CN104115928B - Method for preparing dairy gel - Google Patents

Method for preparing dairy gel Download PDF

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Publication number
CN104115928B
CN104115928B CN201310228075.0A CN201310228075A CN104115928B CN 104115928 B CN104115928 B CN 104115928B CN 201310228075 A CN201310228075 A CN 201310228075A CN 104115928 B CN104115928 B CN 104115928B
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dairy products
gel
mixture
dairy
milk
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CN104115928A (en
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朱中亮
郑大青
王德雄
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Food Industry Research and Development Institute
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Food Industry Research and Development Institute
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Abstract

The invention provides a method for preparing dairy gel, which comprises the following steps: mixing a dairy product and a calcium salt to form a mixture, wherein the calcium salt is present in an amount of at least 0.1wt% based on the weight of the dairy product; and subjecting the mixture to a pressurization step to form a dairy gel, wherein the pressurization step comprises applying a pressure of at least 200 MPa. The method for preparing the dairy gel can be carried out at room temperature in the whole process, and the gel mechanism of the dairy is started by the pressure of at least 200MPa, so that the damage to the gel caused by the packaging step in the traditional gel process can be avoided, and the aim of industrial mass production is fulfilled.

Description

The manufacture method of dairy products gel
Technical field
The present invention relates to dairy products gel, more particularly to a kind of manufacture method of dairy products gel.
Background technology
Product made from dairy products gel is set to be derived from GuangZhou, China one with representative tradition using ginger juice or its ferment Dessert, the ginger juice among the people that is referred to as hit milk.It using hot dairy products and ginger juice is main material that its manufacture method, which is, by 70~80 DEG C of raw milk Pour into a certain proportion of ginger juice, acted on protease in ginger juice and hot charge, promote lactoprotein to condense, being formed has such as pudding As sliding tender mouthfeel ginger juice flavor cheese product.
Influence ginger dairy products gel characteristic factor include the curdled milk retention time, ginger juice addition, ester-less milk solid content, The additions such as calcium sulfate.Past research (the influence molecule of Zingibain activity and its trial-production applied to cow's milk gel product, Chen Yan Yu, 2004, animal science research institute of Taiwan Univ. Master's thesis) once pointed out, as retention time, ester-less milk solid contain The increase of amount, ginger juice and calcium sulfate addition, curdled milk consolidation is in conspicuousness increase.Chen Yan Yu (2004) paper is pointed out in 50mL When 2.5mL ginger juice and calcium sulfate containing 30mmol/L and 9% (volume ratio of fructose and cow's milk) fructose are added in cow's milk, at 80 DEG C 20 minutes products for most preference of reaction.
General traditional gel process is after mixing dairy products and calcium sulfate at room temperature, to be stirred heating, reached in temperature Ginger juice is added during to 70~80 DEG C, rapid mixing, gel is stood after dispensing inner wrapping, obtains finished product after cooling.However, due to Curdled milk process can not must stir rapidly and excessively in traditional preparation method, when causing industrialized production, dispense hot dairy products and mixed with ginger juice Closing the agitation of liquid process can damage to colloid, so that the product so far still can not volume production.
Therefore, a kind of improved gel process is needed at present, it can overcome the difficulty that packing is not easy during industrialized production, with Reach the target of volume production.
The content of the invention
In order to solve the above technical problems, the present invention provides a kind of manufacture method of dairy products gel, comprise the following steps:Mixing One dairy products and a calcium salt are to form a mixture, and the content of wherein calcium salt is at least 0.1wt%, on the basis of the weight of dairy products; And a pressurization steps are carried out to mixture to form a dairy products gel, wherein pressurization steps include imposing at least 200MPa pressure Power.
The dairy products include:Defatted dairy, low fat dairy, dairy fat, the product of casein containing protein composition or foregoing group Close.
The dairy products include the milk of mammal, wherein the milk of the mammal includes cow's milk or sheep breast.
The calcium salt includes selecting from one of following edibility calcium salt:Calcium lactate, calcium sulfate, calcium phosphate, calcium carbonate, citric acid Calcium, calcium gluconate or foregoing combination.
The manufacture method of the dairy products gel is also included in ginger juice, the ginger that 0.001~10wt% is added in the mixture Powder, the powder by ginger juice manufacture or isolate or foregoing combination, on the basis of the weight of the dairy products.
The manufacture method of the dairy products gel, also it is included in the sugar that 0.001~15wt% is added in the mixture, with this On the basis of the weight of dairy products.
