CN104020089A - Method for calibrating PM2.5 (Particulate Matter2.5) monitor - Google Patents

Method for calibrating PM2.5 (Particulate Matter2.5) monitor Download PDF

Info

Publication number
CN104020089A
CN104020089A CN201410244506.7A CN201410244506A CN104020089A CN 104020089 A CN104020089 A CN 104020089A CN 201410244506 A CN201410244506 A CN 201410244506A CN 104020089 A CN104020089 A CN 104020089A
Authority
CN
China
Prior art keywords
monitor
gasoloid
aerosols
pipeline
calibration steps
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410244506.7A
Other languages
Chinese (zh)
Inventor
郭波
许思思
隋峰
许爱华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Institute of Metrology
Original Assignee
Shandong Institute of Metrology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Institute of Metrology filed Critical Shandong Institute of Metrology
Priority to CN201410244506.7A priority Critical patent/CN104020089A/en
Publication of CN104020089A publication Critical patent/CN104020089A/en
Pending legal-status Critical Current

Links

Landscapes

  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a method for calibrating a PM2.5 (Particulate Matter2.5) monitor. The method comprises the following steps: preparing aerosols with different sizes by using an aerosol generator, respectively adding the aerosols into a mixing box of a pipeline through each corresponding channel to be mixed with clean air, and diluting the generated aerosols to the required concentrations; adding the diluted aerosols into a common pipeline and then shunting, enabling one part of the aerosols to flow through the PM2.5 monitor so as to measure the concentrations of PM2.5 aerosols repeatedly and obtain an average value; enabling the other part of the aerosols to flow through a front particle size spectrometer, a PM2.5 cutter and a rear particle size spectrometer so as to measure the concentrations of PM2.5 aerosols repeatedly and obtain an average value; comparing the average values of two pipelines to calibrate the PM2.5 monitor. The method is high in detection accuracy and efficiency and easy to popularize and use.

