CN104109500B - A kind of tackiness agent and preparation method thereof - Google Patents
A kind of tackiness agent and preparation method thereof Download PDFInfo
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- CN104109500B CN104109500B CN201410325234.3A CN201410325234A CN104109500B CN 104109500 B CN104109500 B CN 104109500B CN 201410325234 A CN201410325234 A CN 201410325234A CN 104109500 B CN104109500 B CN 104109500B
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- 238000002360 preparation method Methods 0.000 title abstract description 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 72
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims abstract description 42
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims abstract description 42
- 229940043265 methyl isobutyl ketone Drugs 0.000 claims abstract description 42
- -1 tert butyl phenolic resin Chemical compound 0.000 claims abstract description 35
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 229920013649 Paracril Polymers 0.000 claims abstract description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 23
- 230000003712 anti-aging effect Effects 0.000 claims abstract description 22
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 22
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229920001568 phenolic resin Polymers 0.000 claims abstract description 22
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 21
- 239000008367 deionised water Substances 0.000 claims abstract description 21
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 21
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 21
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000005011 phenolic resin Substances 0.000 claims abstract description 21
- 229920002635 polyurethane Polymers 0.000 claims abstract description 21
- 239000004814 polyurethane Substances 0.000 claims abstract description 21
- 239000008117 stearic acid Substances 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims description 28
- 239000011259 mixed solution Substances 0.000 claims description 7
- 229920001971 elastomer Polymers 0.000 abstract description 19
- 239000005060 rubber Substances 0.000 abstract description 19
- 239000000463 material Substances 0.000 abstract description 9
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000006866 deterioration Effects 0.000 abstract description 3
- 239000013536 elastomeric material Substances 0.000 abstract description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 description 9
- 239000000853 adhesive Substances 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 229920003051 synthetic elastomer Polymers 0.000 description 3
- 239000005061 synthetic rubber Substances 0.000 description 3
- 244000043261 Hevea brasiliensis Species 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
- 229920003052 natural elastomer Polymers 0.000 description 2
- 229920001194 natural rubber Polymers 0.000 description 2
- 229920001084 poly(chloroprene) Polymers 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- OWRCNXZUPFZXOS-UHFFFAOYSA-N 1,3-diphenylguanidine Chemical compound C=1C=CC=CC=1NC(=N)NC1=CC=CC=C1 OWRCNXZUPFZXOS-UHFFFAOYSA-N 0.000 description 1
- KPAPHODVWOVUJL-UHFFFAOYSA-N 1-benzofuran;1h-indene Chemical compound C1=CC=C2CC=CC2=C1.C1=CC=C2OC=CC2=C1 KPAPHODVWOVUJL-UHFFFAOYSA-N 0.000 description 1
- WJQOZHYUIDYNHM-UHFFFAOYSA-N 2-tert-Butylphenol Chemical compound CC(C)(C)C1=CC=CC=C1O WJQOZHYUIDYNHM-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 229920000800 acrylic rubber Polymers 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000036314 physical performance Effects 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- KZVVGZKAVZUACK-BJILWQEISA-N rilpivirine hydrochloride Chemical compound Cl.CC1=CC(\C=C\C#N)=CC(C)=C1NC1=CC=NC(NC=2C=CC(=CC=2)C#N)=N1 KZVVGZKAVZUACK-BJILWQEISA-N 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- RKQOSDAEEGPRER-UHFFFAOYSA-L zinc diethyldithiocarbamate Chemical compound [Zn+2].CCN(CC)C([S-])=S.CCN(CC)C([S-])=S RKQOSDAEEGPRER-UHFFFAOYSA-L 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The present invention relates to field of rubber technology, refer more particularly to a kind of tackiness agent and preparation method thereof, described tackiness agent comprises the raw material of following weight part: aqueous polyurethane 50-100 parts, tert butyl phenolic resin 50-100 parts, paracril 100 parts, 5-15 parts, magnesium oxide, 5-15 parts, diatomite, methyl iso-butyl ketone (MIBK) 100-150, stearic acid 3-8 parts, 1-5 parts, solidifying agent, catalyzer 1-5 parts, 1-5 parts, anti-aging agent, deionized water 300-400 parts.The present invention fills a prescription rationally, and making method is simple, and cohesiveness is very strong, high with rubber item cohesive strength, long service life; What the present invention adopted is the raw material close with rubber item Material texture, does not change the character of material, undergoes no deterioration, make elastomeric material more safe and reliable in use after rubber item is bonding.
