CN103992196B - A kind of special oil phase of heat-sensitized explosive production line and preparation method thereof - Google Patents

A kind of special oil phase of heat-sensitized explosive production line and preparation method thereof Download PDF

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Publication number
CN103992196B
CN103992196B CN201310179921.4A CN201310179921A CN103992196B CN 103992196 B CN103992196 B CN 103992196B CN 201310179921 A CN201310179921 A CN 201310179921A CN 103992196 B CN103992196 B CN 103992196B
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oil phase
waxes
wax
production line
heat
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CN103992196A (en
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张先华
武建安
巫小海
赵仁莲
贾兴慧
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SHAANXI HANYIN HUANENG NEW MATERIALS RESEARCH Co Ltd
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SHAANXI HANYIN HUANENG NEW MATERIALS RESEARCH Co Ltd
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Abstract

A kind of special oil phase of heat-sensitized explosive production line of the present invention and preparation method thereof, relate to the oil phase of emulsion, a kind of special oil phase of heat-sensitized explosive production line and preparation method thereof, a kind of comprehensive function utilizing multiple material is proposed, meet heat-sensitized explosive production and prepare requirement, to substitute the one of similar imported product special oil phase of heat-sensitized explosive production line and preparation method thereof completely.The present invention is mixed by No. 2 waxes, No. 3 wax, soft wax, paraffin, bran wax, machine oil, macromolecule emulsifier, sp--80, soybean phospholipid and erucyl amide.The present invention compares with former imported product, and technique is simple, and without chemical reaction, energy consumption is low, and cost reduces about 30%, and all uses petroleum series product, non-environmental-pollution relevant issues.

