CN104016588A - Bottle parison material for low-calcium thermos - Google Patents
Bottle parison material for low-calcium thermos Download PDFInfo
- Publication number
- CN104016588A CN104016588A CN201410190568.4A CN201410190568A CN104016588A CN 104016588 A CN104016588 A CN 104016588A CN 201410190568 A CN201410190568 A CN 201410190568A CN 104016588 A CN104016588 A CN 104016588A
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- CN
- China
- Prior art keywords
- oxide
- parts
- calcium
- mentioned
- flyash
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011575 calcium Substances 0.000 title claims abstract description 18
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 18
- 239000000463 material Substances 0.000 title claims abstract description 14
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002893 slag Substances 0.000 claims abstract description 17
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011787 zinc oxide Substances 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 8
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910001950 potassium oxide Inorganic materials 0.000 claims abstract description 7
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 7
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910001948 sodium oxide Inorganic materials 0.000 claims abstract description 7
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000292 calcium oxide Substances 0.000 claims abstract description 5
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 5
- GHLITDDQOMIBFS-UHFFFAOYSA-H cerium(3+);tricarbonate Chemical compound [Ce+3].[Ce+3].[O-]C([O-])=O.[O-]C([O-])=O.[O-]C([O-])=O GHLITDDQOMIBFS-UHFFFAOYSA-H 0.000 claims abstract description 4
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910001635 magnesium fluoride Inorganic materials 0.000 claims abstract description 4
- 150000003839 salts Chemical class 0.000 claims abstract description 4
- 229910052814 silicon oxide Inorganic materials 0.000 claims abstract description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- 239000010881 fly ash Substances 0.000 claims description 14
- 238000005352 clarification Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000012752 auxiliary agent Substances 0.000 claims description 10
- 239000002131 composite material Substances 0.000 claims description 10
- 229910002651 NO3 Inorganic materials 0.000 claims description 7
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 7
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims description 7
- 229910001864 baryta Inorganic materials 0.000 claims description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- 238000000498 ball milling Methods 0.000 claims description 6
- 210000000988 bone and bone Anatomy 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000003837 high-temperature calcination Methods 0.000 claims description 3
- 239000000395 magnesium oxide Substances 0.000 claims description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 239000011521 glass Substances 0.000 abstract description 8
- 235000012239 silicon dioxide Nutrition 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 238000010335 hydrothermal treatment Methods 0.000 abstract description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 4
- 239000011707 mineral Substances 0.000 abstract 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 229910001570 bauxite Inorganic materials 0.000 abstract 1
- 229910001576 calcium mineral Inorganic materials 0.000 abstract 1
- 239000002241 glass-ceramic Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000005995 Aluminium silicate Substances 0.000 description 2
- PZZYQPZGQPZBDN-UHFFFAOYSA-N aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 230000005574 cross-species transmission Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229960001866 silicon dioxide Drugs 0.000 description 2
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 2
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Glass Compositions (AREA)
Abstract
The invention discloses a bottle parison material for a low-calcium thermos. The bottle parison material is prepared from the raw materials in parts by weight: 30-40 parts of silica, 50-60 parts of low-calcium mineral slag, 15-20 parts of silicon oxide, 15-20 parts of bauxite, 5-7 parts of sodium oxide, 4-5 parts of zinc oxide, 4-5 parts of potassium oxide, 1-2 parts of antimony trioxide, 0.1-0.14 part of cerium carbonate, 2-4 parts of magnesium fluoride, 2-4 parts of salt and 2-4 parts of compound clarifier. As the calcium content of the traditional mineral slag is high, silicon dioxide can also be added in some traditional mineral slag to be used for preparing glass-ceramics. With the adoption of the bottle parison material, after hydrothermal treatment of the mineral slag, ammonia water is added, the generation of calcium oxide can be promoted; calcium oxide is filtered and removed, and the calcium content can be obviously lowered, so that the usage field of the mineral slag can be broadened, and the condition of manufacturing ordinary glasses can also be satisfied.
Description
Technical field
The present invention relates generally to a kind of low calcium thermos flask bottle base material, belongs to glass material field.
Background technology
Traditional thermos flask bottle base is taking silicon-dioxide as major ingredient, add several oxide compounds to be mixed, physical strength is not high, cause using, in the process of transport than the waste that is easier to break, causes resource, some thermostabilitys are not strong, cannot adapt to for a long time boiling water environment, not only easily break, may damage in addition personnel safety.
Summary of the invention
The object of the invention is just to provide a kind of low calcium thermos flask bottle base material.