Description
Technical field
The present invention relates to field of rubber technology, refer more particularly to a kind of tackiness agent and preparation method thereof.
Background technology
Rubber is a kind of elastomerics, not only has significant snappiness at normal temperatures, and can have this character in very large-temperature range, and deformability can reach several times.Rubber based adhesives is with the tackiness agent of rubber taste base-material configuration, and nearly all natural rubber and synthetic rubber may be used to configure tackiness agent, according to the composition of rubber base-material, can be divided into natural rubber adhesive and the large class of synthetic rubber tackiness agent two.The kind that synthetic rubber tackiness agent is conventional has chloroprene rubber, paracril, styrene-butadiene rubber(SBR), silicon rubber etc.
Chinese patent 201310620265.7 discloses a kind of rubber based adhesives, it is characterized in that, described rubber based adhesives comprises the component of following portions by weight: chloroprene rubber 20-120, paracril 30-90, urethanes 20-60, acrylic elastomer 20-60, nano zine oxide 2-10, potter's clay 1-4, carbon black N10015-50, coumarone indene resin 2-12, diatomite 4-15, sulphur 2-10, anti-aging agent 1-5, tertiary butyl phenol formaldehyde resin 1-8, machine oil 1-6, magnesium oxide 1-3, white carbon black 1-5, scorch retarder 1-5, dibutyl phthalate 1-4, zinc diethyldithiocarbamate 1-4, 2-thiol group tetrahydroglyoxaline 1-4, vulkacit D 1-10.This invention rubber based adhesives snappiness is good, has the characteristics such as excellent resistance to creep, flex endurant and shock-resistant vibrations, can be applicable between different linear expansivity material and the splicing of the parts dynamically used or goods.But this invention cost is high, and tensile strength is weak, differences in viscosity, poor with the cohesive strength of rubber seal.
Summary of the invention
It is low that technical problem to be solved by this invention is to provide a kind of cost, good physical performance, and cohesive strength is good, simple tackiness agent of making method and preparation method thereof.
For solving the problems of the technologies described above, the present invention by the following technical solutions:
A making method for tackiness agent, comprises the following steps:
(1) take raw material by weight, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 120-130 DEG C under vacuo, stir 1-1.5 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent, stir 30-50 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Preferably, the making method of described tackiness agent, step (1) comprises the raw material of following weight part: aqueous polyurethane 50-100 parts, tert butyl phenolic resin 50-100 parts, paracril 100 parts, 5-15 parts, magnesium oxide, 5-15 parts, diatomite, methyl iso-butyl ketone (MIBK) 100-150 parts, stearic acid 3-8 parts, 1-5 parts, solidifying agent, catalyzer 1-5 parts, 1-5 parts, anti-aging agent, deionized water 300-400 parts.
Preferably, the making method of described tackiness agent, step (1) comprises the raw material of following weight part: aqueous polyurethane 50-80 parts, tert butyl phenolic resin 50-80 parts, paracril 100 parts, 5-10 parts, magnesium oxide, 5-10 parts, diatomite, methyl iso-butyl ketone (MIBK) 100-150 parts, stearic acid 5-8 parts, 1-3 parts, solidifying agent, catalyzer 1-3 parts, 1-3 parts, anti-aging agent, deionized water 300-400 parts.
Preferably, the making method of described tackiness agent, step (1) comprises the raw material of following weight part: aqueous polyurethane 70 parts, tert butyl phenolic resin 80 parts, paracril 100 parts, 8 parts, magnesium oxide, 8 parts, diatomite, methyl iso-butyl ketone (MIBK) 100 parts, stearic acid 6 parts, 2 parts, solidifying agent, catalyzer 2 parts, 2 parts, anti-aging agent, deionized water 300 parts.
Preferably, the making method of described tackiness agent, step (1) comprises the raw material of following weight part: aqueous polyurethane 100 parts, tert butyl phenolic resin 100 parts, paracril 100 parts, 12 parts, magnesium oxide, 14 parts, diatomite, methyl iso-butyl ketone (MIBK) 150 parts, stearic acid 8 parts, 6 parts, solidifying agent, catalyzer 6 parts, 3 parts, anti-aging agent, deionized water 400 parts.
