CN104029263A - Wood preservative and preparation method thereof - Google Patents
Wood preservative and preparation method thereof Download PDFInfo
- Publication number
- CN104029263A CN104029263A CN201410273377.4A CN201410273377A CN104029263A CN 104029263 A CN104029263 A CN 104029263A CN 201410273377 A CN201410273377 A CN 201410273377A CN 104029263 A CN104029263 A CN 104029263A
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- China
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- parts
- timber preservative
- preparation
- coal tar
- pinellia
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Links
- 238000002360 preparation method Methods 0.000 title claims description 15
- 239000003171 wood protecting agent Substances 0.000 title abstract description 7
- IZUPBVBPLAPZRR-UHFFFAOYSA-N pentachlorophenol Chemical compound OC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl IZUPBVBPLAPZRR-UHFFFAOYSA-N 0.000 claims abstract description 33
- 241001522129 Pinellia Species 0.000 claims abstract description 19
- 239000011280 coal tar Substances 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 239000011864 timber preservative Substances 0.000 claims description 27
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 241000208296 Datura Species 0.000 claims description 17
- 239000012153 distilled water Substances 0.000 claims description 12
- 235000010297 nisin Nutrition 0.000 claims description 12
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 12
- 235000010234 sodium benzoate Nutrition 0.000 claims description 12
- 239000012530 fluid Substances 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- NVNLLIYOARQCIX-MSHCCFNRSA-N Nisin Chemical compound N1C(=O)[C@@H](CC(C)C)NC(=O)C(=C)NC(=O)[C@@H]([C@H](C)CC)NC(=O)[C@@H](NC(=O)C(=C/C)/NC(=O)[C@H](N)[C@H](C)CC)CSC[C@@H]1C(=O)N[C@@H]1C(=O)N2CCC[C@@H]2C(=O)NCC(=O)N[C@@H](C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(NCC(=O)N[C@H](C)C(=O)N[C@H](CC(C)C)C(=O)N[C@H](CCSC)C(=O)NCC(=O)N[C@H](CS[C@@H]2C)C(=O)N[C@H](CC(N)=O)C(=O)N[C@H](CCSC)C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(N[C@H](C)C(=O)N[C@@H]3C(=O)N[C@@H](C(N[C@H](CC=4NC=NC=4)C(=O)N[C@H](CS[C@@H]3C)C(=O)N[C@H](CO)C(=O)N[C@H]([C@H](C)CC)C(=O)N[C@H](CC=3NC=NC=3)C(=O)N[C@H](C(C)C)C(=O)NC(=C)C(=O)N[C@H](CCCCN)C(O)=O)=O)CS[C@@H]2C)=O)=O)CS[C@@H]1C NVNLLIYOARQCIX-MSHCCFNRSA-N 0.000 claims description 7
- 108010053775 Nisin Proteins 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 7
- 239000004309 nisin Substances 0.000 claims description 7
- 229920000656 polylysine Polymers 0.000 claims description 7
- 239000004299 sodium benzoate Substances 0.000 claims description 7
- 244000080767 Areca catechu Species 0.000 claims description 5
- 235000006226 Areca catechu Nutrition 0.000 claims description 5
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 108010039918 Polylysine Proteins 0.000 claims description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052802 copper Inorganic materials 0.000 abstract description 2
- 239000010949 copper Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 241001096657 Pogostemon stellatus Species 0.000 abstract 2
- 229940126680 traditional chinese medicines Drugs 0.000 abstract 2
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 239000002131 composite material Substances 0.000 abstract 1
- 150000001879 copper Chemical class 0.000 abstract 1
- ZOUQIAGHKFLHIA-UHFFFAOYSA-L copper;n,n-dimethylcarbamodithioate Chemical compound [Cu+2].CN(C)C([S-])=S.CN(C)C([S-])=S ZOUQIAGHKFLHIA-UHFFFAOYSA-L 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000002023 wood Substances 0.000 description 5
- 241000723353 Chrysanthemum Species 0.000 description 4
- 238000004321 preservation Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 1
- 150000003973 alkyl amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- MZGNSEAPZQGJRB-UHFFFAOYSA-N dimethyldithiocarbamic acid Chemical compound CN(C)C(S)=S MZGNSEAPZQGJRB-UHFFFAOYSA-N 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
Landscapes
- Chemical And Physical Treatments For Wood And The Like (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a wood preservative. The wood preservative contains ammoniacal copper quaternary, pentachlorophenol, coal tar, copper (II) dimethyl dithiocarbamate, stramonium, pinellia ternate and eusteralis stellata. The wood preservative is characterized by consisting of the following raw materials in parts by weight: 20-40 parts of chitosan, 30-35 parts of pentachlorophenol, 15-30 parts of coal tar, 10-25 parts of stramonium, 20-30 parts of pinellia ternate, and 12-20 parts of eusteralis stellata. The wood preservative does not contain copper salt, all the raw materials in the adopted composite formula of traditional Chinese medicines plus chemicals are completely environmentally friendly, the traditional Chinese medicines are cheap and the wood preservative has antibacterial and insect-prevention effects.
