CN104119017A - High-temperature retarding and water reducing agent - Google Patents
High-temperature retarding and water reducing agent Download PDFInfo
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- CN104119017A CN104119017A CN201410294217.8A CN201410294217A CN104119017A CN 104119017 A CN104119017 A CN 104119017A CN 201410294217 A CN201410294217 A CN 201410294217A CN 104119017 A CN104119017 A CN 104119017A
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Abstract
The invention discloses a high-temperature retarding and water reducing agent prepared by mixing the following raw materials in parts by weight: 35-45 parts of polycyclic aromatic hydrocarbon sulfonated formaldehyde condensates, 20-30 parts of acyclic hydroxyl sulfonate condensates, 10-15 parts of diethylenetriaminepenta(methylene-phosphonic acid), 8-16 parts of calcium saccharate, 12-18 parts of alunite powder, 5-10 parts of xanthan gum powder, 4-8 parts of barium metaborate, 3-6 parts of sodium lauryl sulfate, 2-4 parts of pentaerythrite di-n-stearate, 6-12 parts of maleic anhydride-styrene sulfoacid copolymers, 10-15 parts of blast furnace slag powder, 5-10 parts of waste saccharide slag powder, 7-13 parts of nekal and 4-7 parts of auxiliary. The water reducing agent disclosed by the invention is excellent in high temperature resistance, relatively wide in applicable temperature range (150-250 DEG C), capable of reducing cement hydration heat release, reducing the temperature stress of the concrete, avoiding generating temperature cracks and completely meeting the construction requirement for high-temperature and high-pressure well cementation, suitable for continuously pouring mass concrete under a high temperature condition, remarkable in water reducing enhancement effect, good in slump loss resistance and wide in market prospect.
Description
Technical field
The present invention relates to a kind of high temperature modification retardation water reducing agent, belong to concrete admixture field.
Background technology
Concrete admixture, is called for short admixture, refers to before mixing concrete mixing or in mix process, mixes to improve the material of concrete performance.Because admixture can improve concrete performance effectively, and have good economic benefit, be all widely used in many countries, the application in engineering more and more comes into one's own, and becomes material indispensable in concrete.Wherein retardation water reducing agent is the one in concrete admixture, and it can delay concrete coagulating time, makes the fresh concrete long period keep plasticity, convenient cast, improve operating efficiency, can not cause detrimentally affect to later concrete properties simultaneously, and have water-reduction concurrently.The retardation water reducing agent resistance to elevated temperatures deficiency that used in the market, cannot meet High Temperature High Pressure cementing operation needs.
Summary of the invention
To the object of the invention is the defect existing in prior art in order solving, a kind of high temperature modification retardation water reducing agent of resistance to elevated temperatures excellence to be provided, to meet the construction needs of High Temperature High Pressure well cementation.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of high temperature modification retardation water reducing agent, is mixed by the raw material of following weight part: polycyclic aromatic hydrocarbon sulfonate formaldehyde condensation products 35-45, aliphatic hydroxyl sulphonate condenses 20-30, diethylene triamine pentamethylene phosphonic 10-15, sugared calcium 8-16, alum stone flour 12-18, xanthan rubber powder 5-10, barium metaborate 4-8, sodium laurylsulfate 3-6, pentaerythritol stearic acid ester 2 2-4, maleic anhydride-styrene sulfonic acid copolymer 6-12, ground granulated blast furnace slag 10-15, useless sugared ground-slag 5-10, pull open powder 7-13, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: magnesia 10-15, Humic acid Magnesium 3-6, ammonium benzoate 2-4, α-sodium olefin sulfonate 6-12, myo-Inositol hexaphosphate 1.5-2.5, iso-butylene triethoxyl silane 3-5, poly-ferric chloride 5-10, germanite powder 12-18, titanium dioxide 5-10, myristyl glucoside 1-2, polyamide wax 4-6, lithium magnesium silicate 2-3, tea saponin 1.5-2.5;
Above-mentioned magnesia, germanite powder, titanium dioxide are mixed, then add α-sodium olefin sulfonate, iso-butylene triethoxyl silane, polyamide wax, lithium magnesium silicate, under 40-60 DEG C of bath temperature, stir 10-15min, after being cooled to normal temperature, add remaining raw material, stir, dry, obtain described auxiliary agent.
