CN104109624A - Preparation method for germinated tartary buckwheat selenium-rich bamboo shoot vinegar - Google Patents
Preparation method for germinated tartary buckwheat selenium-rich bamboo shoot vinegar Download PDFInfo
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- CN104109624A CN104109624A CN201410342084.7A CN201410342084A CN104109624A CN 104109624 A CN104109624 A CN 104109624A CN 201410342084 A CN201410342084 A CN 201410342084A CN 104109624 A CN104109624 A CN 104109624A
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- bitter buckwheat
- bamboo shoot
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Abstract
The invention provides a preparation method for germinated tartary buckwheat selenium-rich bamboo shoot vinegar. The preparation method is as follows: mixing germinated tartary buckwheat with bamboo shoot for fermentation, wherein amylase, saccharifying enzyme, pectinase, cellulose, brewer yeast and acetic acid bacteria are added in the fermentation process. In the prepared table vinegar, amino acid accounts for 3.8-4.1%, rutin accounts for 0.084-0.118%, gamma-aminobutyric acid accounts for 8-12.5mg/100g, and selenium accounts for 185-250 mu g/L. And therefore, the germinated brown rice asparagus fermented vinegar produced by the method disclosed by the invention has multiple nutritional ingredients, is mellow in flavor and crisp in mouthfeel, and is a vinegar product with good mouthfeel and nutrition and health care effects.
Description
technical field:
The invention belongs to vinegar brewing field, more particularly, the present invention relates to a kind of preparation method of the rich selenium reed of bitter buckwheat bamboo shoot vinegar that germinates.
background technology:
Reed bamboo shoot are that a kind of self-sow is in the wild plant on beach, continent, the middle and lower reach of Yangtze River.Reed bamboo shoot are the tender stem of reed reed, are commonly called as bavin bamboo shoot or asparagus.Reed bamboo shoot are a kind of pure wild natural phant, its production environment is not subject to the pollution of modern industry and mankind's activity, process of growth is not used agricultural chemicals, chemical fertilizer and plant-growth regulator, and be rich in the nutritive ingredients such as the necessary multiple amino acids of human body, trace element and Mierocrystalline cellulose, there is the health-care effecies such as eliminating is greasy, the logical intestines of clearing stomach, weight reducing beauty treatment.Its delicate mouthfeel, delicious meat, boil not rotten, tender and crisp good to eat, unique flavor for a long time, enjoy people's favor, become entertain the guests at a banquet, the good merchantable brand of presenting friends.
Bitter buckwheat is Radix Et Rhizoma Fagopyri Tatarici, formal name used at school
tartarbuckwheat is the king of five cereals.It is the medicine-food two-purpose crop that occurring in nature is very few, according to < <
compendium of Materia Medica> > records: bitter buckwheat bitter, and property is flat cold, the real stomach of energy, beneficial strength, continuous spirit, sharp knowledge, refining the five internal organs slag is dirty.Bitter buckwheat integrates seven major nutrient, have remarkable healthy nutritive value and outstanding dietotherapy effect, can calm the nerves, the swollen wind pain of lively atmosphere blood, the wide intestines of sending down abnormally ascending, heat-clearing, long-pendingization of dispelling are stagnant, gut purge, ease constipation, defaecation, cough-relieving, relieving asthma, the effect such as anti-inflammatory, antianaphylaxis, cardiac stimulant, fat-reducing, beauty treatment.Especially the main component rutin in Tartary buckwheat biological flavonoid (claiming again vitamin P), has vessel softening, improves microcirculation, clearing heat and detoxicating, promoting blood circulation and removing blood stasis, toxin expelling myogenic, hypoglycemic, glucose in urine, blood fat, beneficial air lift god, strengthen Regular Insulin peripheral action, so also claim " three fall food ".
Selenium is the trace element of needed by human.Selenium participates in the interior multiple selenoenzyme of synthesized human and contains seleno-protein.Wherein
selenoperoxidase, in vivo catalysis hydroperoxide or
lipid peroxidechange water or various alcohols into, eliminate the biomembranous attack of radical pair, protection microbial film is avoided oxidative damage.
Now, existing correlative study person develops bitter buckwheat vinegar, for example: Chinese Patent Application No. CN20120046603.6 " bitter buckwheat vinegar and production method thereof " etc.What study is all to utilize without the bitter buckwheat germinateing and the vinegar of multiple other material mixed fermentations, and material composition is complicated, and mouthfeel and nutrient composition content are difficult to control.By retrieving domestic and international prior art, find, also not take at present the report that bitter buckwheat and reed bamboo shoot are major ingredient fermented vinegar that germinates.
