司 | A kind of antibacterial blended yarn and preparation method thereof |
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| CN1779004A (en) * | 2004-11-26 | 2006-05-31 | 新乡化纤股份有限公司 | Antibacterial viscose rayon and production thereof |
| CN101067231A (en) * | 2007-04-28 | 2007-11-07 | 江苏盛虹化纤有限公司 | Antibiotic odourproof fiber |
| CN101935893A (en) * | 2010-08-27 | 2011-01-05 | 山东海龙股份有限公司 | Multifunctional aromatic antibiosis viscose fiber and preparation method thereof |
| CN102926013A (en) * | 2012-11-14 | 2013-02-13 | 单修铎 | Viscose containing natural antimicrobials and preparation method thereof |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008010199A2 (en) * | 2006-07-18 | 2008-01-24 | Nanopeutics S.R.O. | A nanofibre product |
| US20110201578A1 (en) * | 2010-02-14 | 2011-08-18 | Nyangenya Maniga | Composition and methods for the treatment of pseudofolliculitis barbae and skin irritation |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1779004A (en) * | 2004-11-26 | 2006-05-31 | 新乡化纤股份有限公司 | Antibacterial viscose rayon and production thereof |
| CN101067231A (en) * | 2007-04-28 | 2007-11-07 | 江苏盛虹化纤有限公司 | Antibiotic odourproof fiber |
| CN101935893A (en) * | 2010-08-27 | 2011-01-05 | 山东海龙股份有限公司 | Multifunctional aromatic antibiosis viscose fiber and preparation method thereof |
| CN102926013A (en) * | 2012-11-14 | 2013-02-13 | 单修铎 | Viscose containing natural antimicrobials and preparation method thereof |
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Effective date of registration: 20160711 Address after: 453000 north of Heping Avenue, Xinxiang, Henan Applicant after: XINXIANG Fengquan Chemical Fiber Textile Co., Ltd. Address before: 453000, Xinxiang economic and Technological Development Zone, Henan Province, after ten junctions Applicant before: Xinxiang Kanghua Worsted Co., Ltd. |
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