Beneficial effect of the present invention:
Water reducer resistance to elevated temperatures excellence of the present invention, there is wider Applicable temperature scope (150 DEG C-250 DEG C), reduce hydrated cementitious heat release, reduce concrete thermal stress, avoid the generation of thermal cracking, be applicable to the continuous placing of mass concrete under hot conditions, and water reducing and strength-increasing effect is remarkable, slump retaining is good, meets the construction needs of High Temperature High Pressure well cementation completely, has wide market outlook.
Embodiment
A kind of high temperature modification retardation water reducing agent, is mixed by the raw material of following weight (kg): polycyclic aromatic hydrocarbon sulfonate formaldehyde condensation products 35-45, aliphatic hydroxyl sulphonate condenses 20-30, diethylene triamine pentamethylene phosphonic 10-15, sugared calcium 8-16, alum stone flour 12-18, xanthan rubber powder 5-10, barium metaborate 4-8, sodium laurylsulfate 3-6, pentaerythritol stearic acid ester 2 2-4, maleic anhydride-styrene sulfonic acid copolymer 6-12, ground granulated blast furnace slag 10-15, useless sugared ground-slag 5-10, pull open powder 7-13, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: magnesia 10-15, Humic acid Magnesium 3-6, ammonium benzoate 2-4, α-sodium olefin sulfonate 6-12, myo-Inositol hexaphosphate 1.5-2.5, iso-butylene triethoxyl silane 3-5, poly-ferric chloride 5-10, germanite powder 12-18, titanium dioxide 5-10, myristyl glucoside 1-2, polyamide wax 4-6, lithium magnesium silicate 2-3, tea saponin 1.5-2.5;
Above-mentioned magnesia, germanite powder, titanium dioxide are mixed, then add α-sodium olefin sulfonate, iso-butylene triethoxyl silane, polyamide wax, lithium magnesium silicate, under 40-60 DEG C of bath temperature, stir 10-15min, after being cooled to normal temperature, add remaining raw material, stir, dry, obtain described auxiliary agent.
It is as shown in the table that the above-mentioned high temperature modification retardation water reducing agent making mixes salient features detected result in concrete:
Claims (1)
1. a high temperature modification retardation water reducing agent, it is characterized in that, mixed by the raw material of following weight part: polycyclic aromatic hydrocarbon sulfonate formaldehyde condensation products 35-45, aliphatic hydroxyl sulphonate condenses 20-30, diethylene triamine pentamethylene phosphonic 10-15, sugared calcium 8-16, alum stone flour 12-18, xanthan rubber powder 5-10, barium metaborate 4-8, sodium laurylsulfate 3-6, pentaerythritol stearic acid ester 2 2-4, maleic anhydride-styrene sulfonic acid copolymer 6-12, ground granulated blast furnace slag 10-15, useless sugared ground-slag 5-10, pull open powder 7-13, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: magnesia 10-15, Humic acid Magnesium 3-6, ammonium benzoate 2-4, α-sodium olefin sulfonate 6-12, myo-Inositol hexaphosphate 1.5-2.5, iso-butylene triethoxyl silane 3-5, poly-ferric chloride 5-10, germanite powder 12-18, titanium dioxide 5-10, myristyl glucoside 1-2, polyamide wax 4-6, lithium magnesium silicate 2-3, tea saponin 1.5-2.5;
Above-mentioned magnesia, germanite powder, titanium dioxide are mixed, then add α-sodium olefin sulfonate, iso-butylene triethoxyl silane, polyamide wax, lithium magnesium silicate, under 40-60 DEG C of bath temperature, stir 10-15min, after being cooled to normal temperature, add remaining raw material, stir, dry, obtain described auxiliary agent.