Description
Technical field
The present invention relates to timber and safeguard aspect, particularly a kind of timber preservative and preparation method thereof.
Background technology
Wood preservation, is to increase timber reserves on the basis that does not need to increase area of woods, effective wood preservation processing service life of prolonging wood greatly.Due to China, area of woods is few per capita, wood preservation weak foundation, and be in developing period, actively develop the meaning that novel wood preservative has important sustainable development, what use was maximum at present is water base anticorrisive agent, wherein mantoquita is as conventional timber preservative, but the low resistance leachability of cost own is poor, very large to the destruction of natural environment.
Summary of the invention
Technical problem to be solved: for above problem the invention provides not containing mantoquita, bactericidal effect by force, easily degraded and on environment without a kind of timber preservative of impact and preparation method thereof.
Technical scheme: in order overcoming the above problems, to the invention provides a kind of timber preservative, to comprise the molten alkylamine copper of ammonia, pentachlorophenol, coal tar, cupric dimethyldithio carbamate, datura, the tuber of pinellia, blinds; Weight portion proportioning between described raw material is successively: shitosan 20-40 part, pentachlorophenol 30-35 part, coal tar 15-30 part, datura 10-25 part, tuber of pinellia 20-30 part, blinds 12-20 part.
Further technical scheme, also comprises nisin 5-8 part, Sodium Benzoate 2-4 part, hydrogen peroxide 7-15 part.
A preparation method for timber preservative, comprises the following steps:
The first step: by shitosan, pentachlorophenol, be dissolved in coal tar, and add distilled water, make distilled water account for 40-60% of gross weight, heat to 40-50 DEG C and stir, add again polylysine 4-6 part, temperature is adjusted to 45-60 DEG C, continue to be stirred to raw material and be all dissolved into homogeneous transparent look;
Second step: datura, the tuber of pinellia, blinds be placed in to frozen water and add Dalmatian chrysanthemum, frutus cnidii, betel nut, soaking 2 hours, more fully grinding, then be positioned over 2500-3500MHZ, microwave 20-30 minute under the condition of 40-50 DEG C, filters, go out after filter residue, obtain filtered fluid;
The 3rd step: in the filtered fluid in second step, add nisin, Sodium Benzoate, hydrogen peroxide, 40 DEG C of water-baths of constant temperature 3 hours, then pour in the mixed solution in the first step, stir, regulate PH to 4-6, leave standstill 3 hours;
The 4th step: the mixed solution absolute ethyl alcohol distillation that the 3rd step is obtained 2-4 time, obtains timber preservative.
Further technical scheme, described 22 parts of 18 parts of 20 parts, 32 parts of 25 parts of shitosans, pentachlorophenols, coal tar, daturas, the tuber of pinellia, 15 parts of blinds.
Further technical scheme, described 4 parts of 6 parts of nisins, Sodium Benzoates, 8 parts of hydrogen peroxide.
Further technical scheme, in the first step, distilled water accounts for 45% of gross mass, heat to 45 DEG C, 5 parts of polylysines, temperature is adjusted to 50 DEG C.
Further technical scheme, in second step, microwave condition is: 3000MHZ, 42 DEG C, 25 minutes.