Description

A kind of PM 2.5monitor calibration steps
Technical field
The present invention relates to a kind of PM 2.5the quick and precisely collimation technique of monitor, concrete, relate to a kind of PM 2.5monitor calibration steps.
Background technology
PM 2.5in finger atmosphere, aerodynamic diameter is less than or equal to the particle of 2.5 μ m, and also referred to as entering lung particle, it forms main with artificially relevant.GB3095-2012 " ambient air quality " has increased PM 2.5monitoring index.Chinese Ministry of Environmental Protection requires from 2012 in key areas such as Beijing-Tianjin Ji, the Yangtze River Delta, Pearl River Deltas and municipality directly under the Central Government and provincial capital carry out PM 2.5monitoring, all to and evaluate surrounding air PM according to above-mentioned standard monitoring to all parts of the country in 2016 2.5concentration.
At present, domestic PM 2.5monitor quality is uneven, cannot accurate evaluation surrounding air in PM 2.5content.For ensureing PM 2.5accurately and reliably, the U.S., Japan, European Union etc. have carried out detection method standardization and the research of metering traceability to Monitoring Data.The external single channel PM having adopted 2.5monitor calibration steps, at calibration PM 2.5when monitor, need to prepare multiple single size gasoloid, before being passed into calibrating installation, different size gasoloid must clean whole pipelines, process is loaded down with trivial details, calibration efficiency is low, and the long rate that exists that purges dead angle that causes of pipeline increases, cause having different size aerosol particle residual, affect calibration accuracy.
Summary of the invention
In order to address the above problem, the invention provides a kind of PM 2.5monitor calibration steps, the method is reasonable in design, has avoided existing calibration system need to repeat to purge the problem of whole pipelines, adopts the method, and precision and efficiency of detecting is high, and cost is lower, simple to operate, is easy to promote the use of.
In order to achieve the above object, technical scheme of the present invention is:
A kind of PM 2.5monitor calibration steps, comprise the steps: that aerosol generator 1 prepares the gasoloid of different size, the blending bin 103,203,303,403,503,603,703,803 that enters its pipeline by every respective channel respectively mixes with pure air, and the gasoloid of generation is diluted to desired concn; After the gasoloid of dilution enters public pipeline, shunt, a part is passed through PM 2.5monitor 5, repeatedly measures PM 2.5aerocolloidal concentration is also averaged, and another part is successively by preposition particle diameter spectrometer 7, PM 2.5cutter 8 and rearmounted particle diameter spectrometer 9, repeatedly measure PM 2.5aerocolloidal concentration is also averaged; By comparing the mean value of two pipelines, to PM 2.5monitor 5 is calibrated.
Described passage is eight, and gasoloid size prepared by every passage is respectively 1.5 ± 0.25 μ m, 2.0 ± 0.25 μ m, 2.2 ± 0.25 μ m, 2.5 ± 0.25 μ m, 2.8 ± 0.25 μ m, 3.0 ± 0.25 μ m, 3.5 ± 0.25 μ m, 4.0 ± 0.5 μ m.
Pure air after described gasoloid is measured by flowmeter in blending bin 103,203,303,403,503,603,703,803 dilutes.
Described each switching gasoloid is flowed through and is purged public pipeline with pure air before pipeline.
Described aerosol discharge to before in air all through clarifier I6, II10 purified treatment.
Owing to having adopted described technical scheme, the present invention has following superiority:
1, eight kinds of single size gasoloids enter detecting instrument by corresponding pipeline separately respectively, need to before passing into different size gasoloid, not purge whole pipelines, only need to purge public part, have improved calibration efficiency, have reduced error.
2, adopt system of the present invention can accurately measure PM 2.5aerocolloidal concentration, meets calibration PM 25the requirement of monitor, and simple to operate, be easy to detect industry in metering and apply.
Brief description of the drawings
Fig. 1 is a kind of PM of the present invention 2.5the process flow diagram of monitor calibration steps; (10-first passage, 20-second channel, 30-third channel, 40-four-way, 50-Five-channel, 60-the 6th passage, 70-the 7th passage, 80-the 8th passage, 1-aerosol generator, 102,202,302,402,502,602,702,802-pure air entrance, 103,203,303,403,503,603,703,803-blending bin, 4-pure air entrance, 5-PM 2.5monitor, 6-clarifier I, the preposition particle diameter spectrometer of 7-, 8-PM 2.5cutter, the rearmounted particle diameter spectrometer of 9-, 10-clarifier II)
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein, only for description and interpretation the present invention, is not intended to limit the present invention.
Embodiment:
Fig. 1 shows an embodiment of calibration system of the present invention, has eight passages: first passage 10, second channel 20, third channel 30, four-way 40, Five-channel 50, the 6th passage 60, the 7th passage 70 and the 8th passage 80.
First passage 10 is prepared the aerosol particle of particle diameter 1.5 ± 0.25 μ m by aerosol generator 1, enter blending bin 103 and mix by 102 pure airs that enter blending bin 103, and the gasoloid of generation is diluted to 35 μ g/m 3, the gasoloid of dilution is shunted after entering public pipeline, and a part is passed through PM 2.5monitor 5, after instrument registration to be monitored is stable, per minute reading once, is read six groups of data, measures PM 2.5aerocolloidal mean concentration, another part is successively by preposition particle diameter spectrometer 7, PM2.5 cutter 8 and rearmounted particle diameter spectrometer 9, and after two particle diameter spectrometer registrations are stable, per minute reading once, is read six groups of data, measures PM 25aerocolloidal mean concentration; By relatively measuring concentration mean value twice, calibration PM 2.5monitor 5.Single size is measured complete, closes first passage 10, and air intake 4 passes into pure air and purges public pipeline, after clarifier I6, II10 filter, discharges.
Second channel 20 is prepared the aerosol particle of particle diameter 2.0 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
Third channel 30 is prepared the aerosol particle of particle diameter 2.2 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
Four-way 40 is prepared the aerosol particle of particle diameter 2.5 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
Five-channel 50 is prepared the aerosol particle of particle diameter 2.8 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
The 6th passage 60 is prepared the aerosol particle of particle diameter 3.0 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
The 7th passage 70 is prepared the aerosol particle of particle diameter 3.5 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.
The 8th passage 80 is prepared the aerosol particle of particle diameter 4.0 ± 0.25 μ m by aerosol generator 1; By relatively measuring concentration value twice, calibration PM 2.5monitor 5.Single size is measured complete, purges public pipeline.