The manufacture method of the dairy products gel, a packing step is carried out to the mixture before being additionally included in the pressurization steps Suddenly.
All steps of the manufacture method are all completed at 0~40 DEG C.
The pressurization includes imposing 200-600MPa pressure.
The pressurization steps are persistently carried out 1 second to 10 minutes.
It is cited below particularly to go out to be preferable to carry out for above and other objects of the present invention, feature and advantage can be become apparent Example, and coordinate accompanying drawing, it is described in detail below.
Brief description of the drawings
Fig. 1 is the flow chart according to the manufacture method of the dairy products gel of one embodiment of the invention.
Wherein, description of reference numerals is as follows:
100:The manufacture method of dairy products gel
110th, 120,130,140 be specific steps.
Embodiment
The invention provides a kind of technology for starting the generation of dairy products gelatification using HIGH PRESSURE TREATMENT, whole room temperature system It is standby, it can not only simplify industrialized production program, can more realize the target of industrial volume production.
Fig. 1 is according to a kind of manufacture method 100 of dairy products gel of the embodiment of the present invention, step 110 is carried out first, in room Temperature is lower to mix a dairy products and a calcium salt to form a mixture.In certain embodiments, dairy products include:Defatted dairy, low fat milk Product, dairy fat, the product of casein containing protein composition or foregoing combination.In further embodiments, dairy products also include:Lactation The milk of class animal, wherein the milk of the mammal includes cow's milk or sheep breast.It should be noted that in the present invention, breast The protein content and concentration of product are without concentration.In certain embodiments, used calcium salt may include to select under One of row edibility calcium salt:Calcium lactate, calcium sulfate, calcium phosphate, calcium carbonate, calcium citrate, calcium gluconate or foregoing group Close.Wherein, the content of calcium salt is at least 0.1wt%, such as:0.1~0.5wt%, on the basis of the weight of dairy products.
Then, the mixture formed by dairy products and calcium salt is stirred at room temperature.In addition, it is addition dairy products gel products Different flavor, also include a step 120 after step 110,0.001~10wt% is added in mixture, such as:0.001 ~4wt% ginger juice, ginger powder or the powder by ginger juice manufacture or isolate or foregoing combination, on the basis of the weight of dairy products. It should be noted that if making the dairy products gel of original flavor, then step 120 can be omitted;Or, it is possible to use other flavouring agents Substitute the addition of ginger juice, such as:Vanilla or caramel.In certain embodiments, step 120 is also included in mixture and added 0.001~15wt% sugar, such as fructose, sucrose, glucose etc., preferably 0.01~9wt% fructose, with the weight of dairy products On the basis of.Afterwards, a packing step 130 is carried out to mixture.It should be noted that this packing step also can be omitted optionally.
Finally, a pressurization steps 140 are carried out to mixture to form a dairy products gel.This pressurization steps may include to mixing Thing imposes at least 200MPa pressure, such as:200~600MPa, and continue 1 second to 12 minutes, such as:10 minutes, pressure Bigger, the duration can be shorter.In step 140, pressurization steps can refrigerated or carried out at room temperature, and refrigerated storage temperature is for example:0~ 10 DEG C, when mixture is after HIGH PRESSURE TREATMENT, its gel mechanism can be started and promote the formation of dairy products gel products.Compared to biography System gel process must mix rapidly, dispense after dairy products is stood gel, the present invention has been dispensed and finished before dairy products formation gel, Agitation of the traditional handicraft because dispensing step is avoided to destroy caused by colloid.
In the food industry, HIGH PRESSURE TREATMENT technology can be used for the sterilization of food, change food materials character, change enzyme activity Deng.By HIGH PRESSURE TREATMENT Technology application in cheese (cheese), its yield, water content can be increased, prevent from hardening, promote mouthfeel Deng.Past attempts have the cow's milk gel mechanism caused by research and inquirement high pressure, including the protein concentration of cow's milk is improved to 66- 114g/kg, or the total solid amount of cow's milk is more than 25% and in the presence of sucrose, gel is caused with high pressure.It is although preceding State research and can reach the purpose for making cow's milk gel, but need to be just able in the case of higher cow's milk concentration and sucrose are present Complete.
Unless stated otherwise, in the manufacture method of dairy products gel provided by the present invention, all steps all can refrigeration or Complete at room temperature, refrigerated storage temperature is for example:0~10 DEG C, room temperature refer to be more than 10 DEG C be less than or equal to 40 DEG C, but the present invention not with This is limited, as long as the temperature will not make mixture produce the phenomenon of gel, is applied to the present invention.The present invention provides one kind in room The lower mixing dairy products of temperature start the dairy products gel manufacture method of gel with ginger juice and then by pressurization steps.And such as this area skill Art personnel are it is to be understood that the mixture that dairy products provided by the present invention and calcium salt ought be formed at room temperature adds ginger juice simultaneously After mixing, then a heating stepses are implemented to mixture, such technique can not start gel mechanism.And after mixing, packing again Heating stepses are carried out to mixture, can not equally obtain the product of dairy products gel.