Compared with prior art, the present invention has the following advantages:
(1) the present invention fills a prescription rationally, and making method is simple, and cohesiveness is very strong, high with rubber item cohesive strength, long service life;
(2) what the present invention adopted is the raw material close with rubber item Material texture, does not change the character of material, undergoes no deterioration, make elastomeric material more safe and reliable in use after rubber item is bonding.
Embodiment
Below in conjunction with embodiment, technical scheme of the present invention is further described in detail.
Embodiment one:
A kind of tackiness agent, is characterized in that, comprise the raw material of following weight part: aqueous polyurethane 70 parts, tert butyl phenolic resin 80 parts, paracril 100 parts, 8 parts, magnesium oxide, 8 parts, diatomite, methyl iso-butyl ketone (MIBK) 100 parts, stearic acid 6 parts, 2 parts, solidifying agent, catalyzer 2 parts, anti-aging agent Tenox PG 2 parts, deionized water 300 parts;
The making method of described tackiness agent, is characterized in that, comprises the following steps:
(1) take described each raw material by described weight part, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 130 DEG C under vacuo, stir 1.5 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent Tenox PG, stir 50 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Tensile strength of the present invention is 3.5MPa, and tensile yield is 1520%, and bonding strength is 226.2N/50mm.
Embodiment two:
A kind of tackiness agent, is characterized in that, comprise the raw material of following weight part: aqueous polyurethane 100 parts, tert butyl phenolic resin 100 parts, paracril 100 parts, 12 parts, magnesium oxide, 14 parts, diatomite, methyl iso-butyl ketone (MIBK) 150 parts, stearic acid 8 parts, 6 parts, solidifying agent, catalyzer 6 parts, 3 parts, anti-aging agent, deionized water 400 parts;
The making method of described tackiness agent, is characterized in that, comprises the following steps:
(1) take described each raw material by described weight part, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 129 DEG C under vacuo, stir 1.4 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent Tenox PG, stir 45 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Tensile strength of the present invention is 3.8MPa, and tensile yield is 1480%, and bonding strength is 232N/50mm.
Embodiment three:
A kind of tackiness agent, is characterized in that, comprise the raw material of following weight part: aqueous polyurethane 50 parts, tert butyl phenolic resin 50 parts, paracril 100 parts, 5 parts, magnesium oxide, 5 parts, diatomite, methyl iso-butyl ketone (MIBK) 120 parts, stearic acid 3 parts, 1 part, solidifying agent, catalyzer 1 part, anti-aging agent Tenox PG 1 part, deionized water 320 parts;
The making method of described tackiness agent, is characterized in that, comprises the following steps:
(1) take described each raw material by described weight part, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 120 DEG C under vacuo, stir 1 hour;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent Tenox PG, stir 30 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Tensile strength of the present invention is 3.2MPa, and tensile yield is 1500%, and bonding strength is 208.5N/50mm.
Embodiment four:
A kind of tackiness agent, is characterized in that, comprise the raw material of following weight part: aqueous polyurethane 80 parts, tert butyl phenolic resin 70 parts, paracril 100 parts, 15 parts, magnesium oxide, 15 parts, diatomite, methyl iso-butyl ketone (MIBK) 140 parts, stearic acid 5 parts, 4 parts, solidifying agent, catalyzer 4 parts, anti-aging agent Tenox PG 4 parts, deionized water 360 parts;
The making method of described tackiness agent, is characterized in that, comprises the following steps:
(1) take described each raw material by described weight part, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 125 DEG C under vacuo, stir 1.3 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent Tenox PG, stir 40 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Tensile strength of the present invention is 3.4MPa, and tensile yield is 1450%, and bonding strength is 220N/50mm.
Embodiment five:
A kind of tackiness agent, is characterized in that, comprise the raw material of following weight part: aqueous polyurethane 60 parts, tert butyl phenolic resin 90 parts, paracril 100 parts, 10 parts, magnesium oxide, 10 parts, diatomite, methyl iso-butyl ketone (MIBK) 130 parts, stearic acid 6 parts, 3 parts, solidifying agent, catalyzer 3 parts, anti-aging agent Tenox PG 3 parts, deionized water 320 parts;
The making method of described tackiness agent, is characterized in that, comprises the following steps:
(1) take described each raw material by described weight part, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 123 DEG C under vacuo, stir 1-1.5 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent Tenox PG, stir 35 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
Tensile strength of the present invention is 3.2MPa, and tensile yield is 1540%, and bonding strength is 230.5N/50mm.
