CN104059385B - The preparation method of yellow dyes - Google Patents
The preparation method of yellow dyes Download PDFInfo
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- CN104059385B CN104059385B CN201410297620.6A CN201410297620A CN104059385B CN 104059385 B CN104059385 B CN 104059385B CN 201410297620 A CN201410297620 A CN 201410297620A CN 104059385 B CN104059385 B CN 104059385B
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Abstract
The present invention discloses a kind of preparation method of yellow dyes, belongs to field of printing and dyeing.Ox-hide is put into pot by the present invention, adds water and is boiled into ox-hide cream, for subsequent use; The pulp of wolfberry fruit and pericarp are removed, collects its seed grain, and put into soybean milk maker, add water, pulverize, pour out, remove slag, by remaining solution left standstill, go upper solution, retain lower floor's sediment; Lower floor's sediment put into soybean milk maker, adds water, pulverize, pour out, leave standstill, go upper solution, retain lower floor's sediment, continue to repeat several times, until the granularity of the lower floor's sediment obtained reaches 50 nanometer ~ 100 nanometers; Obtained lower floor's sediment is mixed with obtained ox-hide cream, makes the yellow dyes of required form.Orchil institute dyeing and weaving thing, the soft nature of dress ornament color and luster that the present invention obtains, colour fastness is higher, not easily fades, variable color, harmless, is a kind of environmental protection, natural dyestuff.
Description
Technical field
The invention belongs to field of printing and dyeing, particularly relate to a kind of preparation method of yellow dyes.
Background technology
At present, conventional dyestuff is synthetic dyestuff, and its dyeing and weaving thing, dress ornament etc. not only easily cause and fade, and mostly belongs to carinogenicity material, not only contaminate environment due to its raw material, intermediate, also directly makes wearer, contactee or the producer be injured.
Along with improving constantly of standard of living, people more and more pay close attention to self health, pursue green product and green consumption becomes trend.Therefore, a kind of environmental protection, natural, harmless dyestuff are by the synthetic dyestuff conventional alternative past.
Wolfberry fruit, is the mature fruit of matrimony vine of solanaceae plant or lycium barbarum, plucks when summer, autumn fruit maturation, removing carpopodium, puts after shady and cool place dries in the air and corrugate to pericarp, then be exposed to the sun stiff to crust, pulp is soft and get final product.Generally, wolfberry fruit brings into medicinal, not yet has the report brought and prepare dyestuff.
Summary of the invention
The invention provides a kind of preparation method of yellow dyes, orchil institute dyeing and weaving thing, the soft nature of dress ornament color and luster that this preparation method obtains, colour fastness is higher, not easily fades, variable color, harmless, is a kind of environmental protection, natural dyestuff.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
A preparation method for yellow dyes, the method comprises the following steps:
A, ox-hide is put into pot, add water and be boiled into paste, obtain ox-hide cream, for subsequent use;
B, the pulp of wolfberry fruit and pericarp to be removed, collect its seed grain, and put into soybean milk maker, add 1 ~ 3 times of water, pulverize 15 minutes ~ 20 minutes, pour out, remove slag, by remaining solution left standstill 1 hour ~ 3 hours, go upper solution, retain lower floor's sediment;
C, step B lower floor sediment put into soybean milk maker, add 1 ~ 3 times of water, pulverize 30 minutes ~ 40 minutes, pour out, leave standstill 1 hour ~ 3 hours, go upper solution, retain lower floor's sediment;
D, continuation repeat step C, until the granularity of the lower floor's sediment obtained reaches 50 nanometer ~ 100 nanometers;
Lower floor's sediment that E, in mass ratio D step obtain: described lower floor sediment mixes with described ox-hide cream by the ratio of ox-hide cream=1:0.01 ~ 0.1 that step A obtains, and makes the yellow dyes of required form.
Owing to adopting technique scheme, the beneficial effect that the present invention obtains is:
The present invention is prepared from using wolfberry fruit as main raw material, in its whole preparation process, unharmful substance adds, harmful waste is not had to produce yet, its obtained orchil is harmless, contaminate fabric, dress ornament in yellow, color even, the soft nature of color and luster, colour fastness is higher, not easily fades, variable color.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described, and protection scope of the present invention is not only confined to following examples.
Embodiment 1
The preparation method of this yellow dyes comprises the following steps:
A, ox-hide is put into pot, add water and be boiled into paste, obtain ox-hide cream, for subsequent use;
B, the pulp of wolfberry fruit and pericarp to be removed, collect its seed grain, and put into soybean milk maker, add 2 times of water, pulverize 15 minutes, pour out, remove slag, by remaining solution left standstill 3 hours, go upper solution, retain lower floor's sediment;
C, step B lower floor sediment is put into soybean milk maker, adds 2 times of water, pulverize 30 minutes, pour out, 3 hours, go upper solution, retain lower floor's sediment;
D, continuation repeat step C, until the granularity of the lower floor's sediment obtained reaches 100 nanometers;
The ox-hide cream that E, the lower floor's sediment and the 0.05kgA step that 1kgD step are obtained obtain mixes, and is then pressed into block yellow dyes.
Yellow dyes obtained for the present embodiment is used for contaminate clothing clothes, then contaminate clothes is carried out cleaning, soaking, find its cleaning, soak after waste water still clarify, colourless, the clothes color after cleaning, immersion is unchanged.