Further technical scheme, in the 3rd step, PH is 4.5.
Further technical scheme, absolute ethyl alcohol distillation 3 times in the 4th step.
Beneficial effect: do not contain mantoquita in timber preservative of the present invention, the Chinese medicine adopting adds the raw material that chemical compound prescription is complete environmental protection, and Chinese medicine is cheap, there is antibacterial, insect protected effect, and also inhibited to domestomycetes, in prolonging wood using life, greatly lower the pollution that anticorrisive agent runs off to environment.
Detailed description of the invention
The present invention is described in further detail below.
Embodiment 1
A kind of timber preservative, comprises shitosan, pentachlorophenol, coal tar, datura, the tuber of pinellia, blinds; Weight portion proportioning between described raw material is successively: 20 parts of shitosans, 30 parts of pentachlorophenols, 15 parts, coal tar, 10 parts of daturas, 20 parts of the tuber of pinellia, 12 parts of blinds.
In the present invention, also comprise 5 parts of nisins, 2 parts of Sodium Benzoates, 7 parts of hydrogen peroxide.
A preparation method for timber preservative, comprises the following steps:
The first step: by shitosan, pentachlorophenol, be dissolved in coal tar, and add distilled water, make distilled water account for 40% of gross weight, heat to 40 DEG C and stir, add again 4 parts of polylysines, temperature is adjusted to 45 DEG C, continue to be stirred to raw material and be all dissolved into homogeneous transparent look;
Second step: datura, the tuber of pinellia, blinds be placed in to frozen water and add Dalmatian chrysanthemum, frutus cnidii, betel nut, soaking 2 hours, more fully grinding, being then positioned over 2500-MHZ, microwave 20 minutes under the condition of 40 DEG C, filters, and goes out after filter residue, obtains filtered fluid;
The 3rd step: in the filtered fluid in second step, add nisin, Sodium Benzoate, hydrogen peroxide, 40 DEG C of water-baths of constant temperature 3 hours, then pour in the mixed solution in the first step, stir, regulate PH to 4, leave standstill 3 hours;
The 4th step: the mixed solution absolute ethyl alcohol distillation that the 3rd step is obtained 2 times, obtains timber preservative.
Embodiment 2
A kind of timber preservative, comprises shitosan, pentachlorophenol, coal tar, datura, the tuber of pinellia, blinds; Weight portion proportioning between described raw material is successively: 40 parts of shitosans, 35 parts of pentachlorophenols, 30 parts, coal tar, 25 parts of daturas, 30 parts of the tuber of pinellia, 20 parts of blinds.
The present invention also comprises 8 parts of nisins, 4 parts of Sodium Benzoates, 15 parts of hydrogen peroxide.
A preparation method for timber preservative, comprises the following steps:
The first step: by shitosan, pentachlorophenol, be dissolved in coal tar, and add distilled water, make distilled water account for 60% of gross weight, heat to 50 DEG C and stir, add again 6 parts of polylysines, temperature is adjusted to 60 DEG C, continue to be stirred to raw material and be all dissolved into homogeneous transparent look;
Second step: datura, the tuber of pinellia, blinds be placed in to frozen water and add Dalmatian chrysanthemum, frutus cnidii, betel nut, soaking 2 hours, more fully grinding, being then positioned over 3500MHZ, microwave 30 minutes under the condition of 50 DEG C, filters, and goes out after filter residue, obtains filtered fluid;
The 3rd step: in the filtered fluid in second step, add nisin, Sodium Benzoate, hydrogen peroxide, 40 DEG C of water-baths of constant temperature 3 hours, then pour in the mixed solution in the first step, stir, regulate PH to 6, leave standstill 3 hours;
The 4th step: the mixed solution absolute ethyl alcohol distillation that the 3rd step is obtained 4 times, obtains timber preservative.
Embodiment 3
A kind of timber preservative, comprises shitosan, pentachlorophenol, coal tar, datura, the tuber of pinellia, blinds; Weight portion proportioning between described raw material is successively: 25 parts of shitosans, 32 parts of pentachlorophenols, 20 parts, coal tar, 18 parts of daturas, 22 parts of the tuber of pinellia, 15 parts of blinds.
