CN103989247B - Sunset abelmoschus flower alcohol extract and the application in cigarette thereof - Google Patents
Sunset abelmoschus flower alcohol extract and the application in cigarette thereof Download PDFInfo
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- CN103989247B CN103989247B CN201410212892.1A CN201410212892A CN103989247B CN 103989247 B CN103989247 B CN 103989247B CN 201410212892 A CN201410212892 A CN 201410212892A CN 103989247 B CN103989247 B CN 103989247B
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Abstract
The present invention relates to a kind of sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the Huang Shuhua volumetric concentration 60 ~ 90% pulverized extract, extract and terminate rear Separation of Solid and Liquid, after extract reduced pressure concentration and get final product.Do not changing on the original performance of cigarette and processing technology basis, add sunset abelmoschus flower alcohol extract of the present invention in cigarette, significantly can improve the fine and smooth soften of flue gas, reduce assorted gas and the excitant of flue gas, improve the sense organ comfort level of perfume quantity and cigarette, improve the integral suction quality of cigarette.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of sunset abelmoschus flower alcohol extract and as the application of the tobacco aromatics in cigarette additive in cigarette.
Background technology
The quality defects such as flue gas drying, odor characteristic are remarkable, comfort level is poor are current China cigarette product problem demanding prompt solutions, and development of new cigarette additive is undoubtedly one of solution.Vast territory and abundant resources in China, and plant resources enriches, and especially Chinese herbal medicine resource, can be furtherd investigate the extracting method of its active ingredient, be effectively applied to by extract in cigarette, to improving suction quality and the sense organ comfort level of cigarette.
Sunset Abelmoschus Root [Abelmoschusmanihot (Linn.) Medicus] has another name called gumbo, is the annual or herbaceos perennial of Malvaceae Abelmoschus.Originate in south China, existing extensively cultivation in all parts of the country, many for ornamental plantation.Sunset abelmoschus stem or bark hide fiber for fiber crops and can manufacture synthetic cotton; Root contains mucilaginous substance, can make papermaking thickener; Its seed, root, flower can do medicinal (Feng Guomei. Chinese Plants will, the 49th volume second fascicle, [M].The Chinese Academy of Sciences's " Chinese Plants will " editorial board, Science Press: Beijing, 1984; P53.).Its flower multiplex in history tree, Compendium of Material Medica is drawn " Jiayou Bencao " cloud: " its flower smell is sweet, cold, sliding, nontoxic; cure mainly urine leaching and expedite the emergence of; control all evil sore pus and not to be recovered for a long time person, and namely that does that end applies heals, and is persons particularly liable to develop skin infection's key medicine; the subcutaneous ulcer that disappears swells; immersion oil is coated with burn " etc. (occupy civilian political affairs. the herbal textual [J] of Sunset Abelmoschus Root. time precious traditional Chinese medicines study, 1994,5 (2): 6-7.).Sunset abelmoschus flower records in 2010 editions pharmacopeia one, and flavone compound is its main component, is also active component, and three kinds of flavone compounds that wherein content is higher are: Hyperoside, quercetin-3'-glucoside, isoquercitin.Modern pharmacological research shows: sunset abelmoschus flower can treat nephrotic syndrome (NS); Anti-hepatitis B virus (HBV); To the heart, cerebral ischemia re-pouring injuredly there is certain protective effect.Multiple flavones ingredient in sunset abelmoschus flower has anti-oxidant, antibacterial, detumescence and the antipyretic effect of anti-inflammatory, can treat canker sore, also have good mitigation to pain.At present, the existing Chinese medicine preparation " Huang Kui capsule " made with maniod ebish flower extract, is used for the treatment of CGN.
The domestic research about Sunset Abelmoschus Root is mainly in growing nursery and culture, chemical constituents determination, quality standard, medicine etc., and the report about sunset abelmoschus flower alcohol extract is less, and does not find its application in tobacco.
Summary of the invention
The object of the invention is to provide a kind of sunset abelmoschus flower alcohol extract and as the application of tobacco aromatics in cigarette, can improve suction quality and the sense organ comfort level of cigarette.
To achieve these goals, the present invention adopts following technical scheme:
Sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the sunset abelmoschus flower volumetric concentration 60 ~ 90% pulverized extract, extract and terminate rear Separation of Solid and Liquid, after extract reduced pressure concentration (in order to remove ethanol) and get final product.Gained sunset abelmoschus flower alcohol extract is at room temperature yellowish-brown liquid or liquid extract, has cream perfume and delicate fragrance, is soluble in a certain proportion of alcohol solution.
Concrete, during alcohol extract, solid-liquid ratio is preferably 1g:5 ~ 20g.
