CN104083991A - Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid - Google Patents

Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid Download PDF

Info

Publication number
CN104083991A
CN104083991A CN201410292218.9A CN201410292218A CN104083991A CN 104083991 A CN104083991 A CN 104083991A CN 201410292218 A CN201410292218 A CN 201410292218A CN 104083991 A CN104083991 A CN 104083991A
Authority
CN
China
Prior art keywords
ammonia
ammonia gas
tourie
water
emptying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410292218.9A
Other languages
Chinese (zh)
Inventor
李久玉
周军
赵以辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Huaihua Co Ltd
Original Assignee
Anhui Huaihua Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Huaihua Co Ltd filed Critical Anhui Huaihua Co Ltd
Priority to CN201410292218.9A priority Critical patent/CN104083991A/en
Publication of CN104083991A publication Critical patent/CN104083991A/en
Pending legal-status Critical Current

Links

Landscapes

  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

The invention discloses a device for recycling ammonia gas in a refrigerating unit with liquid ammonia serving as a refrigerating fluid. The recovery device comprises a cylindrical ammonia gas absorption tank, wherein the diameter of the upper part of the ammonia gas absorption tank is smaller than that of the lower part of the ammonia gas absorption tank; an ammonia emptying inlet and an ammonium water outlet are formed in the middle of the ammonia gas absorption tank; the ammonia emptying inlet is connected with an ammonia gas outlet of the refrigerating unit through a pipeline; a spraying water inlet is formed above the ammonium water outlet; the ammonium water outlet is connected to an underground ammonia water storage tank through a pipeline. In an actual application process, if the pressure of the unit exceeds the standard or other accidents occur, ammonia gas emptied after a unit safety valve is on is recycled into the ammonia gas absorption tank which is mainly filled with water, the ammonia gas and the water are mixed to form ammonium water, and the ammonium water is recycled by virtue of the ammonia gas absorption tank, so that the ammonia gas can be recycled in the accident state, the phenomena that the environment is influenced and the surrounding environment is polluted due to emptying of ammonia gas into the atmosphere are prevented, an operator is prevented from security threat, and the aims of safety, environmental protection, circular economy are achieved.