Summary of the invention
The object of the invention is to provide a kind of production technique of the rich selenium reed of bitter buckwheat bamboo shoot vinegar that germinates.The present invention adopts germinate bitter buckwheat and the mixed fermentation of reed bamboo shoot, the enzyme that enriches that takes full advantage of during the fermentation raw material is, the composition of health-care effect is fully incorporated in vinegar, both mouthfeel and the local flavor of vinegar had been improved, the health-care effect of having strengthened again the bitter buckwheat reed bamboo shoot vinegar that germinates, significantly promotes the health-care effect of vinegar and quality.
The germinate preparation method of the rich selenium reed of bitter buckwheat bamboo shoot vinegar, is characterized in that it is prepared according to the following steps:
(1) select bitter buckwheat, bitter buckwheat is put into the sodium selenite solution of 25mg/L, the thermostat water bath that is placed in 30 ℃ of temperature soaks 12h.Then the growth hormone of lotus seeds being put into 450mg/L soaks 18-20h, under 30-35 ℃ of constant temperature culture condition, cultivates germination, makes the bitter buckwheat that germinates, and by the bitter buckwheat colloidal mill defibrination that germinates, cooled and filtered, obtains selenium-rich germinated bitter buckwheat juice.
(2) get selenium-rich germinated bitter buckwheat juice that reed bamboo shoot fresh, that cleaned obtain with step (1) in mass ratio 1:1 mix, use colloidal mill defibrination, in slurries, add 2-4 doubly to the water of dry material, by mix the amylase 0.40-0.50 g/kg that adds enzyme 10000U/g alive with the weight ratio (g/Kg) of raw material, the saccharifying enzyme 0.30-0.60 g/kg of enzyme 8000 U/g alive, the polygalacturonase 0.15-0.20g/kg of enzyme 12000U/g alive, the cellulase 0.10-0.15 g/kg of enzyme 6000 U/g alive, under 40 ℃ of conditions, enzymolysis is 15 hours;
(3), in the mixed solution obtaining to step (2), by adding yeast saccharomyces cerevisiae 0.40-0.55 g/kg with the weight ratio (g/Kg) of raw material, be placed in 33-36 ℃ of condition bottom fermentation and within 8 days, obtain distiller's wort;
(4) ferment in complete distiller's wort, by adding acetic bacteria 0.50-0.60g/kg with the weight ratio (g/Kg) of raw material, under 30-33 ℃ of condition, adopt solid state fermentation 7 days;
(5) fermented liquid that step (4) obtained is centrifugal, filtration, sterilizing obtain clear liquor, then dilutes, packs, and bitter buckwheat reed bamboo shoot vinegar can obtain germinateing.
Preferably, the preparation method of the rich selenium reed of the bitter buckwheat of germination as above bamboo shoot vinegar, wherein the yeast saccharomyces cerevisiae described in step (3) is yeast saccharomyces cerevisiae CICC1027.
Preferably, the preparation method of the rich selenium reed of the bitter buckwheat of germination as above bamboo shoot vinegar, wherein the acetic bacteria described in step (4) is acetic bacteria CICC21870.
The present invention is with respect to the existing processing technology of vinegar, and tool has the following advantages:
(1) take at present germinate bitter buckwheat and reed bamboo shoot is the production method of waste fermentation vinegar, and the rich selenium reed of the bitter buckwheat of the germination that the present invention produces bamboo shoot vinegar, the excellent flavor not only with reed bamboo shoot, and due to the distinctive functional property of bitter buckwheat of germinateing, make the vinegar that the present invention produces be more suitable for " three height " edible for patients.
(2) adopt solid fermentating mode, utilizing the enzyme that enriches of germinate bitter buckwheat and reed bamboo shoot glycolysis generation is to make raw material glycolysis more
Add fully, product special flavour is mellow, and mouthfeel acid is refreshing.Aminoacids content 3.8-4.1% in the vinegar making, rutin content 0.094-0.118%, alpha-aminobutyric acid content 8-12.5mg/100g, selenium content 185-250ug/L, has guaranteed nutritive ingredient abundant in vinegar, has strengthened its health-care effect.
Embodiment
Be below specific embodiments of the invention, technical scheme of the present invention is done to further description, but protection scope of the present invention is not limited to these embodiment.Every do not deviate from the change of the present invention design or be equal to substitute include within protection scope of the present invention.
embodiment 1
(1) select bitter buckwheat 120kg, bitter buckwheat is put into the sodium selenite solution of 25mg/L, the thermostat water bath that is placed in 30 ℃ of temperature soaks 12h.Then the growth hormone of lotus seeds being put into 450mg/L soaks 18h, under 30 ℃ of constant temperature culture conditions, cultivates germination, makes the bitter buckwheat that germinates, and by the bitter buckwheat colloidal mill defibrination that germinates, cooled and filtered, obtains selenium-rich germinated bitter buckwheat juice.