Following various ways can be adopted during alcohol extract to carry out: 1) lixiviate under room temperature, every batch materials lixiviate 2 times, each 7 ~ 10 days.2) under 60 ~ 85 DEG C of conditions, extraction 1 ~ 2 time is heated, each 1 ~ 3 hour.3) ultrasonic assistant extracts, ultrasonic frequency 30 ~ 60kHz, power 100 ~ 1000W, extraction time 30 ~ 60min, Extracting temperature 30 ~ 50 DEG C.4) microwave radiation exaraction under normal temperature, microwave power 150 ~ 500W, extraction time 5 ~ 30min, extract 1 ~ 2 time.
Can adopt vacuum filtration during Separation of Solid and Liquid, vacuum degree control at 0.05 ~ 0.1MPa, or adopts centrifugation, centrifugal rotational speed 1000 ~ 4000rpm, centrifugation time 20 ~ 40min.
In reduced pressure concentration step, be preferably evaporated to 1/5 ~ 1/20 of original volume.
The application of above-mentioned sunset abelmoschus flower alcohol extract in cigarette.Be specially: after sunset abelmoschus flower alcohol extract ethanol and/or propane diols dilution being dissolved, be sprayed onto on pipe tobacco, after naturally drying or toasting, technique makes cigarette routinely, and wherein, the addition of sunset abelmoschus flower alcohol extract is 0.01 ~ 0.1 ‰ of pipe tobacco weight.Can be used alone or be deployed into essence with other spices and use.
Innovative point of the present invention is: provide a kind of sunset abelmoschus flower alcohol extract taking sunset abelmoschus flower as raw material and extract preparation, and it can be used as cigarette additive to be applied on cigarette.Do not changing on the original performance of cigarette and processing technology basis, the sunset abelmoschus flower alcohol extract of interpolation can improve fine and smooth soften and the flavouring essence quality of flue gas, improves the sense organ comfort level of cigarette.In addition, sunset abelmoschus flower is rich and easy to get, and the flavones ingredient that sunset abelmoschus flower alcohol extract is rich in can also reduce the free-radical contents in cigarette smoke.Extraction production technology of the present invention is simple to operation, and production cost is lower, therefore has more actual production meaning and value.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further, but protection scope of the present invention is not limited thereto.
Embodiment 1
A kind of sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the sunset abelmoschus flower volumetric concentration 90% pulverized (addition of ethanol is 8 times of sunset abelmoschus flower weight) in 75 DEG C of refluxing extraction 3h, extraction terminates rear centrifugation (centrifugal 40min, rotating speed 2000rpm), get supernatant and be evaporated to 1/10 of supernatant original volume and get final product.
Take the above-mentioned sunset abelmoschus flower alcohol extract of 0.020g, be diluted to 1.000g with 90v% ethanol, mixing.To inject 4 μ L(perfuming amounts be 0.1 ‰ to often propping up in blank cigarette to adopt perfuming cigarette injector), be designated as test cigarette.Separately get partial blank cigarette, often prop up injection 4 μ L90v% ethanol cigarette in contrast.Test cigarette and contrast cigarette are put into constant temperature (22 ± 1 DEG C), constant humidity (relative humidity 60 ± 2%) more than case inner equilibrium 48h respectively.Smoke panel test through the above judging panel of 7 people, the results are shown in Table 1.As seen from Table 1: add the test cigarette after sunset abelmoschus flower alcohol extract: aroma quality and perfume quantity all have lifting, assorted gas and excitant reduce, and Hui Tian promotes the production of body fluid sense obviously, significantly improves the suction quality of cigarette.
The aesthetic quality of table 1, contrast cigarette and test cigarette contrasts smoking result
Embodiment 2
A kind of sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the sunset abelmoschus flower volumetric concentration 80% pulverized (addition of ethanol is 15 times of sunset abelmoschus flower weight) adopts ultrasonic and circulated extraction machine ultrasonic extraction 50min in 30 DEG C, ultrasonic frequency 40kHz, power 750W, ultrasonic time and interval time are 2s/1s, mixing speed 1300rpm.Extract and terminate final vacuum suction filtration, filtrate reduced in volume to filtrate original volume 1/20 and get final product.
Take 0.1g above-mentioned sunset abelmoschus flower alcohol extract 80v% ethanol and be diluted to 10g, mixing, for subsequent use.Pipe tobacco is evenly divided into two parts, and portion accounts for 0.05 ‰ of pipe tobacco weight by sunset abelmoschus flower alcohol extract on pipe tobacco, evenly sprays the ethanolic solution (being designated as test cigarette) containing sunset abelmoschus flower alcohol extract; Another part is pressed 0.05 ‰ of pipe tobacco weight and is evenly sprayed 80v% ethanol pipe tobacco in contrast.Then, cigarette is rolled into respectively.Test cigarette and contrast cigarette are put into constant temperature (22 ± 1 DEG C), constant humidity (relative humidity 60 ± 2%) more than case inner equilibrium 48h respectively.Smoke panel test through the above judging panel of 7 people, the results are shown in Table 2.As seen from Table 2: add the test cigarette after sunset abelmoschus flower alcohol extract, flue gas free from extraneous odour, perfume quantity increases, and assorted gas, excitant alleviate, and pleasant impression is clean, has sense of promoting the production of body fluid.