The present invention is achieved by the following technical solutions:
A kind of low calcium thermos flask bottle base material, it is made up of the raw material of following weight parts:
Silica 30-40, low calcium slag 50-60, silicon oxide 15-20, bauxitic clay 15-20, sodium oxide 5-7, zinc oxide 4-5, potassium oxide 4-5, antimonous oxide 1-2, cerous carbonate 0.1-0.14, magnesium fluoride 2-4, salt 2-4, composite clarification auxiliary agent 2-4;
Described low calcium slag is that slag is joined in 3-4 water doubly, and rising temperature is 60-70 DEG C, adds ammoniacal liquor, leaves standstill 1-2 hour, filters, and dries;
After described ammoniacal liquor joins in above-mentioned water, ensure that ammonia concn is between 15-30%;
Described composite clarification auxiliary agent is made up of the raw material of following weight parts:
The sulfuric acid 100 of flyash 25-30, sodium carbonate 8-14, bone black 1-2, nitrate of baryta 4-7,50-60%, zinc oxide 0.8-1;
(1), by flyash deironing after high-temperature calcination, make the component content in selected flyash be
50%≤SiO
2≤ 70%, 30%≤AL2O3≤40%, surplus is calcium oxide, magnesium oxide, sodium oxide, potassium oxide etc.;
(2) by above-mentioned flyash and sodium carbonate mixed grinding, put into retort furnace 800-850 DEG C of calcining 1-2 hour, take out rear and bone black mixed grinding, add above-mentioned sulfuric acid, be uniformly mixed, be placed in 90-100 DEG C of water-bath and heat 1-2 hour, discharging is cooling, put at baking oven 120-130 DEG C and dry, being ground to fineness is 1-2 μ m;
(3) above-mentioned nitrate of baryta, zinc oxide are mixed, ball milling, sieves, and obtains particle diameter 0.5-1.5mm;
(4) above-mentioned each raw material after treatment is mixed, ball milling is abundant, obtains described composite clarification auxiliary agent.
Advantage of the present invention is:
Traditional slag is because its calcium content is higher, what have can add silicon-dioxide again, be used for producing devitrified glass, the present invention, by after slag hydrothermal treatment consists, adds ammoniacal liquor, can promote the generation of calcium hydroxide, filter and remove, can obviously reduce calcium contents, can widen the use field of slag, also meet the condition of making simple glass simultaneously.
The composite clarification auxiliary agent that the present invention uses, by the reaction treatment of flyash and sodium carbonate and sulfuric acid, make to contain Tai-Ace S 150 in the material after drying, pure aluminium silicate etc., the thermostability that wherein pure aluminium silicate can reinforcing glass, meet the heat demand of thermos flask, Tai-Ace S 150 heats and can decomposite sulphur trioxide at 770 DEG C, the unreacted completely each composition in flyash can be used as the base-material of glass, zinc oxide mixes use with nitrate of baryta, put oxygen ability strong, each gas can enter in the bubble of melten glass liquid in different periods, make bubble volume constantly increase floating and discharge liquid level, thereby the clarification of playing.
Embodiment
Embodiment 1
A kind of low calcium thermos flask bottle base material, it by following weight parts (kilogram) raw material form:
Silica 40, low calcium slag 60, silicon oxide 20, bauxitic clay 20, sodium oxide 7, zinc oxide 5, potassium oxide 4, antimonous oxide 2, cerous carbonate 0.14, magnesium fluoride 2, salt 2, composite clarification auxiliary agent 4;
Described low calcium slag is that slag is joined in 3-4 water doubly, and rising temperature is 70 DEG C, adds ammoniacal liquor, leaves standstill 1 hour, filters, and dries;
After described ammoniacal liquor joins in above-mentioned water, ensure that ammonia concn is between 30%;
Described composite clarification auxiliary agent is made up of the raw material of following weight parts:
Flyash 30, sodium carbonate 14, bone black 2, nitrate of baryta 7,60% sulfuric acid 100, zinc oxide 0.8;
(1), by flyash deironing after high-temperature calcination, make the component content in selected flyash be
50%≤SiO
2≤ 70%, 30%≤AL2O3≤40%, surplus is calcium oxide, magnesium oxide, sodium oxide, potassium oxide etc.;
(2) by above-mentioned flyash and sodium carbonate mixed grinding, put into 850 DEG C of calcinings of retort furnace 2 hours, take out rear and bone black mixed grinding, add above-mentioned sulfuric acid, be uniformly mixed, be placed in 100 DEG C of water-baths and heat 2 hours, discharging is cooling, puts at 130 DEG C, baking oven and dries, and being ground to fineness is 2 μ m;
(3) above-mentioned nitrate of baryta, zinc oxide are mixed, ball milling, sieves, and obtains particle diameter 1.5mm;
(4) above-mentioned each raw material after treatment is mixed, ball milling is abundant, obtains described composite clarification auxiliary agent.
Heat-resisting shock property test:
More than keeping 30min at ambient temperature by beginning to speak with the thermos flask that bottle base material of the present invention makes, fill with boiling water to spill-over, maintain 1min, at the time of the no more than 10s water that reduces phlegm and internal heat, pour at once the cold water of 5 DEG C, to spill-over, place 30s, pour out cold water, check that glass liner has or not cracking:
As a result, without cracking.