(2) get reed bamboo shoot 120kg fresh, that cleaned, after mixing with the bitter buckwheat of the resulting germination of step (1), use colloidal mill defibrination, in slurries, add 480kg water, by mixing with the weight ratio (g/Kg) of raw material, add amylase (enzyme 10000U/g alive) 0.40g/kg, saccharifying enzyme (enzyme 8000 U/g alive) 0.30 g/kg, polygalacturonase (enzyme 12000U/g alive) 0.15g/kg, cellulase (enzyme 6000 U/g alive) 0.10g/kg, under 40 ℃ of conditions, enzymolysis is 15 hours.
(3), in the resulting mixed solution of step (2), by adding yeast saccharomyces cerevisiae (CICC1027) 0.40g/kg with the weight ratio (g/Kg) of raw material, be placed in 33 ℃ of condition bottom fermentations and within 8 days, obtain distiller's wort.
(4) in the complete distiller's wort of fermentation, by adding acetic bacteria (CICC21870) 0.50g/kg with the weight ratio (g/Kg) of raw material, under 30 ℃ of conditions, adopt solid state fermentation 7 days.
(5) fermented liquid of acquisition is centrifugal, filtration, sterilizing obtain clear liquor, then dilute, pack, and bitter buckwheat reed bamboo shoot vinegar can obtain germinateing.
embodiment 2
(1) select bitter buckwheat 150kg, bitter buckwheat is put into the sodium selenite solution of 25mg/L, the thermostat water bath that is placed in 30 ℃ of temperature soaks 12h.Then the growth hormone of lotus seeds being put into 450mg/L soaks 20h, under 35 ℃ of constant temperature culture conditions, cultivates germination, makes the bitter buckwheat that germinates, and by the bitter buckwheat colloidal mill defibrination that germinates, cooled and filtered, obtains selenium-rich germinated bitter buckwheat juice.
(2) get reed bamboo shoot 150kg fresh, that cleaned, and the bitter buckwheat of the resulting germination of step (1) mixes the rear colloidal mill defibrination of using, in slurries, add 1200kg water, by mixing with the weight ratio (g/Kg) of raw material, add amylase (enzyme 10000U/g alive) 0.50 g/kg, saccharifying enzyme (enzyme 8000 U/g alive) 0.60 g/kg, polygalacturonase (enzyme 12000U/g alive) 0.20g/kg, cellulase (enzyme 6000U/g alive) 0.15 g/kg, under 40 ℃ of conditions, enzymolysis is 15 hours.
(3), in the resulting mixed solution of step (2), by adding yeast saccharomyces cerevisiae (CICC1027) 0.55 g/kg with the weight ratio (g/Kg) of raw material, be placed in 36 ℃ of condition bottom fermentations and within 8 days, obtain distiller's wort.
(4) in the complete distiller's wort of fermentation, by adding acetic bacteria (CICC21870) 0.60g/kg with the weight ratio (g/Kg) of raw material, under 33 ℃ of conditions, adopt solid state fermentation 7 days.
(5) fermented liquid obtaining is centrifugal, to filter, sterilizing obtains clear liquor, then dilutes, packs, and bitter buckwheat reed bamboo shoot vinegar can obtain germinateing.
comparative example 1
Supplementary material kind, the fermentation condition in interpolation quantity, order of addition and each stage that this embodiment is used with embodiment 1 are all identical, only in comparative example, bitter buckwheat are not carried out to germination treatment.
comparative example 2
In this embodiment, do not use various corresponding zymins, lack amylase, saccharifying enzyme, polygalacturonase, cellulase in example 2, all the other steps are all identical with example 2.
comparative example 3
this embodiment compares with embodiment 1, does not use raw material reed bamboo shoot, and all the other steps are all identical with embodiment 1.
comparative example 4
This embodiment compares with embodiment 2, does not carry out rich selenium, and all the other steps are all identical with embodiment 2.