Description

Liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid
Technical field
The present invention relates to liquefied ammonia and make the retracting device of ammonia in the freezing unit of freezing liquid.
Background technology
Chilled water required in synthesis gas preparing ethylene glycol device is mostly from freezing unit, the freezing liquid of freezing unit is liquefied ammonia, it is the freezing liquid that current freezing unit is generally used that liquefied ammonia is done freezing liquid, because liquefied ammonia economy, but in actual application, if run into system overhaul or unit pressure exceeds standard or occurs under the state of other accidents, unit safety valve can take-off, gas ammonia emptying after take-off, thus caused environmental pollution and field personnel's personal safety has been formed to threat.
Summary of the invention
The present invention does freezing liquid freezing unit for solving existing liquefied ammonia in application process, runs into system overhaul or unit pressure exceeds standard or occurs the problem that other contingencies cause ammonia to be revealed, and the retracting device of ammonia in the freezing unit that a kind of liquefied ammonia does freezing liquid is provided.
Liquefied ammonia of the present invention is made the retracting device of ammonia in the freezing unit of freezing liquid, comprise that upper diameter is less than the cylindricality ammonia tourie of lower diameter, medium position at described ammonia tourie is provided with ammonia emptying import and ammoniacal liquor outlet, and described ammonia emptying import connects the ammonia outlet of freezing unit by pipeline; Above described ammoniacal liquor outlet, be provided with shower water import; Described ammoniacal liquor outlet is connected to the underground storage tank of ammoniacal liquor by pipeline.
Described ammonia emptying import department is connected with the Inserting Tube that gos deep into ammonia tourie bottom, and the termination of described Inserting Tube is provided with several Inserting Tube jet pipes, and described Inserting Tube jet pipe is provided with several spray orifices.
Described shower water import department is connected with the shower that gos deep into ammonia tourie inside, and described shower is provided with several spray apertures.
The bottom surface of described ammonia tourie is inclined-plane, on the ammonia tourie near lower position place, described inclined-plane, is provided with discharging hole.
Ammonia tourie principle of the present invention, is by freezing unit discharge ammonia, by pipeline, enters into ammonia tourie, by the Inserting Tube in ammonia tourie, by the jet pipe of Inserting Tube end opening, ammonia is discharged in water again, utilizes the high-dissolvability of ammonia in water, allow the fast reaction of gas ammonia and water, generate ammoniacal liquor, utilize the outlet of ammonia tourie, ammoniacal liquor by automatic overflow to the underground storage tank of ammoniacal liquor, thereby the ammoniacal liquor of absorption can be delivered to ammonia water tank to sell, reduce industrial cost; Ammonia tourie of the present invention is suitable for reading also designs a set of spray water system, utilize the even spray of shower water, allow gas ammonia in water, there is no the ammonia dissolving, in the process of spray, dissolve gas ammonia completely, and spray water system is returned the good supplementing water of ammonia tourie.Low cost of manufacture of the present invention, high efficiency, makes simple, using environment-friendly; The ammonia that fully emptying in the state of accident of absorption refrigerating unit is replaced to the liquefied ammonia of atmosphere with when the system overhaul, effectively preventing that gas ammonia emptying is to air, impact is operating environment around, when affecting operating personnel's safety, also ammonia has been carried out to recycling, lowered industrial cost.
In actual application, if unit pressure exceeds standard or occurs under the state of other accidents, after the take-off of unit safety valve, the gas ammonia of emptying will be recovered to ammonia tourie, in ammonia tourie, be mainly water, gas ammonia and water mix, form ammoniacal liquor, utilize ammonia tourie, reclaim ammoniacal liquor, thereby realized in the state of accident, reclaimed gas ammonia, prevented that gas ammonia emptying from affecting environment and polluting surrounding environment to atmosphere, avoid the security threat to operating personnel, played the object of safety, environmental protection and recycling economy.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
In figure: 2, freezing unit; 3, ammonia tourie; 4, liquid level gauge; 5, ammonia emptying import; 51, Inserting Tube; 52, Inserting Tube jet pipe; 6, shower water import; 7, ammoniacal liquor outlet; 8, manhole; 9, discharging hole; 10, the underground storage tank of ammoniacal liquor; 11, inclined-plane; 12, shower.
The specific embodiment
As shown in Figure 1, liquefied ammonia of the present invention is made the retracting device of ammonia in the freezing unit of freezing liquid, comprise that upper diameter is less than the cylindricality ammonia tourie 3 of lower diameter, medium position at ammonia tourie 3 is provided with ammonia emptying import 5 and ammoniacal liquor outlet 7, and ammonia emptying import 5 connects the ammonia outlet of freezing unit 2 by pipeline; Above ammoniacal liquor outlet 7, be provided with shower water import 6; Ammoniacal liquor outlet 7 is connected to the underground storage tank 10 of ammoniacal liquor by pipeline; Ammonia emptying import 5 places are connected with the Inserting Tube 51 that gos deep into ammonia tourie 3 bottoms, and the termination of Inserting Tube 51 is provided with several Inserting Tube jet pipes 52, and Inserting Tube jet pipe 52 is provided with several spray orifices; Shower water import 6 places are connected with the shower 12 that gos deep into ammonia tourie 3 inside, and shower 12 is provided with several spray apertures; The bottom surface of ammonia tourie 3 is inclined-plane 11, on the ammonia tourie 3 near 11 lower position places, described inclined-plane, is provided with discharging hole 9.
Ammonia tourie principle of the present invention, is by freezing unit discharge ammonia, by pipeline, enters into ammonia tourie, by the Inserting Tube in ammonia tourie, by the jet pipe of Inserting Tube end opening, ammonia is discharged in water again, utilizes the high-dissolvability of ammonia in water, allow the fast reaction of gas ammonia and water, generate ammoniacal liquor, utilize the outlet of ammonia tourie, ammoniacal liquor by automatic overflow to the underground storage tank of ammoniacal liquor, thereby the ammoniacal liquor of absorption can be delivered to ammonia water tank to sell, reduce industrial cost; Ammonia tourie of the present invention is suitable for reading also designs a set of spray water system, utilize the even spray of shower water, allow gas ammonia in water, there is no the ammonia dissolving, in the process of spray, dissolve gas ammonia completely, and spray water system is returned the good supplementing water of ammonia tourie.Low cost of manufacture of the present invention, high efficiency, makes simple, using environment-friendly; The ammonia that fully emptying in the state of accident of absorption refrigerating unit is replaced to the liquefied ammonia of atmosphere with when the system overhaul, effectively preventing that gas ammonia emptying is to air, impact is operating environment around, when affecting operating personnel's safety, also ammonia has been carried out to recycling, lowered industrial cost.

Claims (4)

1. liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid, it is characterized in that, comprise that upper diameter is less than the cylindricality ammonia tourie (3) of lower diameter, medium position at described ammonia tourie (3) is provided with ammonia emptying import (5) and ammoniacal liquor outlet (7), and described ammonia emptying import (5) connects the ammonia outlet of freezing unit (2) by pipeline; Top in described ammoniacal liquor outlet (7) is provided with shower water import (6); Described ammoniacal liquor outlet (7) is connected to the underground storage tank of ammoniacal liquor (10) by pipeline.
2. liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid as claimed in claim 1, it is characterized in that, described ammonia emptying import (5) locates to be connected with the Inserting Tube (51) that gos deep into ammonia tourie (3) bottom, and the termination of described Inserting Tube (51) is provided with several Inserting Tube jet pipes (52), and described Inserting Tube jet pipe (52) is provided with several spray orifices.
3. liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid as claimed in claim 1, it is characterized in that, described shower water import (6) is located to be connected with and is goed deep into the inner shower (12) of ammonia tourie (3), and described shower (12) is provided with several spray apertures.
4. liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid as claimed in claim 1, it is characterized in that, the bottom surface of described ammonia tourie (3) is inclined-plane (11), on the ammonia tourie (3) near lower position place, described inclined-plane (11), is provided with discharging hole (9).
CN201410292218.9A 2014-06-26 2014-06-26 Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid Pending CN104083991A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410292218.9A CN104083991A (en) 2014-06-26 2014-06-26 Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410292218.9A CN104083991A (en) 2014-06-26 2014-06-26 Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid

Publications (1)

Publication Number Publication Date
CN104083991A true CN104083991A (en) 2014-10-08

Family

ID=51631809

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410292218.9A Pending CN104083991A (en) 2014-06-26 2014-06-26 Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid

Country Status (1)

Country Link
CN (1) CN104083991A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107303458A (en) * 2016-04-19 2017-10-31 五冶集团上海有限公司 Pressure Vessels Ammonia Leak Testing residual gas recycling device
CN108120189A (en) * 2017-11-13 2018-06-05 舒沿钦 A kind of absorption type refrigerating agent retracting device
CN108332458A (en) * 2018-03-26 2018-07-27 河南开祥精细化工有限公司 The ammonia recycling device of ammonia refrigeration system
CN110665337A (en) * 2018-07-03 2020-01-10 山东恒昌圣诚化工股份有限公司 Ammonia tail gas recovery device

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1258556A (en) * 1999-12-01 2000-07-05 上海交通大学 Equipment and method to exhaust nitridation waste gas and recover residual ammonia
JP4169234B2 (en) * 1999-07-22 2008-10-22 株式会社前川製作所 Simple ammonia removal device for air-conditioning ammonia refrigerator
CN203155674U (en) * 2013-04-08 2013-08-28 郑明成 Ammonia gas absorption machine for blueprint machine
CN203990251U (en) * 2014-06-26 2014-12-10 安徽淮化股份有限公司 Liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4169234B2 (en) * 1999-07-22 2008-10-22 株式会社前川製作所 Simple ammonia removal device for air-conditioning ammonia refrigerator
CN1258556A (en) * 1999-12-01 2000-07-05 上海交通大学 Equipment and method to exhaust nitridation waste gas and recover residual ammonia
CN203155674U (en) * 2013-04-08 2013-08-28 郑明成 Ammonia gas absorption machine for blueprint machine
CN203990251U (en) * 2014-06-26 2014-12-10 安徽淮化股份有限公司 Liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107303458A (en) * 2016-04-19 2017-10-31 五冶集团上海有限公司 Pressure Vessels Ammonia Leak Testing residual gas recycling device
CN108120189A (en) * 2017-11-13 2018-06-05 舒沿钦 A kind of absorption type refrigerating agent retracting device
CN108332458A (en) * 2018-03-26 2018-07-27 河南开祥精细化工有限公司 The ammonia recycling device of ammonia refrigeration system
CN110665337A (en) * 2018-07-03 2020-01-10 山东恒昌圣诚化工股份有限公司 Ammonia tail gas recovery device

Similar Documents

Publication Publication Date Title
CN203990251U (en) Liquefied ammonia is made the retracting device of ammonia in the freezing unit of freezing liquid
CN104083991A (en) Device for recycling ammonia gas in refrigerating unit with liquid ammonia serving as refrigerating fluid
CN206439633U (en) A kind of fire-proof and explosion-proof hydrogen sulfide air accumulator
CN202607482U (en) Water circulation system with filtering net
CN204056838U (en) A kind of ammoniacal liquor safety tanks
CN206091913U (en) Stifled mixed fire fighting equipment of operation liquid water disposal is separated in oil field efflux sand washing
CN208019075U (en) A kind of high-pressure rubber pipe energy-saving washing device
CN204312994U (en) Natural gas production pipeline hydrops recovery unit
CN202590581U (en) Defogger adapted to changes in gas flow
CN104261150B (en) Discharge system for ammonium nitrate tank car
CN208907031U (en) A kind of liquefied ammonia is from press mounting vehicle system
CN206203875U (en) A kind of fuel charger petroleum vapor recovery detection means
CN203187385U (en) Liquid recovery system
CN106402439A (en) Automatic exhaust valve
CN201404616Y (en) Low-pressure fine water fog fire extinguishing system
CN202066019U (en) Molecule sealer used in torch discharging system
CN202933804U (en) Foam hydraulic giant
CN205155561U (en) Ethylene spherical tank cools off pressure reduction means
CN104383790A (en) Technology for reducing noise and ammonia content generated during discharging process of CO2 stripping process urea device
CN206970198U (en) A kind of gas station oil gas retracting device with electrostatic-proof function
CN203816512U (en) Ammonia storeroom accident spray water recovering system of SCR denitration device
CN204543951U (en) Ammonia treating apparatus
CN102878425B (en) Device for avoiding liquid layering in liquefied natural gas storage tank
CN104214519A (en) Method and device for preventing high-pressure and low-pressure flare gas channeling of gas inlet cabinet
CN208869521U (en) A kind of heptafluoro-propane recyclable device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C12 Rejection of a patent application after its publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20141008