The present invention has the following advantages: the present invention fills a prescription rationally, and making method is simple, and cohesiveness is very strong, high with rubber item cohesive strength, long service life; What the present invention adopted is the raw material close with rubber item Material texture, does not change the character of material, undergoes no deterioration, make elastomeric material more safe and reliable in use after rubber item is bonding.
It should be noted last that, above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted, although with reference to preferred embodiment to invention has been detailed description, those of ordinary skill in the art is to be understood that, can modify to technical scheme of the present invention or equivalent replacement, and not departing from the spirit and scope of technical solution of the present invention, it all should be encompassed in the middle of right of the present invention.
Claims (5)
1. a making method for tackiness agent, is characterized in that, comprises the following steps:
(1) take raw material by weight, the aqueous polyurethane of calculated amount, tert butyl phenolic resin, paracril are added in the deionized water of calculated amount, stirs, be heated to 120-130 DEG C under vacuo, stir 1-1.5 hours;
(2) in the mixed solution of step (1) gained, add magnesium oxide, diatomite, stearic acid, solidifying agent, catalyzer, anti-aging agent, stir 30-50 minutes, then add methyl iso-butyl ketone (MIBK) and stir.
2. the making method of tackiness agent according to claim 1, is characterized in that, step (1) comprises the raw material of following weight part: aqueous polyurethane 50-100 parts, tert butyl phenolic resin 50-100 parts, paracril 100 parts, 5-15 parts, magnesium oxide, 5-15 parts, diatomite, methyl iso-butyl ketone (MIBK) 100-150 parts, stearic acid 3-8 parts, 1-5 parts, solidifying agent, catalyzer 1-5 parts, 1-5 parts, anti-aging agent, deionized water 300-400 parts.
3. the making method of tackiness agent according to claim 1, is characterized in that, step (1) comprises the raw material of following weight part: aqueous polyurethane 50-80 parts, tert butyl phenolic resin 50-80 parts, paracril 100 parts, 5-10 parts, magnesium oxide, 5-10 parts, diatomite, methyl iso-butyl ketone (MIBK) 100-150 parts, stearic acid 5-8 parts, 1-3 parts, solidifying agent, catalyzer 1-3 parts, 1-3 parts, anti-aging agent, deionized water 300-400 parts.
4. the making method of tackiness agent according to claim 1, is characterized in that, step (1) comprises the raw material of following weight part: aqueous polyurethane 70 parts, tert butyl phenolic resin 80 parts, paracril 100 parts, 8 parts, magnesium oxide, 8 parts, diatomite, methyl iso-butyl ketone (MIBK) 100 parts, stearic acid 6 parts, 2 parts, solidifying agent, catalyzer 2 parts, 2 parts, anti-aging agent, deionized water 300 parts.
5. the making method of tackiness agent according to claim 1, is characterized in that, step (1) comprises the raw material of following weight part: aqueous polyurethane 100 parts, tert butyl phenolic resin 100 parts, paracril 100 parts, 12 parts, magnesium oxide, 14 parts, diatomite, methyl iso-butyl ketone (MIBK) 150 parts, stearic acid 8 parts, 6 parts, solidifying agent, catalyzer 6 parts, 3 parts, anti-aging agent, deionized water 400 parts.
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| CN201410325234.3A CN104109500B (en) | 2014-07-08 | 2014-07-08 | A kind of tackiness agent and preparation method thereof |
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| CN201410325234.3A CN104109500B (en) | 2014-07-08 | 2014-07-08 | A kind of tackiness agent and preparation method thereof |
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| CN104109500B true CN104109500B (en) | 2015-11-18 |
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| CN105542686A (en) * | 2016-02-17 | 2016-05-04 | 广西大学 | Environment-friendly high-strength binder and preparing method thereof |
| CN106590116A (en) * | 2016-12-18 | 2017-04-26 | 钦州市科学技术开发中心 | Building UV (ultra violet) paint and preparation method thereof |
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| CN104109500A (en) | 2014-10-22 |
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Denomination of invention: A type of adhesive and its manufacturing method Granted publication date: 20151118 Pledgee: China Construction Bank Corporation Ningguo sub branch Pledgor: ANHUI JINGHONG SEALING ELEMENT TECHNOLOGY Co.,Ltd. Registration number: Y2024980037975 |
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