CN103992859B - A kind of antibacterial type slushing oil - Google Patents
A kind of antibacterial type slushing oil Download PDFInfo
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- CN103992859B CN103992859B CN201410171260.5A CN201410171260A CN103992859B CN 103992859 B CN103992859 B CN 103992859B CN 201410171260 A CN201410171260 A CN 201410171260A CN 103992859 B CN103992859 B CN 103992859B
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- slushing oil
- auxiliary agent
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 10
- OCBHHZMJRVXXQK-UHFFFAOYSA-M benzyl-dimethyl-tetradecylazanium;chloride Chemical compound [Cl-].CCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 OCBHHZMJRVXXQK-UHFFFAOYSA-M 0.000 claims abstract description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 8
- 239000000194 fatty acid Substances 0.000 claims abstract description 8
- 229930195729 fatty acid Natural products 0.000 claims abstract description 8
- -1 fatty acid ester Chemical class 0.000 claims abstract description 8
- JPMIIZHYYWMHDT-UHFFFAOYSA-N octhilinone Chemical compound CCCCCCCCN1SC=CC1=O JPMIIZHYYWMHDT-UHFFFAOYSA-N 0.000 claims abstract description 8
- DKIDEFUBRARXTE-UHFFFAOYSA-N 3-mercaptopropanoic acid Chemical compound OC(=O)CCS DKIDEFUBRARXTE-UHFFFAOYSA-N 0.000 claims abstract description 7
- HMVCFZCJPVUFQG-UHFFFAOYSA-N C(CCCCCCCCCCCCCCCCC)(=O)N.C(CCCCCCCCCCCCCCCCC)(=O)N.OCCC=C Chemical compound C(CCCCCCCCCCCCCCCCC)(=O)N.C(CCCCCCCCCCCCCCCCC)(=O)N.OCCC=C HMVCFZCJPVUFQG-UHFFFAOYSA-N 0.000 claims abstract description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 241000158728 Meliaceae Species 0.000 claims abstract description 7
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 7
- 239000011575 calcium Substances 0.000 claims abstract description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 7
- 239000003350 kerosene Substances 0.000 claims abstract description 4
- 229920000223 polyglycerol Polymers 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims description 22
- KPAPHODVWOVUJL-UHFFFAOYSA-N 1-benzofuran;1h-indene Chemical compound C1=CC=C2CC=CC2=C1.C1=CC=C2OC=CC2=C1 KPAPHODVWOVUJL-UHFFFAOYSA-N 0.000 claims description 6
- QDCPNGVVOWVKJG-VAWYXSNFSA-N 2-[(e)-dodec-1-enyl]butanedioic acid Chemical compound CCCCCCCCCC\C=C\C(C(O)=O)CC(O)=O QDCPNGVVOWVKJG-VAWYXSNFSA-N 0.000 claims description 6
- 239000001089 [(2R)-oxolan-2-yl]methanol Substances 0.000 claims description 6
- 239000002199 base oil Substances 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000011347 resin Substances 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- BSYVTEYKTMYBMK-UHFFFAOYSA-N tetrahydrofurfuryl alcohol Chemical compound OCC1CCCO1 BSYVTEYKTMYBMK-UHFFFAOYSA-N 0.000 claims description 6
- NHXVNEDMKGDNPR-UHFFFAOYSA-N zinc;pentane-2,4-dione Chemical compound [Zn+2].CC(=O)[CH-]C(C)=O.CC(=O)[CH-]C(C)=O NHXVNEDMKGDNPR-UHFFFAOYSA-N 0.000 claims description 6
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000006722 reduction reaction Methods 0.000 claims description 2
- 241000894006 Bacteria Species 0.000 abstract description 2
- 208000027418 Wounds and injury Diseases 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 230000006378 damage Effects 0.000 abstract description 2
- 230000001408 fungistatic effect Effects 0.000 abstract description 2
- 208000014674 injury Diseases 0.000 abstract description 2
- 230000003245 working effect Effects 0.000 abstract description 2
- 150000002576 ketones Chemical class 0.000 abstract 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of antibacterial type slushing oil, it is made up of the raw material of following weight parts: dewaxing kerosene 60-70, hydroxyethyl ethylene bis stearamide 1-2, 2-n-octyl-4-isothiazoline-3-? ketone 0.7-1, 3-thiohydracrylic acid 0.5-1, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, polyglycerol fatty acid ester 3-4, calcium mahogany sulfonate 3-5, sorbitan fatty acid ester 0.3-1, antirust auxiliary agent 5-7, irgasfos 168? 0.3-1, the Kathon that slushing oil of the present invention adds, myristyl benzyl dimethyl ammonium chloride etc. all has good fungistatic effect, the absorption to bacterium can be reduced, reduce the injury to oil film, increase the work-ing life of slushing oil.
Description
Technical field
The present invention relates generally to lubricating oil field, particularly relates to a kind of antibacterial type slushing oil.