It should be noted that Journal of Agricultural and Food Chemistry, 49,3394-3402 (2001) inquired into text for cow's milk gel mechanism caused by pressure, wherein referring to that the total solids content in cow's milk is more than 25% and in the presence of sucrose, cow's milk can be made to produce gel by impressed pressure.In addition, this studies and pointed out, add Excessive calcium chloride (CaCl2) there can be inhibitory action to above-mentioned gelatin phenomenon.However, dairy products gel work provided by the present invention Skill is to use the cow's milk with general total solids content, and in the presence of no sucrose, is opened using pressurization steps Dynamic gel.In addition, with Journal of Agricultural and Food Chemistry, 49,3394-3402 (2001) institute Unlike stating, the calcium salt in the present invention contributes to the generation of gelatin phenomenon.
The manufacture method whole process of dairy products gel provided by the present invention is carried out at room temperature, by an at least 200MPa pressure Power starts the gel mechanism of dairy products, avoids packing step in conventional gel technique and is destroyed to caused by colloid, reaches industrialization The purpose of volume production.In a preferred embodiment, the dairy products gel products formed in the process of the present invention, not only there is good coagulate Colloid, and instant standard is reached, also there is preferably scoring in terms of preference sensory evaluation.
Embodiment
Experiment material and equipment
Material used in the present invention includes:Milk;Ginger juice, ginger is ground into mud, slag, the filter of collection are filtered out using filter towel Liquid is ginger juice;Fructose (good year Fenghe enterprise stock Co., Ltd);Calcium sulfate and calcium lactate (Zhen Fang companies).
One pressurization steps all are carried out to mixture using hydrostatic pressing high voltage processing equipment in the examples below, wherein, add Pressure medium is water.
In the examples below all using texture analyzer (Texture analyzer, TA.XT.plus) to dairy products gel Finished product carries out gellation analysis, and measures its gellation to push maximum, force (g).
The percentage by weight wt% is on the basis of the weight of dairy products in the examples below.
Embodiment 1
High voltage startup gel
Cow's milk is added to 9wt% fructose and different amounts of calcium sulfate at room temperature, with magnetic stirrer 10 minutes, added Enter 5wt% ginger juice and mix, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, with HIGH PRESSURE TREATMENT 3 minutes.As a result as shown in table 1, found after visual observations, it is mixed when not adding calcium sulfate, or when HIGH PRESSURE TREATMENT be less than 200MPa Compound can not gel forming.
Table 1
Calcium sulfate (wt%) 0 0.35 0.5 0.5
Pressure (MPa) 600 600 600 600
Temperature (DEG C) 35 35 35 10
Gellation It can not be molded It is plastic It is plastic It is plastic
Embodiment 2
Ginger juice concentration and gel
Cow's milk is added to 9wt% fructose and 0.5wt% calcium sulfate at room temperature, with magnetic stirrer 10 minutes, point Not Jia Ru different proportion ginger juice and mixing, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, With 600MPa pressure treatment 3 minutes.Found after visual observations, the group for being handled by pressurization steps and adding ginger juice is sent out Raw obvious gelatin phenomenon.Gel strength analysis result is as shown in table 2-1, and after the ginger juice of addition is more than 2wt%, its gel is strong Degree can gradually increase, but when addition increases to more than 4wt%, gel strength is without the trend being further added by.
Table 2-1:Add the gel quality of different proportion ginger juice
Ginger juice (wt%) 2 3 4 5
Gel strength (g) 12.7 26.5 23.9 22
Gellation Shaping is good Shaping is good Shaping is good Shaping is good
Cow's milk is added to 9wt% fructose and 0.5wt% calcium lactates at room temperature, with magnetic stirrer 10 minutes, point Not Jia Ru different proportion ginger juice and mixing, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, With 600MPa pressure treatment 10 minutes.Found through visual observations, the group handled by pressurization steps occurs obvious solidifying Glue phenomenon.Gellation analysis result does not add ginger juice, or 0.05~1wt% of addition as shown in table 2-2 in 100g cow's milk The group of ginger juice, its gellation are quite good.Display carries out a pressurization steps in process, regardless of whether addition ginger juice, The good dairy products gel products of gellation can be prepared.
Table 2-2:Add the gel quality of different proportion ginger juice
Ginger juice (wt%) 0 0.05 0.25 0.5 1
Gellation Shaping is good Shaping is good Shaping is good Shaping is good Shaping is good
Embodiment 3
Calcium concentration and gel