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CN201410294217.8A CN104119017A (en) | 2014-06-25 | 2014-06-25 | High-temperature retarding and water reducing agent |
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CN201410294217.8A CN104119017A (en) | 2014-06-25 | 2014-06-25 | High-temperature retarding and water reducing agent |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105481323A (en) * | 2016-02-02 | 2016-04-13 | 金陵科技学院 | Carbon fiber composite concrete and preparation method thereof |
CN105713207A (en) * | 2015-12-31 | 2016-06-29 | 江苏苏博特新材料股份有限公司 | Set-retarding type efficient dispersant and preparation method thereof |
CN106220029A (en) * | 2016-08-08 | 2016-12-14 | 合肥永佳新材料科技有限公司 | A kind of high collapse protection type cement water reducing agent and preparation method thereof |
CN107285654A (en) * | 2017-08-16 | 2017-10-24 | 柳州市天开企业管理有限公司 | A kind of additional water reducer of concrete |
CN107500595A (en) * | 2017-09-22 | 2017-12-22 | 贵州凯襄新材料有限公司 | A kind of water reducer and preparation method thereof |
CN112456827A (en) * | 2020-11-30 | 2021-03-09 | 中国葛洲坝集团水泥有限公司 | Road base retarding cement and preparation method thereof |
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WO1999058465A1 (en) * | 1998-05-12 | 1999-11-18 | Tolsa, S.A. | Technological additive for agglomerating projectable building materials and utilization of the additive in projected mortars and concretes |
CN1634794A (en) * | 2003-12-31 | 2005-07-06 | 吴霖秀 | High efficiency aliphatic sulfonate water reducing agent and method for preparing same |
CN1704371A (en) * | 2004-05-28 | 2005-12-07 | 班俊生 | High performance water-reducing agent of sulfanilate-sulfonated acetone-formaldehyde condensate and process for making same |
CN1887775A (en) * | 2006-07-13 | 2007-01-03 | 内蒙古科技大学 | Efficient retarding and water reducing agent for concrete |
CN102659342A (en) * | 2012-05-14 | 2012-09-12 | 华北水利水电学院 | Retarding superplasticizer composition for roller compacted concrete |
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2014
- 2014-06-25 CN CN201410294217.8A patent/CN104119017A/en active Pending
Patent Citations (5)
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WO1999058465A1 (en) * | 1998-05-12 | 1999-11-18 | Tolsa, S.A. | Technological additive for agglomerating projectable building materials and utilization of the additive in projected mortars and concretes |
CN1634794A (en) * | 2003-12-31 | 2005-07-06 | 吴霖秀 | High efficiency aliphatic sulfonate water reducing agent and method for preparing same |
CN1704371A (en) * | 2004-05-28 | 2005-12-07 | 班俊生 | High performance water-reducing agent of sulfanilate-sulfonated acetone-formaldehyde condensate and process for making same |
CN1887775A (en) * | 2006-07-13 | 2007-01-03 | 内蒙古科技大学 | Efficient retarding and water reducing agent for concrete |
CN102659342A (en) * | 2012-05-14 | 2012-09-12 | 华北水利水电学院 | Retarding superplasticizer composition for roller compacted concrete |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105713207A (en) * | 2015-12-31 | 2016-06-29 | 江苏苏博特新材料股份有限公司 | Set-retarding type efficient dispersant and preparation method thereof |
CN105713207B (en) * | 2015-12-31 | 2019-11-05 | 江苏苏博特新材料股份有限公司 | A kind of retardation setting type dispersant with high efficiency and preparation method thereof |
CN105481323A (en) * | 2016-02-02 | 2016-04-13 | 金陵科技学院 | Carbon fiber composite concrete and preparation method thereof |
CN105481323B (en) * | 2016-02-02 | 2017-12-22 | 金陵科技学院 | A kind of carbon fiber composite concrete and preparation method thereof |
CN106220029A (en) * | 2016-08-08 | 2016-12-14 | 合肥永佳新材料科技有限公司 | A kind of high collapse protection type cement water reducing agent and preparation method thereof |
CN107285654A (en) * | 2017-08-16 | 2017-10-24 | 柳州市天开企业管理有限公司 | A kind of additional water reducer of concrete |
CN107500595A (en) * | 2017-09-22 | 2017-12-22 | 贵州凯襄新材料有限公司 | A kind of water reducer and preparation method thereof |
CN112456827A (en) * | 2020-11-30 | 2021-03-09 | 中国葛洲坝集团水泥有限公司 | Road base retarding cement and preparation method thereof |
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Application publication date: 20141029 |