Background technology
Slushing oil is oil based on lubricating oil, adds rust-preventive agent wherein and some improve additive and making.Usual slushing oil can be divided into displacing type rust preventive oil, lubricating type rust preventing oil, solvent cutback rust preventing oil etc.Wherein, lubricating type rust preventing oil is the main slushing oil kind of China, and its use range is very wide, and it is antirust to be mainly used in machine internal, lubricates use immediately after may be used for rust-proof seal and unpacking.In addition, this product also goes for the use of the antirust and lubrication of the operation friction working face of various machinery, especially, friction position on harbour machinery, ship machinery is widely used, such as wireline etc., slushing oil Problems existing of today is also a lot, such as corrosion-resistant, weather resistance, tackiness, bad, the phenomenon that easy appearance is hardening, come off, ftracture, the overall quality therefore improving constantly slushing oil also has for social development and well promotes meaning.
Summary of the invention
The object of the invention is just to provide a kind of antibacterial type slushing oil.
The present invention is achieved by the following technical solutions:
A kind of antibacterial type slushing oil, is characterized in that what it was made up of the raw material of following weight parts:
Dewaxing kerosene 60-70, hydroxyethyl ethylene bis stearamide 1-2, Kathon 0.7-1,3-thiohydracrylic acid 0.5-1, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, polyglycerol fatty acid ester 3-4, calcium mahogany sulfonate 3-5, sorbitan fatty acid ester 0.3-1, antirust auxiliary agent 5-7, irgasfos 168 0.3-1;
Described antirust auxiliary agent is made up of the raw material of following weight parts:
Coumarone indene resin 26-30, tetrahydrofurfuryl alcohol 4-5, zinc acetylacetonate 0.6-1, dodecenylsuccinic acid half ester 3-5,150SN base oil 11-19, Viscoat 295 2-3;
Above-mentioned coumarone indene resin is heated to 75-80 DEG C, adds zinc acetylacetonate, be uniformly mixed 10-15 minute, add tetrahydrofurfuryl alcohol, be stirred to normal temperature;
The 30-40% of 150SN base oil weight is mixed with dodecenylsuccinic acid half ester, is uniformly mixed 1-2 hour at 100-110 DEG C;
By each raw material mixing after above-mentioned process, add each raw material of residue, 100-200 rev/min of dispersed with stirring 30-50 minute, obtains described antirust auxiliary agent.
A preparation method for antibacterial type slushing oil, comprises the following steps:
(1) by above-mentioned hydroxyethyl ethylene bis stearamide, myristyl benzyl dimethyl ammonium chloride, calcium mahogany sulfonate mixing, insulated and stirred 1-2 hour at 80-100 DEG C;
(2) add 3-thiohydracrylic acid, Kathon, continue to be uniformly mixed 1-2 hour;
(3) add each raw material of residue, stir, dehydration, reduction temperature is 30-40 DEG C, filters discharging.
Advantage of the present invention is:
The Kathon that slushing oil of the present invention adds, myristyl benzyl dimethyl ammonium chloride etc. all have good fungistatic effect, can reduce the absorption to bacterium, reduce the injury to oil film, increase the work-ing life of slushing oil.
Embodiment
Embodiment 1
A kind of antibacterial type slushing oil, is characterized in that what it was made up of the raw material of following weight parts (kilogram):
Dewaxing kerosene 60, hydroxyethyl ethylene bis stearamide 2, Kathon 0.7,3-thiohydracrylic acid 0.5, myristyl benzyl dimethyl ammonium chloride 0.2, polyglycerol fatty acid ester 3, calcium mahogany sulfonate 3, sorbitan fatty acid ester 0.3, antirust auxiliary agent 5, irgasfos 168 0.3;
Described antirust auxiliary agent is made up of the raw material of following weight parts:
Coumarone indene resin 30, tetrahydrofurfuryl alcohol 4, zinc acetylacetonate 0.6, dodecenylsuccinic acid half ester 5,150SN base oil 19, Viscoat 295 2;
Above-mentioned coumarone indene resin is heated to 80 DEG C, adds zinc acetylacetonate, be uniformly mixed 15 minutes, add tetrahydrofurfuryl alcohol, be stirred to normal temperature;
Mix 40% of 150SN base oil weight with dodecenylsuccinic acid half ester, be uniformly mixed 1 hour at 110 DEG C;
By each raw material mixing after above-mentioned process, add each raw material of residue, 200 revs/min of dispersed with stirring 50 minutes, obtain described antirust auxiliary agent.
A preparation method for antibacterial type slushing oil, comprises the following steps:
(1) by above-mentioned hydroxyethyl ethylene bis stearamide, myristyl benzyl dimethyl ammonium chloride, calcium mahogany sulfonate mixing, insulated and stirred 1 hour at 100 DEG C;
(2) add 3-thiohydracrylic acid, Kathon, continue to be uniformly mixed 1 hour;
(3) add each raw material of residue, stir, dehydration, reducing temperature is 30 DEG C, filters discharging.
