CN104082851A - Tobacco adhesive and preparing method and application thereof - Google Patents
Tobacco adhesive and preparing method and application thereof Download PDFInfo
- Publication number
- CN104082851A CN104082851A CN201410319783.XA CN201410319783A CN104082851A CN 104082851 A CN104082851 A CN 104082851A CN 201410319783 A CN201410319783 A CN 201410319783A CN 104082851 A CN104082851 A CN 104082851A
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- tobacco
- binder
- adhesive
- pulullan
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Abstract
The invention discloses a tobacco adhesive and a preparing method and application thereof. The tobacco adhesive is composed of a pullulan and water solution with the mass concentration of 0.5-5% (W/V). The tobacco adhesive and tobacco leftovers are evenly mixed according to the mass ratio of 1:1-100, air dying is conducted for 0.5-18 hours under the condition of 25-50 DEG C, the mixture is then rolled into a sheet, and a tobacco sheet is obtained. The tobacco adhesive is safe, non-toxic and harmless and has good adhesion performance, the quality of original tobacco can be maintained when the tobacco adhesive is applied to preparing the tobacco sheet, and the tobacco adhesive is novel.
Description
Technical field
The present invention relates to tobacco binder preparing technical field, relate in particular to a kind of adhesive that the tobacco powder of cigar mill or tobacco leftovers are laminated and preparation method thereof and application.
Background technology
In the production process of cigarette, can produce 3～8% leftover bits and pieces, as offal, crumbled tobacco, offal etc.In order to make full use of raw material, save production cost, after being pulverized, these tobacco leftovers mix a kind of adhesive, and be processed into reconstituted tobacoo by roll-in method, and then be cut into pipe tobacco.The use of this regeneration tobacco leaf has improved utilization ratio of tobacco, has improved economic benefit.In the production process of reconstituted tobacoo, adhesive and technical process are all crucial.There is the tobacco binder of report taking chitin as base-material before, add CMS and wood pulp cellulose, and a small amount of glycerine and phosphoric acid, manufacture craft is comparatively complicated, and this adhesive regenerated cut tobacco of making to produce to inhale taste not good, in pipe tobacco combustion process, irritant smell produces.
Pulullan is a kind ofly to have another name called Pul, pullulan by the ferment outer water-soluble cement polysaccharide of born of the same parents of the similar glucan that produces, xanthans of Aureobasidium pullulans, English name Pullulan, and transliteration is Propiram.It is a kind of special microbial polysaccharide of being found by R.Bauer for 1938.This polysaccharide is mainly to pass through α-1 by maltotriose, and 6 glycosidic bonds are formed by connecting.Due to structure and the character of this polysaccharide uniqueness, be with a wide range of applications in industries such as medicine, food, oil, chemical industry.Because it is in the nature utilization that can be degraded by microorganisms, can not cause environmental pollution, therefore be described as nuisanceless plastics.On May 19th, 2006, health ministry has been issued bulletin No. 8, and pulullan, for one of newly-increased four kinds of food additives products, can be used as fruit glaze agent and thickener in candy, chocolate-coated, diaphragm, compound seasoner and fruit-vegetable juice beverage.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of natural safe, nontoxic, has good adhesion and can keep the tobacco binder of original cigarette quality.
For solving the problems of the technologies described above, technical scheme of the present invention is: tobacco binder is 0.5～5%(W/V by mass concentration) the pulullan aqueous solution form.
Preferably, described pulullan is microorganism fermentation source, and molecular mass is 100000～1000000Da, taking mass fraction purity as 80～99%.
The present invention also provides the preparation method of above-mentioned tobacco binder, and method is as follows: by ultra-pure water stirring and dissolving under 30～70 DEG C of conditions for described pulullan, can make described tobacco binder.
The present invention also provides the application of above-mentioned tobacco binder in reconstituted tobacoo preparation, by even according to mass ratio 1:1～100 mix to described tobacco binder and tobacco leftovers, air-dry 0.5～18h under 25～50 DEG C of conditions, is then rolled into thin slice, can make reconstituted tobacoo.
