CN103893243A - Method for extracting jatropha curcas branch and leaf extract and foot bath formula - Google Patents
Method for extracting jatropha curcas branch and leaf extract and foot bath formula Download PDFInfo
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- CN103893243A CN103893243A CN201410142536.7A CN201410142536A CN103893243A CN 103893243 A CN103893243 A CN 103893243A CN 201410142536 A CN201410142536 A CN 201410142536A CN 103893243 A CN103893243 A CN 103893243A
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Abstract
The invention discloses a method for extracting jatropha curcas branch and leaf extract and a foot bath formula. The method comprises the following steps: smashing jatropha curcas branches and/or leaves; adding the smashed jatropha curcas branches and/or leaves into an extracting solution, and extracting at the temperature between room temperature and 100 DEG C for 3-20 hours; filtering the extracting solution, concentrating under reduced pressure, and drying at the temperature of 50-70 DEG C to obtain the jatropha curcas branch and leaf extract. The formula comprises a jatropha curcas anti-bacterial extract, and the foot bath formula is dissolved into water to obtain foot bath liquid; the weight ratio of the jatropha curcas anti-bacterial extract to water is 0.2-1.2g to 1,000g-3,000g. By adopting the method, the problem of extraction of anti-bacterial substances from jatropha curcas trees is solved, and the jatropha curcas anti-bacterial substances are utilized; a pure Chinese medicinal foot bath formula is prepared by using the natural fungus and bacteria killing capabilities of the jatropha curcas anti-bacterial extract; by using the foot bath formula, drug resistance of fungi of patients is prevented, fungi can be killed fully, and the aim of completely curing is fulfilled; the method is easy to operate, and convenient to use.
Description
Technical field
The present invention relates to a kind of method of extracting antibacterial from little seeds of a tung oil tree branch and leaf, also relate to the foot bath formula of a kind of use from the antibacterial of little seeds of a tung oil tree extraction.
Background technology
Little seeds of a tung oil tree tree contains abundant antibacterial substance, but, how from little seeds of a tung oil tree tree, to extract antibacterial substance and to be used, still belong to so far in the art technological gap.
In existing foot bath formula, the medicine for the treatment of beriberi adopts Western medicine mostly, and these medicines, except having very strong toxic and side effects, also can make fungus produce drug resistance, and of a specified duration can cause beriberi protracted course of disease, is difficult to real elimination.
Summary of the invention
One of the technical problem to be solved in the present invention is, a kind of little seeds of a tung oil tree branch and leaf extractum extracting method is provided, and overcomes the defect that prior art can not be extracted antibacterial substance and be used from little seeds of a tung oil tree tree.
Two of the technical problem to be solved in the present invention is, a kind of foot bath formula is provided, and overcomes the defect that existing treatment beriberi is difficult to effect a radical cure beriberi.
The present invention solves the technical scheme that one of its technical problem adopts: a kind of little seeds of a tung oil tree branch and leaf extractum extracting method is provided, comprises the steps:
S1, little seeds of a tung oil tree leaves and/or branch are pulverized;
S2, the little seeds of a tung oil tree leaves of pulverizing and/or branch are added in extracting solution and extracted, extraction time is 3～20 hours, and extracting temperature is that room temperature is to 100 ℃ Celsius;
S3, will after extracting liquid filtering, carry out concentrating under reduced pressure, dry at 50 ℃～70 ℃ Celsius, obtain little seeds of a tung oil tree branch and leaf extractum.
2, little seeds of a tung oil tree branch and leaf extractum extracting method as claimed in claim 1, is characterized in that, described extracting solution is water or ethanol water or ethanol.
In little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention, described extracting solution is water or ethanol water or ethanol.
In little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention, described extraction time is 10～15 hours.
In little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention, described extraction temperature is 30 ℃ Celsius; In described step S2, the little seeds of a tung oil tree leaves of pulverizing and/or the solid-liquid ratio of branch and extracting solution are 1:15.
In little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention, described extracting solution is the ethanol water that water or alcoholic strength are less than 50%, and described step S3 comprises: by Powdered by being milled into the little seeds of a tung oil tree branch and leaf extractum obtaining.
In little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention, in step S3, comprise precipitate with ethanol processing: after extracting liquid filtering, add the ethanol of two volumes, at 4 ℃ Celsius, leave standstill 6～12 hours, then remove by filter precipitate; Extracting solution, after precipitate with ethanol is processed, then carries out concentrating under reduced pressure and oven dry, obtains little seeds of a tung oil tree branch and leaf extractum.
The present invention solves the technical scheme that two of its technical problem adopts: a kind of foot bath formula is provided, it is characterized in that, comprise little seeds of a tung oil tree bacteriostatic extractive, the water-soluble foot bath liquid that makes of this foot bath formula medicament; The weight ratio of this little seeds of a tung oil tree bacteriostatic extractive and water is: 0.2 gram～1.2 grams little seeds of a tung oil tree bacteriostatic extractives are than 1000 grams～3000 grams water.
