CN104003607B - Glass microbead segmentation spheroidizing process and spheroidizing gun - Google Patents

Glass microbead segmentation spheroidizing process and spheroidizing gun Download PDF

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Publication number
CN104003607B
CN104003607B CN201410224192.4A CN201410224192A CN104003607B CN 104003607 B CN104003607 B CN 104003607B CN 201410224192 A CN201410224192 A CN 201410224192A CN 104003607 B CN104003607 B CN 104003607B
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nodularization
spheroidizing
glass microballoon
flame
oxygen
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CN104003607A (en
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王世杰
査伟强
章学文
邱尚皇
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Zhejiang Xinghua New Materials Group Co ltd
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HANGZHOU CHINASTARS REFLECTIVE MATERIAL CO Ltd
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Abstract

The invention relates to a glass microbead segmentation spheroidizing process capable of being less in glass microbead combination, less in crystal separation phenomenon and uniform in particle diameter distribution, and a spheroidizing gun. The spheroidizing process comprises the following steps: segmenting smashed SiO2 or Al2O3 with the particle diameter of 10mu m to 100mu m into three segments according to the particle diameters of 10mu m to 40mu m, 40mu m to 70mu m and 70mu m to 100mu m and then spheroidizing, namely, carrying out continuous spheroidizing production by regulating a flame temperature within 1500 DEG C to 1800 DEG C due to a small specific surface area and a weak spheroidizing flame during the spheroidizing of the fine material with the particle diameter of 10mu m to 40mu m; carrying out the continuous spheroidizing production by regulating the flame temperature within 1800 DEG C to 2100 DEG C due to a large specific surface area and a relatively strong spheroidizing flame during the spheroidizing of the fine material with the particle diameter of 40mu m to 70mu m; carrying out the continuous spheroidizing production by regulating the flame temperature within 2100 DEG C to 2500 DEG C due to the large specific surface area and the relatively strong spheroidizing flame during the spheroidizing of the fine material with the particle diameter of 70mu m to 100mu m.