Wherein, described tobacco leftovers is offal, crumbled tobacco and/or offal.
Owing to having adopted technique scheme, tobacco binder, is 0.5～5%(W/V by mass concentration) the pulullan aqueous solution form; By even according to mass ratio 1:1～100 mix to described tobacco binder and tobacco leftovers, air-dry 0.5～18h under 25～50 DEG C of conditions, is then rolled into thin slice, can make reconstituted tobacoo; The present invention has following beneficial effect: pulullan has very strong bonding force, also there is stronger coagulation force, there is good overlay film simultaneously, easily at the face coat such as food, metal, simultaneously, can form easy solubization, water white transparency, tough film by the pulullan aqueous solution, it has gas barrier property, keeps the characteristics such as armaticity, oil resistivity, electrical insulating property.Product of the present invention is natural safe, nontoxic, has good adhesion, when being applied to reconstituted tobacoo and preparing, can keep the quality of original tobacco.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further.
embodiment 1
Take 5g pulullan, be dissolved in 100mL ultra-pure water, under 40 DEG C of conditions, stir 2h, obtain tobacco binder;
Get the tobacco leftovers uniform mixing of 100g tobacco binder and 1kg, air-dry 10h under 40 DEG C of conditions, is then rolled into thin slice, makes reconstituted tobacoo.
embodiment 2
Take 1g pulullan, be dissolved in 100mL ultra-pure water, under 50 DEG C of conditions, stir 1h, obtain tobacco binder;
Get the tobacco leftovers uniform mixing of 100g tobacco binder and 0.5kg, air-dry 6h under 30 DEG C of conditions, is then rolled into thin slice, makes reconstituted tobacoo.
embodiment 3
Take 0.5g pulullan, be dissolved in 100mL ultra-pure water, under 30 DEG C of conditions, stir 50min, obtain tobacco binder;
Get the tobacco leftovers uniform mixing of 100g tobacco binder and 10kg, air-dry 3h under 30 DEG C of conditions, is then rolled into thin slice, makes reconstituted tobacoo.
embodiment 4
Take 2g pulullan, be dissolved in 100mL ultra-pure water, under 70 DEG C of conditions, stir 30min, obtain tobacco binder;
Get the tobacco leftovers uniform mixing of 100g tobacco binder and 10kg, air-dry 4h under 50 DEG C of conditions, is then rolled into thin slice, makes reconstituted tobacoo.
The foregoing is only the schematic detailed description of the invention of the present invention, not in order to limit scope of the present invention.Any those skilled in the art, not departing from equivalent variations and the amendment done under the prerequisite of design of the present invention and principle, all should belong to the scope of protection of the invention.
Claims (6)
1. tobacco binder, is characterized in that: be 0.5～5%(W/V by mass concentration) the pulullan aqueous solution form.
2. tobacco binder as claimed in claim 1, is characterized in that: the molecular mass of described pulullan is 100000～1000000Da, and being calculated in mass percent purity is 80～99%.
3. the preparation method of tobacco binder as claimed in claim 1 or 2, is characterized in that: by ultra-pure water stirring and dissolving under 30～70 DEG C of conditions for described pulullan, make described tobacco binder.
4. the preparation method of tobacco binder as claimed in claim 3, is characterized in that: the molecular mass of described pulullan is 100000～1000000Da, and being calculated in mass percent purity is 80～99%.
5. the application of tobacco binder as claimed in claim 1 or 2 in reconstituted tobacoo preparation, it is characterized in that: by even according to mass ratio 1:1～100 mix to described tobacco binder and tobacco leftovers, air-dry 0.5～18h under 25～50 DEG C of conditions, then be rolled into thin slice, make reconstituted tobacoo.