Description

A kind of special oil phase of heat-sensitized explosive production line and preparation method thereof
Art
The present invention relates to the oil phase for emulsion, a kind of special oil phase of heat-sensitized explosive production line and preparation method thereof.
Background technology
China people quick-fried production target and direction are big production capacity, low energy consumption, essential safety, automaticity is high, employment is few.Heat-sensitized explosive production line researches and develops the emulsion explosive production line meeting Mirae Corp. of country developing direction, having international most advanced level the most in this context.But this production line used oil phase product to use about 50% import raw material, and uses inconvenience, relatively costly.This technical barrier is artificially captured in application, by test of many times, develops special oil phase of heat-sensitized explosive production line and preparation method thereof.Through retrieval, do not have to find the technical scheme identical with the present invention.
Summary of the invention
The technical problem to be solved in the present invention is: propose a kind of comprehensive function utilizing multiple material, meets heat-sensitized explosive production and prepares requirement, to substitute the one of similar imported product special oil phase of heat-sensitized explosive production line and preparation method thereof completely.
The present invention solves the technical scheme of technical problem:
The special oil phase of the heat-sensitized explosive production line of the present invention, is mixed by No. 2 waxes, No. 3 wax, soft wax, paraffin, bran wax, machine oil, macromolecule emulsifier, sp--80, soybean phospholipid and erucyl amide, and it is characterized by, included proportioning raw materials weight portion is No. 2 complex wax 8 10, No. 3 complex wax 8 10, soft wax 18 23, paraffin 13 18, bran wax 8 12, machine oil 38, macromolecule emulsifier 8 12, sp 808 10, soybean phospholipid 6 12, erucyl amide 0.5 2.
The preparation method of the special oil phase of the heat-sensitized explosive production line of the present invention is:
With No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran wax, machine oil, macromolecule emulsifier, sp 80, soybean phospholipid, erucyl amides as raw material, prepare as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. starting agitator, successively machine oil, macromolecule emulsifier, sp 80, soybean phospholipid are added melting pot, be allowed to stir, after treating that all materials add, constant temperature to holding temperature Celsius is 80 DEG C 100 DEG C, is further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product.
The invention has the beneficial effects as follows:
The present invention compares with former imported product, and technique is simple, and without chemical reaction, energy consumption is low, and cost reduces about 30%, and all uses petroleum series product, non-environmental-pollution relevant issues.
Now a lot of explosive factories use import oil phase also to need scene to be blended into the import microwax of 22%, the existing market price of import microwax is 20,000 yuan/ton, oil phase the most per ton at least increases cost 4400 yuan, oil phase content in emulsion is 6.5%-7.0%, it is 10,000 tons that general explosive factory is produced per year, year, oil phase was 650 tons-700 tons, then year oil phase cost increases by 2,860,000 yuan-308 ten thousand yuan.
The present invention heat-sensitized oil phase product price is less than import oil phase, and easy to use, need not additional import microwax, integrated cost is per ton lower about 5500 yuan than import oil phase, if calculating by just now producing 10000 tons of explosives per year, year oil phase can save production cost about 357.5 ten thousand yuan-385 ten thousand yuan, cost-effective considerable, and steady quality, convenient transportation, procurement cycle is short, and after-sale service is excellent, there is not language, word difference.Use and purchase commodities conveniently.Economic benefits.
The present invention compared with prior art, easily implement by technology.
Detailed description of the invention
Embodiment 1
With No. 2 complex wax 8 kilograms, No. 3 complex wax 8 kilograms, soft wax 18 kilograms, 13 kilograms of paraffin, 8 kilograms of bran wax, 3 kilograms of machine oil, macromolecule emulsifier 8 kilograms, sp 808 kilograms, soybean phospholipid 6 kilograms, erucyl amide 0.5 kilogram is raw material, prepares as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. starting agitator, successively machine oil, macromolecule emulsifier, sp-80, soybean phospholipid are added melting pot, be allowed to stir, after treating that all materials add, constant temperature to holding temperature Celsius is 80 DEG C 100 DEG C, is further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product.
Embodiment 2
With No. 2 complex wax 10 kilograms, No. 3 complex wax 10 kilograms, soft wax 23 kilograms, 18 kilograms of paraffin, 12 kilograms of bran wax, 8 kilograms of machine oil, macromolecule emulsifier 12 kilograms, sp 8010 kilograms, soybean phospholipid 12 kilograms, erucyl amide 2 kilograms is raw material, prepares as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. starting agitator, successively machine oil, macromolecule emulsifier, sp-80, soybean phospholipid are added melting pot, be allowed to stir, after treating that all materials add, constant temperature to holding temperature Celsius is 80 DEG C 100 DEG C, is further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product.
Embodiment 3
With No. 2 complex wax 9 kilograms, No. 3 complex wax 9 kilograms, soft wax 20 kilograms, 15 kilograms of paraffin, 9 kilograms of bran wax, 5 kilograms of machine oil, macromolecule emulsifier 10 kilograms, sp 809 kilograms, soybean phospholipid 8 kilograms, erucyl amide 1 kilogram is raw material, prepares as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. startup agitator, adds melting pot by machine oil, macromolecule emulsifier, sp-80, soybean phospholipid successively, is allowed to stir, and after treating that all materials add, constant temperature to holding temperature Celsius is 80 DEG C 100 DEG C, is further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product.
Embodiment 4
With No. 2 complex wax 10 kilograms, No. 3 complex wax 8 kilograms, soft wax 21 kilograms, 16 kilograms of paraffin, 10 kilograms of bran wax, 6 kilograms of machine oil, macromolecule emulsifier 10 kilogram 2, sp-8010 kilogram, soybean phospholipid 10 kilograms, erucyl amide 1.5 kilograms is raw material, prepares as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. starting agitator, successively machine oil, macromolecule emulsifier, sp-80, soybean phospholipid are added melting pot, be allowed to stir, after treating that all materials add, constant temperature to holding temperature Celsius is 80 DEG C 100 DEG C, is further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product.
Described in the present invention No. 2 and No. 3 complex wax, for the paraffinized plant produced in Nanyang, henan oil field, predominantly petroleum series product.