Claims (1)
1. a low calcium thermos flask bottle base material, is characterized in that what it was made up of the raw material of following weight parts:
Silica 30-40, low calcium slag 50-60, silicon oxide 15-20, bauxitic clay 15-20, sodium oxide 5-7, zinc oxide 4-5, potassium oxide 4-5, antimonous oxide 1-2, cerous carbonate 0.1-0.14, magnesium fluoride 2-4, salt 2-4, composite clarification auxiliary agent 2-4;
Described low calcium slag is that slag is joined in 3-4 water doubly, and rising temperature is 60-70 DEG C, adds ammoniacal liquor, leaves standstill 1-2 hour, filters, and dries;
After described ammoniacal liquor joins in above-mentioned water, ensure that ammonia concn is between 15-30%;
Described composite clarification auxiliary agent is made up of the raw material of following weight parts:
The sulfuric acid 100 of flyash 25-30, sodium carbonate 8-14, bone black 1-2, nitrate of baryta 4-7,50-60%, zinc oxide 0.8-1;
(1), by flyash deironing after high-temperature calcination, make the component content in selected flyash be
50%≤SiO
2≤ 70%, 30%≤AL2O3≤40%, surplus is calcium oxide, magnesium oxide, sodium oxide, potassium oxide etc.;
(2) by above-mentioned flyash and sodium carbonate mixed grinding, put into retort furnace 800-850 DEG C of calcining 1-2 hour, take out rear and bone black mixed grinding, add above-mentioned sulfuric acid, be uniformly mixed, be placed in 90-100 DEG C of water-bath and heat 1-2 hour, discharging is cooling, put at baking oven 120-130 DEG C and dry, being ground to fineness is 1-2 μ m;
(3) above-mentioned nitrate of baryta, zinc oxide are mixed, ball milling, sieves, and obtains particle diameter 0.5-1.5mm;
(4) above-mentioned each raw material after treatment is mixed, ball milling is abundant, obtains described composite clarification auxiliary agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410190568.4A CN104016588B (en) | 2014-05-07 | 2014-05-07 | A kind of low calcium thermos flask bottle base material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410190568.4A CN104016588B (en) | 2014-05-07 | 2014-05-07 | A kind of low calcium thermos flask bottle base material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104016588A true CN104016588A (en) | 2014-09-03 |
| CN104016588B CN104016588B (en) | 2016-07-13 |
Family
ID=51433647
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410190568.4A Expired - Fee Related CN104016588B (en) | 2014-05-07 | 2014-05-07 | A kind of low calcium thermos flask bottle base material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104016588B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005052208A (en) * | 2003-08-05 | 2005-03-03 | Nippon Electric Glass Co Ltd | Glass lined for sealing metal vacuum double container |
| CN103356082A (en) * | 2013-08-01 | 2013-10-23 | 顺帆家庭用品(南通)有限公司 | Production process of pink glass liner |
| CN103626384A (en) * | 2013-11-27 | 2014-03-12 | 顺帆家庭用品(南通)有限公司 | Production process of liquid-level-visible glass liner |
-
2014
- 2014-05-07 CN CN201410190568.4A patent/CN104016588B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005052208A (en) * | 2003-08-05 | 2005-03-03 | Nippon Electric Glass Co Ltd | Glass lined for sealing metal vacuum double container |
| CN103356082A (en) * | 2013-08-01 | 2013-10-23 | 顺帆家庭用品(南通)有限公司 | Production process of pink glass liner |
| CN103626384A (en) * | 2013-11-27 | 2014-03-12 | 顺帆家庭用品(南通)有限公司 | Production process of liquid-level-visible glass liner |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104016588B (en) | 2016-07-13 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wang Hongliang Inventor before: Xue Zonghong |
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| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160613 Address after: 233200, No. 22, North Zhao village, former Sun Village, Zhang Qiao Town, Dingyuan County, Chuzhou, Anhui Applicant after: Wang Hongliang Address before: 233200, No. 132 Renhe street, Dingyuan County, Chuzhou, Anhui Applicant before: Xue Zonghong |
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Inventor after: Sun Mingxiu Inventor before: Wang Hongliang |
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Effective date of registration: 20170804 Address after: 253612 Shandong city of Dezhou province Leling city Lazi Lou Zhen Sun Village No. 81 Patentee after: Sun Mingxiu Address before: 233200, No. 22, North Zhao village, former Sun Village, Zhang Qiao Town, Dingyuan County, Chuzhou, Anhui Patentee before: Wang Hongliang |
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Granted publication date: 20160713 Termination date: 20180507 |
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| CF01 | Termination of patent right due to non-payment of annual fee |