The present invention also comprises 6 parts of nisins, 4 parts of Sodium Benzoates, 8 parts of hydrogen peroxide.
A preparation method for timber preservative, comprises the following steps:
The first step: by shitosan, pentachlorophenol, be dissolved in coal tar, and add distilled water, make distilled water account for 45% of gross weight, heat to 45 DEG C and stir, add again 5 parts of polylysines, temperature is adjusted to 50 DEG C, continue to be stirred to raw material and be all dissolved into homogeneous transparent look;
Second step: datura, the tuber of pinellia, blinds be placed in to frozen water and add Dalmatian chrysanthemum, frutus cnidii, betel nut, soaking 2 hours, more fully grinding, being then positioned over 3000MHZ, microwave 25 minutes under the condition of 42 DEG C, filters, and goes out after filter residue, obtains filtered fluid;
The 3rd step: in the filtered fluid in second step, add nisin, Sodium Benzoate, hydrogen peroxide, 40 DEG C of water-baths of constant temperature 3 hours, then pour in the mixed solution in the first step, stir, regulate PH to 4.5, leave standstill 3 hours;
The 4th step: the mixed solution absolute ethyl alcohol distillation that the 3rd step is obtained 3 times, obtains timber preservative.
Claims (9)
1. a timber preservative, is characterized in that, comprises shitosan, pentachlorophenol, coal tar, datura, the tuber of pinellia, blinds; Weight portion proportioning between described raw material is successively: shitosan 20-40 part, pentachlorophenol 30-35 part, coal tar 15-30 part, datura 10-25 part, tuber of pinellia 20-30 part, blinds 12-20 part.
2. a kind of timber preservative according to claim 1, is characterized in that, also comprises nisin 5-8 part, Sodium Benzoate 2-4 part, hydrogen peroxide 7-15 part.
3. a preparation method for timber preservative, is characterized in that, comprises the following steps:
The first step: by shitosan, pentachlorophenol, be dissolved in coal tar, and add distilled water, make distilled water account for 40-60% of gross weight, heat to 40-50 DEG C and stir, add again polylysine 4-6 part, temperature is adjusted to 45-60 DEG C, continue to be stirred to raw material and be all dissolved into homogeneous transparent look;
Second step: datura, the tuber of pinellia, blinds be placed in to frozen water and add Dalmatian chrysanthemum, frutus cnidii, betel nut, soaking 2 hours, more fully grinding, then be positioned over 2500-3500MHZ, microwave 20-30 minute under the condition of 40-50 DEG C, filters, go out after filter residue, obtain filtered fluid;
The 3rd step: in the filtered fluid in second step, add nisin, Sodium Benzoate, hydrogen peroxide, 40 DEG C of water-baths of constant temperature 3 hours, then pour in the mixed solution in the first step, stir, regulate PH to 4-6, leave standstill 3 hours;
The 4th step: the mixed solution absolute ethyl alcohol distillation that the 3rd step is obtained 2-4 time, obtains timber preservative.
4. according to a kind of timber preservative described in claim 1 or 3 and preparation method thereof, it is characterized in that described 22 parts of 18 parts of 20 parts, 32 parts of 25 parts of shitosans, pentachlorophenols, coal tar, daturas, the tuber of pinellia, 15 parts of blinds.
5. according to a kind of timber preservative described in claim 2 or 3 and preparation method thereof, it is characterized in that described 4 parts of 6 parts of nisins, Sodium Benzoates, 8 parts of hydrogen peroxide.
6. the preparation method of a kind of timber preservative according to claim 3, is characterized in that, in the first step, distilled water accounts for 45% of gross mass, heat to 45 DEG C, and 5 parts of polylysines, temperature is adjusted to 50 DEG C.
7. the preparation method of a kind of timber preservative according to claim 3, is characterized in that, in second step, microwave condition is: 3000MHZ, 42 DEG C, 25 minutes.
8. the preparation method of a kind of timber preservative according to claim 3, is characterized in that, in the 3rd step, PH is 4.5.