Claims (1)

1. a preparation method for the special oil phase of heat-sensitized explosive production line, is characterized in that: with No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran wax, machine oil, macromolecule emulsifier, sp--80, soybean phospholipid, erucyl amides as raw material, prepare as follows
1. No. 2 waxes, No. 3 waxes, soft wax, paraffin, bran waxes being put in melting pot, be heated up to 90 DEG C 110 DEG C and be allowed to be completely melt, then start melting pot agitator, stir about 30-50 minute, be allowed to stir, stop stirring, keeping temperature is 90 DEG C 110 DEG C;
2. start agitator, successively machine oil, macromolecule emulsifier, sp-80, soybean phospholipid are added melting pot, be allowed to stir, after treating that all materials add, be cooled to 80 DEG C 100 DEG C and keep temperature Celsius, be further continued for stirring 30 minutes;
3. erucyl amide puts into melting pot, and keeping temperature is 90 DEG C 110 DEG C, stirs 30 minutes;
4. the liquid oil phase being stirred is stood 12 hours, be naturally cooling to room temperature state, be i.e. solidified as waxy solid, obtain heat-sensitized explosive production line special oil phase finished product;
Described proportioning raw materials weight portion is 8 10, No. 3 waxes 8 10 of No. 2 waxes, soft wax 18 23, paraffin 13 18, bran wax 8 12, machine oil 38, macromolecule emulsifier 8 12, sp-808 10, soybean phospholipid 6 12, erucyl amide 0.5 2.
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Publication number Priority date Publication date Assignee Title
CN104370667A (en) * 2014-09-10 2015-02-25 山东凯乐化工有限公司 Emulsion explosive composite oil phase material and preparation method
CN104909966A (en) * 2015-06-30 2015-09-16 葛洲坝易普力湖北昌泰民爆有限公司 Formula of composite oil phase for static emulsified and high-temperature sensitized emulsified explosive
CN104945206B (en) * 2015-06-30 2017-11-24 葛洲坝易普力湖北昌泰民爆有限公司 A kind of heat-sensitized technique Compound oil phase for emulsion explosive and preparation method thereof
CN112521237A (en) * 2020-12-25 2021-03-19 雅化集团雅安实业有限公司 Special emulsifier for liquid integrated oil phase and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101560128A (en) * 2009-05-27 2009-10-21 湖北天神实业股份有限公司 Composite oil phase for emulsion explosive
CN102079681A (en) * 2010-12-15 2011-06-01 广东众和化塑有限公司 Integrated oil phase for emulsion explosive and preparation method thereof
CN102584501A (en) * 2012-01-11 2012-07-18 山东天宝化工有限公司 Special composite oil phase for emulsion explosive and preparation method thereof
CN102603437A (en) * 2012-02-28 2012-07-25 薛世忠 Method for manufacturing emulsion explosive with swill-cooked dirty oil
CN102731229A (en) * 2012-07-17 2012-10-17 辽宁红山化工股份有限公司 Method for preparing special compound oil phase for emulsion explosive
CN103086811A (en) * 2013-02-03 2013-05-08 福建达安能源实业有限责任公司 Special biological grease for powder emulsion explosive

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101560128A (en) * 2009-05-27 2009-10-21 湖北天神实业股份有限公司 Composite oil phase for emulsion explosive
CN102079681A (en) * 2010-12-15 2011-06-01 广东众和化塑有限公司 Integrated oil phase for emulsion explosive and preparation method thereof
CN102584501A (en) * 2012-01-11 2012-07-18 山东天宝化工有限公司 Special composite oil phase for emulsion explosive and preparation method thereof
CN102603437A (en) * 2012-02-28 2012-07-25 薛世忠 Method for manufacturing emulsion explosive with swill-cooked dirty oil
CN102731229A (en) * 2012-07-17 2012-10-17 辽宁红山化工股份有限公司 Method for preparing special compound oil phase for emulsion explosive
CN103086811A (en) * 2013-02-03 2013-05-08 福建达安能源实业有限责任公司 Special biological grease for powder emulsion explosive

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