Claims (5)

1. a PM 2.5monitor calibration steps, comprise the steps: that aerosol generator 1 prepares the gasoloid of different size, the blending bin 103,203,303,403,503,603,703,803 that enters its pipeline by every respective channel respectively mixes with pure air, and the gasoloid of generation is diluted to desired concn; After the gasoloid of dilution enters public pipeline, shunt, a part is passed through PM 25monitor 5, repeatedly measures PM 25aerocolloidal concentration is also averaged, and another part is successively by preposition particle diameter spectrometer 7, PM 25cutter 8 and rearmounted particle diameter spectrometer 9, repeatedly measure PM 25aerocolloidal concentration is also averaged; By comparing the mean value of two pipelines, to PM 25monitor 5 is calibrated.
2. a kind of PM according to claim 1 2.5monitor calibration steps, it is characterized in that described passage is eight, gasoloid size prepared by every passage is respectively 1.5 ± 0.25 μ m, 2.0 ± 0.25 μ m, 2.2 ± 0.25 μ m, 2.5 ± 0.25 μ m, 2.8 ± 0.25 μ m, 3.0 ± 0.25 μ m, 3.5 ± 0.25 μ m, 4.0 ± 0.5 μ m.
3. a kind of PM according to claim 1 2.5monitor calibration steps, is characterized in that the pure air after described gasoloid is measured by flowmeter in blending bin 103,203,303,403,503,603,703,803 dilutes.
4. a kind of PM according to claim 1 25monitor calibration steps, is characterized in that described each switching gasoloid is flowed through to purge public pipeline with pure air before pipeline.
5. a kind of PM according to claim 1 2.5monitor calibration steps, it is characterized in that described aerosol discharge to before in air all through clarifier I6, II10 purified treatment.
CN201410244506.7A 2014-06-05 2014-06-05 Method for calibrating PM2.5 (Particulate Matter2.5) monitor Pending CN104020089A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410244506.7A CN104020089A (en) 2014-06-05 2014-06-05 Method for calibrating PM2.5 (Particulate Matter2.5) monitor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410244506.7A CN104020089A (en) 2014-06-05 2014-06-05 Method for calibrating PM2.5 (Particulate Matter2.5) monitor

Publications (1)

Publication Number Publication Date
CN104020089A true CN104020089A (en) 2014-09-03

Family

ID=51436968

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410244506.7A Pending CN104020089A (en) 2014-06-05 2014-06-05 Method for calibrating PM2.5 (Particulate Matter2.5) monitor

Country Status (1)

Country Link
CN (1) CN104020089A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105865994A (en) * 2016-04-22 2016-08-17 苏州翰霖汽车科技有限公司 Calibration device for PM2.5 sensors and calibrating method thereof
CN107102350A (en) * 2017-05-03 2017-08-29 中国核动力研究设计院 A kind of radioactivity inert gas monitor calibration method and system
CN107110756A (en) * 2014-11-21 2017-08-29 海因里希·伊格尔塞德尔 Method and system for measuring fine particle concentration PM1, PM2.5 and PM10 simultaneously
CN108169101A (en) * 2018-01-18 2018-06-15 广州纤维产品检测研究院 A kind of haze window screening filter effect test device and test method
CN111812002A (en) * 2020-06-29 2020-10-23 上海交通大学 Small flow aerosol measuring method
CN113720747A (en) * 2021-08-31 2021-11-30 北京航空航天大学 Aerosol particle dilution system and aerosol particle counting device with same

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201402268Y (en) * 2009-02-25 2010-02-10 北京泰华恒越科技发展有限责任公司 Intelligent environmental air quality monitor
CN202548040U (en) * 2011-12-14 2012-11-21 河北先河环保科技股份有限公司 Automatic particle monitoring instrument
CN202793976U (en) * 2012-06-13 2013-03-13 北京绿林创新数码科技有限公司 Multi-cutter dust on-line monitoring system
CN103674796A (en) * 2013-12-23 2014-03-26 青岛科技大学 Multi-channel PM2.5 monitor calibration device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201402268Y (en) * 2009-02-25 2010-02-10 北京泰华恒越科技发展有限责任公司 Intelligent environmental air quality monitor
CN202548040U (en) * 2011-12-14 2012-11-21 河北先河环保科技股份有限公司 Automatic particle monitoring instrument
CN202793976U (en) * 2012-06-13 2013-03-13 北京绿林创新数码科技有限公司 Multi-cutter dust on-line monitoring system
CN103674796A (en) * 2013-12-23 2014-03-26 青岛科技大学 Multi-channel PM2.5 monitor calibration device