Embodiment 2
The preparation method of this yellow dyes comprises the following steps:
A, ox-hide is put into pot, add water and be boiled into paste, obtain ox-hide cream, for subsequent use;
B, the pulp of wolfberry fruit and pericarp to be removed, collect its seed grain, and put into soybean milk maker, add 1 times of water, pulverize 20 minutes, pour out, remove slag, by remaining solution left standstill 1 hour, go upper solution, retain lower floor's sediment;
C, step B lower floor sediment put into soybean milk maker, add 1 times of water, pulverize 40 minutes, pour out, leave standstill 1 hour, go upper solution, retain lower floor's sediment;
D, continuation repeat step C, until the granularity of the lower floor's sediment obtained reaches 50 nanometers;
The ox-hide cream that E, the lower floor's sediment and the 0.1kgA step that 1kgD step are obtained obtain mixes, and add water stirring, obtained aqueous yellow dyes.
Yellow dyes obtained for the present embodiment is used for contaminate clothing clothes, then contaminate clothes is carried out cleaning, soaking, find its cleaning, soak after waste water still clarify, colourless, the clothes color after cleaning, immersion is unchanged.
Embodiment 3
The preparation method of this yellow dyes comprises the following steps:
A, ox-hide is put into pot, add water and be boiled into paste, obtain ox-hide cream, for subsequent use;
B, the pulp of wolfberry fruit and pericarp to be removed, collect its seed grain, and put into soybean milk maker, add 3 times of water, pulverize 17 minutes, pour out, remove slag, by remaining solution left standstill 2 hours, go upper solution, retain lower floor's sediment;
C, step B lower floor sediment put into soybean milk maker, add 3 times of water, pulverize 36 minutes, pour out, leave standstill 2 hours, go upper solution, retain lower floor's sediment;
D, continuation repeat step C, until the granularity of the lower floor's sediment obtained reaches 80 nanometers;
The ox-hide cream that E, the lower floor's sediment and the 0.01kgA step that 1kgD step are obtained obtain mixes, and is then pressed into block yellow dyes.
Yellow dyes obtained for the present embodiment is used for contaminate clothing clothes, then contaminate clothes is carried out cleaning, soaking, find its cleaning, soak after waste water still clarify, colourless, the clothes color after cleaning, immersion is unchanged.
Claims (1)
1. a preparation method for yellow dyes, is characterized in that comprising the following steps:
A, ox-hide is put into pot, add water and be boiled into paste, obtain ox-hide cream, for subsequent use;
B, the pulp of wolfberry fruit and pericarp to be removed, collect its seed grain, and put into soybean milk maker, add 1 ~ 3 times of water, pulverize 15 minutes ~ 20 minutes, pour out, remove slag, by remaining solution left standstill 1 hour ~ 3 hours, go upper solution, retain lower floor's sediment;
C, step B lower floor sediment put into soybean milk maker, add 1 ~ 3 times of water, pulverize 30 minutes ~ 40 minutes, pour out, leave standstill 1 hour ~ 3 hours, go upper solution, retain lower floor's sediment;
D, continuation repeat step C, until the granularity of the lower floor's sediment obtained reaches 50 nanometer ~ 100 nanometers;
Lower floor's sediment that E, in mass ratio D step obtain: described lower floor sediment mixes with described ox-hide cream by the ratio of ox-hide cream=1:0.01 ~ 0.1 that step A obtains, and makes the yellow dyes of required form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410297620.6A CN104059385B (en) | 2014-06-29 | 2014-06-29 | The preparation method of yellow dyes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410297620.6A CN104059385B (en) | 2014-06-29 | 2014-06-29 | The preparation method of yellow dyes |
Publications (2)
| Publication Number | Publication Date |
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| CN104059385A CN104059385A (en) | 2014-09-24 |
| CN104059385B true CN104059385B (en) | 2016-03-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410297620.6A Active CN104059385B (en) | 2014-06-29 | 2014-06-29 | The preparation method of yellow dyes |
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| CN (1) | CN104059385B (en) |
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2014
- 2014-06-29 CN CN201410297620.6A patent/CN104059385B/en active Active
Non-Patent Citations (2)
| Title |
|---|
| 超声波提取-分光光度法测定枸杞中黄色素的研究;高岐 等;《粮油加工》;20081231(第4期);第123-124页 * |
| 黄色素提取工艺的研究进展;呼延晓颖 等;《饮料工业》;20111231;第14卷(第02期);第9-12页 * |
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Effective date of registration: 20171027 Address after: 6 417A room, building No. 1188, west two ring road, Shengze Town, Wujiang District, Jiangsu, Suzhou, 215228 Patentee after: Suzhou hair textile Co., Ltd. Address before: Rongshui Miao Autonomous County of Liuzhou City, 545311 the Guangxi Zhuang Autonomous Region Pei Dong Cun Tai Xiang Lin Tun No. 11 Patentee before: Rongshui Guangxi snow weasel Science and Technology Development Co., Ltd. |
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Effective date of registration: 20181010 Address after: 215200 No. 1188 west two ring road, Shengze Town, Wujiang District, Suzhou, Jiangsu. Patentee after: Suzhou Shengze science and Technology Pioneer Park Development Co., Ltd. Address before: 215228 417A, 6 building, 1188 west two ring road, Shengze Town, Wujiang District, Suzhou, Jiangsu. Patentee before: Suzhou hair textile Co., Ltd. |