The bitter buckwheat reed of germination prepared by embodiment of the present invention 1-2 and comparative example 1-4 bamboo shoot vinegar, its attributional analysis is as following table:
Table 1 embodiment attributional analysis table
。
Claims (3)
1. the germinate preparation method of the rich selenium reed of bitter buckwheat bamboo shoot vinegar, is characterized in that: the method comprises the following steps:
(1) select bitter buckwheat, bitter buckwheat is put into the sodium selenite solution of 25mg/L, the thermostat water bath that is placed in 30 ℃ of temperature soaks 12h;
Then the growth hormone of lotus seeds being put into 450mg/L soaks 18-20h, under 30-35 ℃ of constant temperature culture condition, cultivates germination, makes the bitter buckwheat that germinates, and by the bitter buckwheat colloidal mill defibrination that germinates, cooled and filtered, obtains selenium-rich germinated bitter buckwheat juice;
(2) choose reed bamboo shoot fresh, that cleaned, with the bitter buckwheat juice of the germination of step (1) gained in mass ratio 1:1 mix, use colloidal mill defibrination, in slurries, add 2-4 doubly to the water of dry material, by mix the amylase 0.40-0.50 g/kg that adds enzyme 10000U/g alive with the weight ratio (g/Kg) of raw material, the saccharifying enzyme 0.30-0.60 g/kg of enzyme 8000 U/g alive, the polygalacturonase 0.15-0.20g/kg of enzyme 12000U/g alive, the cellulase 0.10-0.15 g/kg of enzyme 6000 U/g alive, under 40 ℃ of conditions, enzymolysis is 15 hours;
(3), in the mixed solution obtaining in step (2), by adding yeast saccharomyces cerevisiae 0.40-0.55 g/kg with the weight ratio (g/Kg) of raw material, be placed in 33-36 ℃ of condition bottom fermentation and within 8 days, obtain distiller's wort;
(4) in the complete distiller's wort of fermentation, by adding acetic bacteria 0.50-0.60g/kg with the weight ratio (g/Kg) of raw material, under 30-33 ℃ of condition, adopt solid state fermentation 7 days;
(5) fermented liquid that step (4) obtained is centrifugal, filtration, sterilizing obtain clear liquor, then dilutes, packs, and bitter buckwheat reed bamboo shoot vinegar can obtain germinateing.
2. according to the preparation method of the rich selenium reed of the bitter buckwheat of germination claimed in claim 1 bamboo shoot vinegar, it is characterized in that: the described yeast saccharomyces cerevisiae of step (3) is yeast saccharomyces cerevisiae CICC1027.
3. according to the preparation method of the rich selenium reed of the bitter buckwheat of germination claimed in claim 1 bamboo shoot vinegar, it is characterized in that: the described acetic bacteria of step (4) is acetic bacteria CICC21870.
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| CN201410342084.7A CN104109624B (en) | 2014-07-18 | 2014-07-18 | A kind of preparation method of bitter buckwheat rich selenium reed bamboo shoot vinegar that germinates |
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| CN201410342084.7A CN104109624B (en) | 2014-07-18 | 2014-07-18 | A kind of preparation method of bitter buckwheat rich selenium reed bamboo shoot vinegar that germinates |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2013005779A (en) * | 2011-06-27 | 2013-01-10 | Q P Corp | Vegetable vinegar and processed food using the same |
| CN103087895A (en) * | 2013-01-05 | 2013-05-08 | 水城县满全农业开发有限公司 | Tartary buckwheat vinegar submerged fermentation process |
| CN103351997A (en) * | 2013-07-14 | 2013-10-16 | 山西银杏食品科技有限公司 | Selenium-enriched vinegar preparation method |
| CN103734836A (en) * | 2014-01-28 | 2014-04-23 | 程健博 | Method for preparing germinated black tartary buckwheat and hawthorn fruit vinegar beverage |
-
2014
- 2014-07-18 CN CN201410342084.7A patent/CN104109624B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2013005779A (en) * | 2011-06-27 | 2013-01-10 | Q P Corp | Vegetable vinegar and processed food using the same |
| CN103087895A (en) * | 2013-01-05 | 2013-05-08 | 水城县满全农业开发有限公司 | Tartary buckwheat vinegar submerged fermentation process |
| CN103351997A (en) * | 2013-07-14 | 2013-10-16 | 山西银杏食品科技有限公司 | Selenium-enriched vinegar preparation method |
| CN103734836A (en) * | 2014-01-28 | 2014-04-23 | 程健博 | Method for preparing germinated black tartary buckwheat and hawthorn fruit vinegar beverage |
Non-Patent Citations (1)
| Title |
|---|
| 申瑞玲等: "苦荞醋发酵工艺条件的优化", 《郑州轻工业学院学报》, vol. 29, no. 1, 28 February 2014 (2014-02-28), pages 29 - 33 * |
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Effective date of registration: 20201119 Address after: No.8, yangqueba group, yangqueba village, wuyangba sub district office, Enshi Tujia and Miao Autonomous Prefecture, Hubei Province Patentee after: ENSHI XISHENG PLANT TECHNOLOGY Co.,Ltd. Address before: 430068 Wuchang City, Wuhan Province, South Lake, Li Jia Dun village, No. 1, No., No. 1 Patentee before: HUBEI University OF TECHNOLOGY |
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