The aesthetic quality of table 2, contrast cigarette and test cigarette contrasts smoking result
Embodiment 3
A kind of sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the sunset abelmoschus flower volumetric concentration 70% pulverized (addition of ethanol is 5 times of sunset abelmoschus flower weight) Microwave Extraction 20min under 160W power, extract 2 times altogether, extract and terminate final vacuum suction filtration.Merge twice gained extract, be evaporated to 1/15 of original volume and get final product.
Take 0.1g above-mentioned sunset abelmoschus flower alcohol extract 70v% ethanol and be diluted to 10g, mixing, for subsequent use.Pipe tobacco is evenly divided into two parts, and portion accounts for 0.02 ‰ of pipe tobacco weight by sunset abelmoschus flower alcohol extract on pipe tobacco, evenly sprays the ethanolic solution (being designated as test cigarette) containing sunset abelmoschus flower alcohol extract; Another part is pressed 0.02 ‰ of pipe tobacco weight and is evenly sprayed 70v% ethanol pipe tobacco in contrast.Then, cigarette is rolled into respectively.Test cigarette and contrast cigarette are put into constant temperature (22 ± 1 DEG C), constant humidity (relative humidity 60 ± 2%) more than case inner equilibrium 48h respectively.Smoke panel test through the above judging panel of 7 people, the results are shown in Table 3.As seen from Table 3: add the test cigarette after sunset abelmoschus flower alcohol extract: flue gas free from extraneous odour, perfume quantity increases, and fragrance is coordinated, and assorted gas and excitant alleviate, and pleasant impression is comfortable, and overall sucking quality is improved.
The aesthetic quality of table 3, contrast cigarette and test cigarette contrasts smoking result
Claims (2)
1. the application of sunset abelmoschus flower alcohol extract in cigarette, is characterized in that, after sunset abelmoschus flower alcohol extract ethanol and/or propane diols dilution being dissolved, be evenly sprayed onto on pipe tobacco, after naturally drying or toasting, technique makes cigarette routinely; Wherein, the addition of sunset abelmoschus flower alcohol extract is 0.01 ~ 0.1 ‰ of pipe tobacco weight;
Described sunset abelmoschus flower alcohol extract, it is obtained by following step: by drying and the ethanol of the sunset abelmoschus flower volumetric concentration 60 ~ 90% pulverized extract, extract and terminate rear Separation of Solid and Liquid, after extract reduced pressure concentration and get final product.
2. the application of sunset abelmoschus flower alcohol extract in cigarette as claimed in claim 1, it is characterized in that, during alcohol extract, solid-liquid ratio is 1g:5 ~ 20g.
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Citations (4)
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|---|---|---|---|---|
| CN1615947A (en) * | 2004-09-16 | 2005-05-18 | 凌沛学 | Medicine for treating oral ulcer, gastric ulcer, burn and scald and traumatic infection and preparing method |
| CN1994337A (en) * | 2006-11-11 | 2007-07-11 | 周亚球 | Total flavone extract of maniod eibish, its preparation and application |
| CN101313942A (en) * | 2007-05-30 | 2008-12-03 | 江苏正大天晴药业股份有限公司 | Chinese medicine composition for treating nephropathy |
| CN102166039A (en) * | 2011-04-08 | 2011-08-31 | 深圳波顿香料有限公司 | Method for extracting roselle extractive and application in cigarettes as well as cigarettes |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JPS5163922A (en) * | 1974-12-02 | 1976-06-02 | Hikaru Nukada | Okurayori koshuyoseijukoseibuno chushutsusuru hoho |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1615947A (en) * | 2004-09-16 | 2005-05-18 | 凌沛学 | Medicine for treating oral ulcer, gastric ulcer, burn and scald and traumatic infection and preparing method |
| CN1994337A (en) * | 2006-11-11 | 2007-07-11 | 周亚球 | Total flavone extract of maniod eibish, its preparation and application |
| CN101313942A (en) * | 2007-05-30 | 2008-12-03 | 江苏正大天晴药业股份有限公司 | Chinese medicine composition for treating nephropathy |
| CN102166039A (en) * | 2011-04-08 | 2011-08-31 | 深圳波顿香料有限公司 | Method for extracting roselle extractive and application in cigarettes as well as cigarettes |
Non-Patent Citations (1)
| Title |
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| 烟用天然植物增香保润技术的研究进展;叶超凡等;《农产品加工.学刊》;20120331(第3期);33-38 * |
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Address after: 450000 Yulin South Road, Henan, Zheng Dong, No. 16 South Road, Zhengzhou Patentee after: China Tobacco Henan Industrial Co., Ltd. Patentee after: Zhengzhou Tobacco Research Institute of CNTC Address before: 450000 Zhengzhou agricultural road, Henan, No. 29 Patentee before: China Tobacco Henan Industrial Co., Ltd. Patentee before: Zhengzhou Tobacco Research Institute of CNTC |