Cow's milk is added to the calcium sulfate of 9wt% fructose and different proportion at room temperature, with magnetic stirrer 10 minutes, 1.3wt% ginger juice and mixing are added, pours into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, with 600MPa pressure treatment is after 3 minutes, and gellation analysis result is as shown in table 3-1.
Table 3-1:Add the gel quality of different calcium sulfate concentrations
Calcium sulfate (wt%) 0.1 0.2 0.3 0.4 0.5
Gellation Shaping is good Shaping is good Shaping is good Shaping is good Shaping is good
Cow's milk is added to the calcium lactate of different proportion at room temperature, does not add fructose, with magnetic stirrer 10 minutes, 4wt% ginger juice and mixing are added, pours into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, with 600MPa pressure treatment is after 10 minutes, and gellation analysis result is as shown in table 3-2.
Table 3-2:Add the gel quality of different lactate concentrations
As shown in table 3-1,3-2, when cow's milk to be added to the calcium sulfate or calcium lactate of different proportion in room temperature, seen through range estimation Found after examining, obvious gelatin phenomenon occurs for all groups handled by pressurization steps.And shown by result, work as addition When 0.1wt% calcium sulfate or calcium lactate, just there is good gelatin phenomenon.
Embodiment 4
Pressure and gel
Cow's milk is added to 0.5wt% calcium lactates at room temperature, does not add fructose, with magnetic stirrer 10 minutes, is added Enter 2wt% ginger juice and mixing, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine.Table 4-1 is The gellation of 3 minutes is handled under different moulding pressures.Found after visual observations, when treated between be 3 minutes when, apply Good gel quality can be obtained by giving 400MPa pressure.
Table 4-1:Different moulding pressures handle the gel quality of 3 minutes
Pressure (MPa) 400 500
Time (min) 3 3
Gellation Shaping is good Shaping is good
Cow's milk is added to 0.5wt% calcium lactates at room temperature, does not add fructose, with magnetic stirrer 10 minutes, is added Enter 4wt% ginger juice, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine.Table 4-2 is in difference Moulding pressure under handle the gellation of 10 minutes.Found after visual observations, when treated between be 10 minutes when, bestow 200MPa pressure can obtain good gel quality.
Table 4-2:Different moulding pressures handle the gel quality of 10 minutes
Embodiment 5
Time and gel
Cow's milk is added to 0.5wt% calcium lactates at room temperature, does not add fructose, with magnetic stirrer 10 minutes, is added Enter 4wt% ginger juice, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine.Table 5-1 be with The gellation of 400MPa pressure treatment different time.Table 5-2 is with the gel journey of 600MPa pressure treatment different time Degree.Found after visual observations, when with 400MPa pressure treatments 1 minute, or with 600MPa pressure treatments 1 second, you can reach To good gel quality.
Table 5-1:The gel quality of different pressing times under 400MPa pressure
Table 5-2:The gel quality of different pressing times under 600MPa pressure
Pressure (MPa) 600 600
Time (sec) 1 10
Gellation Shaping is good Shaping is good
Embodiment 6
Gel ginger milk aerobic plate count
Cow's milk is added to 9wt% fructose and 0.5wt% calcium sulfate at room temperature, with magnetic stirrer 10 minutes, added Enter 5wt% ginger juice and mixing, pour into polyethylene (Polyethylene;PE) in container, and sealed with sealing machine, with 600MPa Pressure treatment 3 minutes.Treat that gel is completed, after finished gel stored under refrigeration one day, take 1mL samples to be serially diluted, it is dilute Release total aerobic plate count that liquid respectively takes 1mL to 3M microbial rapid detections piece (Pertrifilm) (St.Paul, Minnesota, USA) Quick verification test piece (Aerobic Plate Count), and after 35 DEG C are cultivated 48 hours, red colonies are counted, it is each dilute Release to do and repeat twice.Testing result shows that total aerobic plate count of finished gel is less than 20CFU/g, and micro- life can effectively be suppressed by representing it Thing grows, up to instant standard.
In addition, with the product that the method for Chen Yan Yu (2004) paper makes and dairy products gel products provided by the present invention with Preference sensory evaluation compares, and is scored with 9 points of systems, the present invention is using the product made by 600MPa pressure treatments 3 minutes as 8.1 Point, and the product made according to the method for Chen Yan Yu (2004) paper is 6.5 points, shows dairy products gel process provided by the present invention Made product has preferable preference sensory evaluation.
Shown by the above results, according to a kind of manufacture method of dairy products gel of the present invention, its whole process is carried out at room temperature, Containing at least 0.1wt% calcium salt and under bestowing at least 200MPa pressurization steps, regardless of whether addition ginger juice and fructose, The dairy products gel products with good gel quality can be formed.
Although the present invention is disclosed above with several preferred embodiments, so it is not limited to the present invention, any ability Field technique personnel, without departing from the spirit and scope of the present invention, arbitrarily change and retouch when that can make, therefore the guarantor of the present invention Scope is protected when as defined in claim.