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107110756A (en) * 2014-11-21 2017-08-29 海因里希·伊格尔塞德尔 Method and system for measuring fine particle concentration PM1, PM2.5 and PM10 simultaneously
CN107110756B (en) * 2014-11-21 2020-12-29 海因里希·伊格尔塞德尔 Method and system for simultaneously measuring fine particulate matter concentrations PM1, PM2.5, and PM10
CN105865994A (en) * 2016-04-22 2016-08-17 苏州翰霖汽车科技有限公司 Calibration device for PM2.5 sensors and calibrating method thereof
CN107102350A (en) * 2017-05-03 2017-08-29 中国核动力研究设计院 A kind of radioactivity inert gas monitor calibration method and system
CN107102350B (en) * 2017-05-03 2018-11-13 中国核动力研究设计院 A kind of radioactivity inert gas monitor calibration method and system
CN108169101A (en) * 2018-01-18 2018-06-15 广州纤维产品检测研究院 A kind of haze window screening filter effect test device and test method
CN108169101B (en) * 2018-01-18 2023-12-19 广州纤维产品检测研究院 Anti-haze window screening filtering effect testing device and testing method
CN111812002A (en) * 2020-06-29 2020-10-23 上海交通大学 Small flow aerosol measuring method
CN113720747A (en) * 2021-08-31 2021-11-30 北京航空航天大学 Aerosol particle dilution system and aerosol particle counting device with same
CN113720747B (en) * 2021-08-31 2023-08-18 北京航空航天大学 Aerosol particulate matter dilution system and aerosol particulate matter counting device with same

Similar Documents

Publication Publication Date Title
CN104020089A (en) Method for calibrating PM2.5 (Particulate Matter2.5) monitor
CN105572307B (en) The calibration tooling and scaling method of a kind of gas sensor
CN103674796B (en) A kind of hyperchannel PM2.5 monitor calibrating installation
CN205484299U (en) Quality of water on -line measuring device
CN209055534U (en) A kind of device for distributing standard gas for environmental gas analyzer calibration
CN101776581A (en) Method for photometric analysis of trace pollutant in water sample and device thereof
KR20120018273A (en) Exhaust gas analyzing system
CN102337341B (en) MALDI-TOF (Matrix-assisted laser desorption/ionization-Time-of-flight) mass spectrum double internal standard and quantitative detecting method thereof
CN105067495A (en) Filtration efficiency calibration system for air filtration equipment
CN109765154A (en) The on-line calibration system and calibration method of PM2.5/PM10 optical scatter object monitor
CN103616521A (en) Exhaust pollutant measuring system for in-use vehicle
CN205720164U (en) Portable dynamic air distribution system
EP3454037B1 (en) Exhaust gas analysis device, exhaust gas analysis method and program for exhaust gas analysis device
CN106872366A (en) A kind of low concentration ozone concentration detector of single light source
CN105717065A (en) Continuous monitoring device for non-methane total hydrocarbon and working method of continuous monitoring device
CN104729891A (en) PM2.5 (Particulate Matter 2.5) source analyzing and sampling device based on carbon dioxide concentration control
CN103295871A (en) Ion mobility spectrometry detection system
CN106841495A (en) The high-sensitivity analysis method of genotoxicity impurity in ethyl sulfonic acid Nintedanib
CN205719955U (en) The continuous monitoring device of NMHC
CN204594710U (en) A kind of easy penetrating grain size method high efficiency particulate air filter test board
CN103954691B (en) Nondestructive testing method for material component fraction
CN105953836A (en) Test method for multi-parameter SF6 detection device
CN209559501U (en) A kind of marine gas turbine gas handling system comprehensive simulation test system
CN107643261A (en) A kind of monitor of long light path White pond DOAS methods measurement dusty gas concentration
CN107941895A (en) Ionic migration spectrum detection instrument

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20140903