6. the application of tobacco binder as claimed in claim 5 in reconstituted tobacoo preparation, is characterized in that: described tobacco leftovers is offal, crumbled tobacco and/or offal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410319783.XA CN104082851A (en) | 2014-07-08 | 2014-07-08 | Tobacco adhesive and preparing method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410319783.XA CN104082851A (en) | 2014-07-08 | 2014-07-08 | Tobacco adhesive and preparing method and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104082851A true CN104082851A (en) | 2014-10-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410319783.XA Pending CN104082851A (en) | 2014-07-08 | 2014-07-08 | Tobacco adhesive and preparing method and application thereof |
Country Status (1)
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| CN (1) | CN104082851A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104745119A (en) * | 2014-12-25 | 2015-07-01 | 天津北洋百川生物技术有限公司 | Solid binder and preparation method thereof |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
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| US4018233A (en) * | 1974-02-05 | 1977-04-19 | Sumitomo Chemical Company Limited | Shaped matters of tobaccos and process for producing the same |
| CN1988815A (en) * | 2004-07-29 | 2007-06-27 | 布朗及威廉森控股公司 | Flavoring a cigarette by using a flavored filter plug wrap |
| US20090208559A1 (en) * | 2006-06-14 | 2009-08-20 | Bruce Drew | Device for delivering active ingredients to humans, animals and plants |
| CN101795710A (en) * | 2007-05-16 | 2010-08-04 | 麦克内尔股份公司 | Oral nicotine formulation buffered with amino acid |
| CN101862024A (en) * | 2010-06-07 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablets containing tobacco components |
| CN102432921A (en) * | 2011-09-16 | 2012-05-02 | 中国烟草总公司郑州烟草研究院 | Pullulan additive and application thereof in cigarettes |
| CN102499451A (en) * | 2011-10-11 | 2012-06-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablet smokeless tobacco product added with sea-buckthorn preparation |
| CN103005668A (en) * | 2007-07-23 | 2013-04-03 | R.J.雷诺兹烟草公司 | Smokeless tobacco compositions and methods for treating tobacco for use therein |
| CN103015175A (en) * | 2012-12-06 | 2013-04-03 | 张家口卷烟厂有限责任公司 | Pullulan polysaccharide modified polypropylene (PP) fiber for cigarette and preparation method thereof |
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2014
- 2014-07-08 CN CN201410319783.XA patent/CN104082851A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4018233A (en) * | 1974-02-05 | 1977-04-19 | Sumitomo Chemical Company Limited | Shaped matters of tobaccos and process for producing the same |
| CN1988815A (en) * | 2004-07-29 | 2007-06-27 | 布朗及威廉森控股公司 | Flavoring a cigarette by using a flavored filter plug wrap |
| US20090208559A1 (en) * | 2006-06-14 | 2009-08-20 | Bruce Drew | Device for delivering active ingredients to humans, animals and plants |
| CN101795710A (en) * | 2007-05-16 | 2010-08-04 | 麦克内尔股份公司 | Oral nicotine formulation buffered with amino acid |
| CN103005668A (en) * | 2007-07-23 | 2013-04-03 | R.J.雷诺兹烟草公司 | Smokeless tobacco compositions and methods for treating tobacco for use therein |
| CN101862024A (en) * | 2010-06-07 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablets containing tobacco components |
| CN102432921A (en) * | 2011-09-16 | 2012-05-02 | 中国烟草总公司郑州烟草研究院 | Pullulan additive and application thereof in cigarettes |
| CN102499451A (en) * | 2011-10-11 | 2012-06-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablet smokeless tobacco product added with sea-buckthorn preparation |
| CN103015175A (en) * | 2012-12-06 | 2013-04-03 | 张家口卷烟厂有限责任公司 | Pullulan polysaccharide modified polypropylene (PP) fiber for cigarette and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104745119A (en) * | 2014-12-25 | 2015-07-01 | 天津北洋百川生物技术有限公司 | Solid binder and preparation method thereof |
| CN104745119B (en) * | 2014-12-25 | 2017-07-21 | 天津北洋百川生物技术有限公司 | Solid binder and preparation method thereof |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
| US11878079B2 (en) | 2017-04-14 | 2024-01-23 | Capsugel Belgium Nv | Pullulan capsules |
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Application publication date: 20141008 |