Performance test:
Apparent: without precipitation, to separate out without layering, nodeless mesh thing;
Corrosion test (10# steel, 100h, 100 DEG C): 0 grade;
Salt mist experiment (10# steel A level): 7 days;
Damp and hot experiment (10# steel A level): 20 days;
Low-temperature adhesion: qualified.
Claims (1)
1. an antibacterial type slushing oil, is characterized in that what it was made up of the raw material of following weight parts:
Dewaxing kerosene 60-70, hydroxyethyl ethylene bis stearamide 1-2, Kathon 0.7-1,3-thiohydracrylic acid 0.5-1, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, polyglycerol fatty acid ester 3-4, calcium mahogany sulfonate 3-5, sorbitan fatty acid ester 0.3-1, antirust auxiliary agent 5-7, irgasfos 168 0.3-1;
Described antirust auxiliary agent is made up of the raw material of following weight parts:
Coumarone indene resin 26-30, tetrahydrofurfuryl alcohol 4-5, zinc acetylacetonate 0.6-1, dodecenylsuccinic acid half ester 3-5,150SN base oil 11-19, Viscoat 295 2-3;
Above-mentioned coumarone indene resin is heated to 75-80 DEG C, adds zinc acetylacetonate, be uniformly mixed 10-15 minute, add tetrahydrofurfuryl alcohol, be stirred to normal temperature;
The 30-40% of 150SN base oil weight is mixed with dodecenylsuccinic acid half ester, is uniformly mixed 1-2 hour at 100-110 DEG C;
By each raw material mixing after above-mentioned process, add each raw material of residue, 100-200 rev/min of dispersed with stirring 30-50 minute, obtains described antirust auxiliary agent;
The preparation method of described antibacterial type slushing oil comprises the following steps:
(1) by above-mentioned hydroxyethyl ethylene bis stearamide, myristyl benzyl dimethyl ammonium chloride, calcium mahogany sulfonate mixing, insulated and stirred 1-2 hour at 80-100 DEG C;
(2) add 3-thiohydracrylic acid, Kathon, continue to be uniformly mixed 1-2 hour;
(3) add each raw material of residue, stir, dehydration, reduction temperature is 30-40 DEG C, filters discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410171260.5A CN103992859B (en) | 2014-04-25 | 2014-04-25 | A kind of antibacterial type slushing oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410171260.5A CN103992859B (en) | 2014-04-25 | 2014-04-25 | A kind of antibacterial type slushing oil |
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| Publication Number | Publication Date |
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| CN103992859A CN103992859A (en) | 2014-08-20 |
| CN103992859B true CN103992859B (en) | 2016-02-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410171260.5A Active CN103992859B (en) | 2014-04-25 | 2014-04-25 | A kind of antibacterial type slushing oil |
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| Country | Link |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106118824A (en) * | 2016-06-29 | 2016-11-16 | 无锡伊佩克科技有限公司 | A kind of preparation method of solvent cutback soft film anti-rust oil |
| CN109097171B (en) * | 2018-09-25 | 2021-05-28 | 中国石油化工股份有限公司 | Oil film bearing oil composition and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101037636A (en) * | 2006-03-14 | 2007-09-19 | 上海帕卡兴产化工有限公司 | Antirust composition and preparation method thereof |
| CN103374447A (en) * | 2012-04-13 | 2013-10-30 | 启东天地机械制造有限公司 | Bearing slushing oil |
| CN103497805A (en) * | 2013-10-07 | 2014-01-08 | 李阳 | Rust preventive oil and preparation method thereof |
-
2014
- 2014-04-25 CN CN201410171260.5A patent/CN103992859B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101037636A (en) * | 2006-03-14 | 2007-09-19 | 上海帕卡兴产化工有限公司 | Antirust composition and preparation method thereof |
| CN103374447A (en) * | 2012-04-13 | 2013-10-30 | 启东天地机械制造有限公司 | Bearing slushing oil |
| CN103497805A (en) * | 2013-10-07 | 2014-01-08 | 李阳 | Rust preventive oil and preparation method thereof |
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| CN103992859A (en) | 2014-08-20 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20190826 Address after: Moling streets blue Xia Road Jiangning District Nanjing City, Jiangsu Province, No. 2 211111 Patentee after: Wu Yan Address before: 233000 Anhui city of Bengbu province high tech District Road No. 168 Patentee before: BENGBU HONGAN PRECISION MACHINERY Co.,Ltd. |
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| TR01 | Transfer of patent right |
Effective date of registration: 20231208 Address after: 246000, No. 23 Weijiu Road, Daguan District, Anqing City, Anhui Province (south) Patentee after: Anhui Delimei Technology Co.,Ltd. Address before: 211111 No. 2 Lanxia Road, Ziling Street, Jiangning District, Nanjing City, Jiangsu Province Patentee before: Wu Yan |
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| TR01 | Transfer of patent right |