Description

Glass microballoon is segmented spheroidizing process and nodularization rifle
Technical field
The present invention relates to can make in a kind of glass microballoon segmentation spheroidizing process glass microballoon and pearl is few, crystallization is few, The more uniform glass microballoon segmentation spheroidizing process of particle diameter distribution and nodularization rifle, category glass microballoon manufacture field.
Background technology
CN203333461U, title " glass microballoon burner " include delivery pipe, oxygen hose, Gas Pipe, feed opening, and it is special Levy and be:Described feed opening is arranged at the end of delivery pipe and connects with conveying tube cavity, and described oxygen hose is arranged at The bottom of conveying tube cavity, described oxygen tube head is more than described feed opening and delivery pipe with conveying bottom of the tube apart from A Bottom apart from B, described Gas Pipe is arranged in the cavity wall of delivery pipe.Its weak point:Because Gas Pipe outlet is arranged on On burner horn outlet skew wall, thus both cannot realize between combustion gas and oxygen it is uniform mix, also cannot realize to gaseous mixture The rectification of body, causes combustion flame temperature constant, cause glass microballoon shaping quality it cannot be guaranteed that.
The content of the invention
Purpose of design:Avoid the weak point in background technology, design one kind can make glass microballoon and pearl is few, crystallize is existing As less, particle diameter distribution more uniform glass microballoon segmentation spheroidizing process and nodularization rifle.
Design:In order to realize above-mentioned purpose of design.1st, the raw material for adopting is the material powder after segmentation, is pressed Carry out the design of nodularization respectively according to carse, medium and small 3 particle diameter sections or thick, thin 2 particle diameter sections, be the present invention technical characteristic it One.So design purpose be:If carse, medium and small or thick, fine grain section material powder is carried out into nodularization, work as glass Microballon is in certain flame nodularization because coarse fodder and fines are mixed, it may appear that fines superfusion causes and pearl, coarse fodder ball Change deficiency and cause the not good phenomenon of physical property, and the present invention carries out being segmented nodularization due to big by the material of nodularization to glass microballoon It is little relatively uniform, superfusion phenomenon both will not occur, the not good phenomenon of nodularization physical property also will not occur.2nd, combustion gas in nodularization rifle First mixing between oxygen, rear rectification, the design for spraying combustion technology scheme again, be the present invention technical characteristic two.So set The purpose of meter is:Both realized between combustion gas and oxygen and uniformly mixed, and made combustion gas stream obtain rectification before combustion again, it is ensured that The concordance of ignition temperature and the concordance of combustion gas stream, and then make the quality of nodularization glass microballoon obtain the raising of essence.
Technical scheme 1:A kind of glass microballoon is segmented spheroidizing process, using 10-100 μm of SiO2 or Al2O3Grinding bodies is pressed According to 10-40 μm of particle diameter, 40-70 μm, being divided into three sections after 70-100 μm of segmentation carries out respectively nodularization, when using 10-40 μm of fines ball During change, because specific surface area is less, nodularization flame is relatively small, continuous balling production when adjusting flame temperature 1500-1800 DEG C; When coarse fodder nodularization in using 40-70 μm, because specific surface area is larger, nodularization flame is relatively large, adjusts flame temperature 1800- 2100 DEG C of continuous balling productions;When using 70-100 μm of coarse fodder nodularization, because specific surface area is larger, nodularization flame is relatively Greatly, the production of flame temperature 2100-2500 DEG C continuous balling is adjusted.
Technical scheme 2:A kind of glass microballoon is segmented nodularization rifle, and gun body top is connected with blanking bin by blanking control valve, Gun body tail end is respectively equipped with oxygen air inlet and gas inlet, and oxygen air inlet connects with the oxygen control valve being located in the middle part of gun body Logical, gas inlet is connected with the gas control valve in the middle part of gun body, and gun barrel end is equipped with rifle mouth.
Compared with background technology, one is to solve cannot uniformly mix between the combustion gas of background technology presence and oxygen to the present invention Close, cannot combustion flame temperature caused by rectification can not be constant, the glass microballoon shaping unwarrantable defect of quality caused by institute; Two is to solve occur during glass microballoon nodularization and pearl and the unwarrantable defect of nodularization physical property.
Description of the drawings
Fig. 1 is the schematic diagram that glass microballoon is segmented nodularization rifle.
Specific embodiment
Embodiment 1:Referring to the drawings 1.A kind of glass microballoon is segmented nodularization rifle, and the top of gun body 10 passes through blanking with blanking bin 1 Control valve 2 is connected, and in gun body 10 combustion gas, oxygen mix chamber are provided with, and gun body tail end is respectively equipped with oxygen air inlet 3 and gas inlet Mouth 4, the oxygen air inlet 3 is connected with the oxygen control valve 6 in the middle part of gun body, and oxygen control valve 6 exports straight to combustion gas, oxygen Hybrid chamber, according to required flame temperature, by the regulation to oxygen control valve 6, can efficiently control the quantity delivered of oxygen;Combustion Gas air inlet 4 is connected with the gas control valve 7 in the middle part of gun body, and gas control valve 7 exports straight to combustion gas, oxygen mix chamber, According to required flame temperature, the quantity delivered of fuel gas can be efficiently controlled;Gun barrel one end connects with combustion gas, oxygen mix chamber It is logical, gun barrel(It is another)End is equipped with rifle mouth 8, and gun barrel tube core is that mixed gas accelerate rectification passage.Feeding oxygen valve is provided with gun body 1 5, the feeding oxygen valve 5 forces the outlet of oxygenating valve directly to material to force oxygenating valve, makes material first quilt before into gun body intracavity Oxygen is cladded, to improve the Spheroidization quality of material.Oxygen control valve 6 and the export department of gas control valve 7 are gas mixer chamber.Gun body Gun barrel in 1 is that mixed gas accelerate rectification passage.The gas outlet of rifle mouth 8 is tubaeform in extending out.The flame hole of pipette tips has 5-20 Mouth number, bore is 0.3-3.0mm.The flame of label 9. in figure.
Embodiment 2:On the basis of embodiment 1, a kind of glass microballoon is segmented spheroidizing process, using 10-100 μm of SiO2 Or Al2O3According to 10-40 μm of particle diameter, 40-70 μm, be divided into three sections after 70-100 μm of segmentation carries out respectively nodularization to grinding bodies, when adopting With during 10-40 μm of fines nodularization, because specific surface area is less, nodularization flame is relatively small, adjusts flame temperature 1500-1800 DEG C When continuous balling production;When coarse fodder nodularization in using 40-70 μm, because specific surface area is larger, nodularization flame is relatively large, adjusts The continuous balling production of section flame temperature 1800-2100 DEG C;When using 70-100 μm of coarse fodder nodularization, due to specific surface area it is larger, Nodularization flame is relatively large, adjusts the production of flame temperature 2100-2500 DEG C continuous balling.The inlet pressure control of oxygen and combustion gas System is in 0.1-2.0MPa.Oxygen inlet speed controlling is in 0.1-10m/s, combustion gas inlet velocity control station 0.1-10m/s.
Embodiment 3:On the basis of embodiment 2, when using 10-40 μm of fines nodularization, flame temperature 1500- is adjusted 1800 DEG C, blanking velocity is 500-1000g/min.
Embodiment 4:On the basis of embodiment 2, when using 40-70 μm of fines nodularization, flame temperature 1800- is adjusted 2100 DEG C, blanking velocity is 1000-2000g/min.
Embodiment 5:On the basis of embodiment 2, when using 70-100 μm of fines nodularization, flame temperature 2100- is adjusted 2500 DEG C, blanking velocity is 2000-3000g/min.
Embodiment 6:On the basis of embodiment 2, when using fines nodularization, due to specific surface area it is larger, nodularization flame It is relatively large, flame length control in 30-60cm, adjust flame reach nodularization it is optimal when can continuously produce;When adopting coarse fodder During nodularization, because specific surface area is less, nodularization flame is relatively small, and flame length control adjusts flame and reach most in 10-40cm Can continuously produce during good nodularization flame.
It is to be understood that:Although above-described embodiment is contrasted to the mentality of designing of the present invention, detailed word is retouched State, but these word descriptions, simply the simple text of mentality of designing of the present invention is described, rather than to mentality of designing of the present invention Restriction, any combination without departing from mentality of designing of the present invention, increase or change, each fall within protection scope of the present invention.