9. the preparation method of a kind of timber preservative according to claim 3, is characterized in that, absolute ethyl alcohol distillation 3 times in the 4th step.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410273377.4A CN104029263B (en) | 2014-06-19 | 2014-06-19 | A kind of timber preservative and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410273377.4A CN104029263B (en) | 2014-06-19 | 2014-06-19 | A kind of timber preservative and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104029263A true CN104029263A (en) | 2014-09-10 |
| CN104029263B CN104029263B (en) | 2016-08-03 |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104858952A (en) * | 2015-06-19 | 2015-08-26 | 淄博大创自动化科技有限公司 | Processing technology for perfuming, corrosion-prevention and bacteria-prevention of folding fan bamboo ribs |
| CN104924389A (en) * | 2015-06-11 | 2015-09-23 | 阜南县中泰工艺品有限公司 | Use method for wood treating agent |
| CN104924402A (en) * | 2015-06-19 | 2015-09-23 | 淄博大创自动化科技有限公司 | Mosquito driving and antiseptic antibacterial processing technology for folding-fan bamboo ribs |
| CN104924403A (en) * | 2015-06-19 | 2015-09-23 | 淄博大创自动化科技有限公司 | Antimicrobial antiseptic cooking liquid for folding-fan bamboo ribs and antimicrobial antiseptic technology of antimicrobial antiseptic cooking liquid |
| CN105360163A (en) * | 2015-11-18 | 2016-03-02 | 广德县常丰竹木业制品有限公司 | Bamboo wood mould inhibitor and preparation method thereof |
| CN106863515A (en) * | 2017-01-13 | 2017-06-20 | 亚振家具股份有限公司 | A kind of environment-friendly type compounding timber protective agent and preparation method thereof |
| CN107053408A (en) * | 2017-06-22 | 2017-08-18 | 合肥月煌新型装饰材料有限公司 | A kind of Wood construction preservative and preparation method thereof |
| CN111496962A (en) * | 2020-05-08 | 2020-08-07 | 福建省尤溪县百源木业有限公司 | Preparation process of integrated plate with corrosion resistance |
| CN112042680A (en) * | 2020-09-14 | 2020-12-08 | 何述安 | Environment-friendly preservative and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104924389A (en) * | 2015-06-11 | 2015-09-23 | 阜南县中泰工艺品有限公司 | Use method for wood treating agent |
| CN104858952A (en) * | 2015-06-19 | 2015-08-26 | 淄博大创自动化科技有限公司 | Processing technology for perfuming, corrosion-prevention and bacteria-prevention of folding fan bamboo ribs |
| CN104924402A (en) * | 2015-06-19 | 2015-09-23 | 淄博大创自动化科技有限公司 | Mosquito driving and antiseptic antibacterial processing technology for folding-fan bamboo ribs |
| CN104924403A (en) * | 2015-06-19 | 2015-09-23 | 淄博大创自动化科技有限公司 | Antimicrobial antiseptic cooking liquid for folding-fan bamboo ribs and antimicrobial antiseptic technology of antimicrobial antiseptic cooking liquid |
| CN105360163A (en) * | 2015-11-18 | 2016-03-02 | 广德县常丰竹木业制品有限公司 | Bamboo wood mould inhibitor and preparation method thereof |
| CN106863515A (en) * | 2017-01-13 | 2017-06-20 | 亚振家具股份有限公司 | A kind of environment-friendly type compounding timber protective agent and preparation method thereof |
| CN107053408A (en) * | 2017-06-22 | 2017-08-18 | 合肥月煌新型装饰材料有限公司 | A kind of Wood construction preservative and preparation method thereof |
| CN111496962A (en) * | 2020-05-08 | 2020-08-07 | 福建省尤溪县百源木业有限公司 | Preparation process of integrated plate with corrosion resistance |
| CN112042680A (en) * | 2020-09-14 | 2020-12-08 | 何述安 | Environment-friendly preservative and preparation method thereof |
| CN112042680B (en) * | 2020-09-14 | 2022-06-21 | 何述安 | Environment-friendly preservative and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104029263B (en) | 2016-08-03 |
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