Claims (6)

1. a kind of manufacture method of dairy products gel, comprises the following steps:
A dairy products and a calcium salt are mixed to form a mixture, the content of the wherein calcium salt is at least 0.1wt%, with the dairy products On the basis of weight, wherein the step of forming the mixture is completed at 0~40 DEG C, the dairy products are without concentration;With And
0.001~5wt% ginger juice, ginger powder, the powder or isolate or foregoing manufactured by ginger juice is added in the mixture Combination, on the basis of the weight of the dairy products, wherein the calcium salt in the mixture is calcium lactate, carrying out one to the mixture adds Step is pressed to start gel mechanism, to form a dairy products gel, the wherein pressurization steps include the pressure for imposing 200~600MPa; Or 0.001~10wt% ginger juice, ginger powder, the powder or isolate or foregoing manufactured by ginger juice are added in the mixture Combination, on the basis of the weight of the dairy products, wherein the calcium salt in the mixture is calcium sulfate, one is carried out to the mixture Pressurization steps start gel mechanism, and to form a dairy products gel, the wherein pressurization steps include the pressure for imposing 600MPa;
All steps of the manufacture method are all completed at 0~40 DEG C, and the temperature will not make the phenomenon of mixture generation gel.
2. the manufacture method of dairy products gel according to claim 1, wherein the dairy products include:Defatted dairy, low fat milk Product, dairy fat, the product of casein containing protein composition or foregoing combination.
3. the manufacture method of dairy products gel according to claim 1, wherein the dairy products include the milk of mammal, The milk of the mammal includes cow's milk or sheep breast.
4. the manufacture method of dairy products gel according to claim 1,0.001 is added wherein being also included in the mixture ~15wt% sugar, on the basis of the weight of the dairy products.
5. the manufacture method of dairy products gel according to claim 1, wherein being additionally included in before the pressurization steps to described Mixture carries out a packing step.
6. the manufacture method of dairy products gel according to claim 1, wherein the pressurization steps are persistently carried out 1 second to 10 Minute.
CN201310228075.0A 2013-04-25 2013-06-08 Method for preparing dairy gel Active CN104115928B (en)

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KR102425208B1 (en) * 2020-02-24 2022-07-26 안동과학대학교 산학협력단 Method for manufacturing dessert using sweet pumpkin and ginger
CN115530238A (en) * 2021-06-29 2022-12-30 内蒙古伊利实业集团股份有限公司 Solidified ginger milk product and preparation method thereof

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TWI554213B (en) 2016-10-21
JP2014212788A (en) 2014-11-17

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