Claims (6)

1. a kind of glass microballoon is segmented the preparation technology of nodularization, it is characterized in that:Using 10-100 μm of SiO2 or Al2O3 powder Broken body 40-70 μm, is divided into three sections respectively in glass microballoon segmentation nodularization rifle according to 10-40 μm of particle diameter after 70-100 μm of segmentation Nodularization is carried out, when using 10-40 μm of fines nodularization, nodularization flame is relatively small, when adjusting flame temperature 1500-1800 DEG C Continuous balling is produced, and blanking velocity is 500-1000g/min;When coarse fodder nodularization in using 40-70 μm, nodularization flame is relative It is larger, the production of flame temperature 1800-2100 DEG C continuous balling is adjusted, blanking velocity is 1000-2000g/min;When adopting 70- During 100 μm of coarse fodder nodularizations, nodularization flame is relatively large, adjusts the production of flame temperature 2100-2400 DEG C continuous balling, blanking speed Spend for 2000-3000g/min;Described glass microballoon segmentation nodularization rifle, including gun body(10)Top and blanking bin(1)Pass through Blanking control valve(2)Connection, gun body tail end is respectively equipped with oxygen air inlet(3)And gas inlet(4), oxygen air inlet(3) With the oxygen control valve in the middle part of gun body(6)Connection, gas inlet(4)With the gas control valve in the middle part of gun body(7) Connection, gun barrel end is equipped with rifle mouth(8), the gun body(10)In be provided with feeding oxygen valve(5), oxygen control valve(6)With combustion gas control Valve processed(7)Export department is gas mixer chamber.
2. the glass microballoon according to claim 1 is segmented the preparation technology of nodularization, it is characterized in that:The glass microballoon point The gun body of section nodularization rifle(10)In gun barrel be mixed gas accelerate rectification passage.
3. the glass microballoon according to claim 1 is segmented the preparation technology of nodularization, it is characterized in that:The glass microballoon point The rifle mouth of section nodularization rifle(8)Gas outlet is tubaeform in extending out.
4. the glass microballoon according to claim 1 is segmented the preparation technology of nodularization, it is characterized in that:The glass microballoon point The flame hole of the pipette tips of section nodularization rifle has 5-20 mouth number, and bore is 0.3-3.0mm.
5. the glass microballoon according to claim 1 is segmented the preparation technology of nodularization, it is characterized in that:Oxygen and combustion gas Inlet pressure is controlled in 0.1-2.0MPa.
6. the glass microballoon according to claim 1 is segmented the preparation technology of nodularization, it is characterized in that:Oxygen inlet speed control System is controlled in 0.1-10m/s in 0.1-10m/s, combustion gas inlet velocity.
CN201410224192.4A 2014-05-26 2014-05-26 Glass microbead segmentation spheroidizing process and spheroidizing gun Active CN104003607B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110919013A (en) * 2019-12-11 2020-03-27 湖南天际智慧材料科技有限公司 Metal powder flame spheroidizing equipment and processing technology thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202322397U (en) * 2011-11-19 2012-07-11 蚌埠中凯电子材料有限公司 Full-oxygen combustor for balling powdery materials
CN202482194U (en) * 2012-02-08 2012-10-10 马浪超 Glass bead combustor
CN103319075A (en) * 2013-07-01 2013-09-25 浙江龙游道明光学有限公司 Glass bead combustor
CN203922986U (en) * 2014-05-26 2014-11-05 杭州星华反光材料有限公司 Glass microballon segmentation nodularization rifle

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202322397U (en) * 2011-11-19 2012-07-11 蚌埠中凯电子材料有限公司 Full-oxygen combustor for balling powdery materials
CN202482194U (en) * 2012-02-08 2012-10-10 马浪超 Glass bead combustor
CN103319075A (en) * 2013-07-01 2013-09-25 浙江龙游道明光学有限公司 Glass bead combustor
CN203922986U (en) * 2014-05-26 2014-11-05 杭州星华反光材料有限公司 Glass microballon segmentation nodularization rifle

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