In foot bath formula of the present invention, the weight ratio of described little seeds of a tung oil tree bacteriostatic extractive and water is: 0.5 gram～1.0 grams little seeds of a tung oil tree bacteriostatic extractives are than 1000 grams～3000 grams water.
In foot bath formula of the present invention, comprise Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci, described Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, the weight ratio of Herba Lysimachiae foenum-graeci and water is: each 0.5 gram～0.7 gram Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci is than 1000 grams～3000 grams water,
Or comprise Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae, described Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, the weight ratio of Radix Achyranthis Bidentatae and water is: each 0.5 gram～0.7 gram Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae is than 1000 grams～3000 grams water.
In foot bath formula of the present invention, described little seeds of a tung oil tree bacteriostatic extractive is little seeds of a tung oil tree tree slurry crude extract or little seeds of a tung oil tree branch and leaf extractum described above.
Implement little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention and a kind of foot bath formula, compared with the prior art, its beneficial effect is:
1. solved from little seeds of a tung oil tree tree and extracted the problem of antibacterial substance, to little seeds of a tung oil tree antibacterial substance is used;
2. the natural ability of killing of utilizing little seeds of a tung oil tree bacteriostatic extractive to possess fungus, antibacterial, prepares pure footbath with traditional Chinese medicines formula, uses this foot bath formula, and patient fungus can not produce drug resistance, and thoroughly killing fungus reaches the object of thorough healing.
3. simple to operate, easy to use.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described.
Little seeds of a tung oil tree branch and leaf extractum extracting method of the present invention comprises the steps:
The first, by little seeds of a tung oil tree leaves or branch or leaves and branch pulverizing.The fresh leaves of the little seeds of a tung oil tree can be placed in after shady and cool ventilation place natural drying, is crushed to 0.25cm2, also fresh little seeds of a tung oil tree leaves directly can be pulverized.
The second, the little seeds of a tung oil tree branch and leaf of above-mentioned pulverizing are added in extracting solution and extracted, extraction time is 3～20 hours, extracting temperature is that room temperature is to 100 ℃ Celsius.Extracting solution can adopt and include but not limited to water, ethanol water or ethanol, extraction time is better at 10～15 hours scope extraction effects, it is better that extraction temperature is got room temperature (as 25 ℃～30 ℃) extraction effect, the little seeds of a tung oil tree branch and leaf of pulverizing and the solid-liquid ratio of extracting solution can be determined on demand, common desirable 1:10～1:25, it is better that solid-liquid ratio is got 1:15 extraction effect.
The 3rd, will after extracting liquid filtering, carry out concentrating under reduced pressure, at 50 ℃～70 ℃ Celsius, dry, obtain little seeds of a tung oil tree branch and leaf extractum.When bake out temperature is got 60 ℃, effect is better.
In other embodiments, when extracting solution is water or alcoholic strength while being less than 50% ethanol water, step 3 comprises: by Powdered by being milled into the little seeds of a tung oil tree branch and leaf extractum obtaining.
In other embodiments, step 3 comprises precipitate with ethanol processing, by after extracting liquid filtering, adds the ethanol of two volumes that is:, under 4 ℃ of conditions Celsius, leaves standstill 6～12 hours, then filtration, disgorging.Extracting solution, after precipitate with ethanol is processed, then carries out concentrating under reduced pressure and oven dry, obtains little seeds of a tung oil tree branch and leaf extractum.
Foot bath formula of the present invention comprises little seeds of a tung oil tree bacteriostatic extractive.Foot bath formula can only use little seeds of a tung oil tree bacteriostatic extractive, also can be on the basis of little seeds of a tung oil tree bacteriostatic extractive, add the medicine of other treatment beriberi: Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis etc., the medicine of promoting blood circulation to remove obstruction in the collateral, wind-damp dispelling bone and muscle strengthening: warming, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade etc. all over the body; The medicine of invigorating QI and tranquilization: Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird do not stand, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci etc.Also can, on the basis of little seeds of a tung oil tree bacteriostatic extractive, add the medicines such as Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae.
By water-soluble this foot bath formula medicament foot bath liquid that makes.
Wherein, the weight ratio of little seeds of a tung oil tree bacteriostatic extractive and water is: 0.2 gram～1.2 grams little seeds of a tung oil tree bacteriostatic extractives are than 1000 grams～3000 grams water.
In other embodiments, little seeds of a tung oil tree bacteriostatic extractive adopts 0.5 gram～1.0 grams little seeds of a tung oil tree bacteriostatic extractives than 1000 grams～3000 grams water with the weight ratio of water, and effect is better.
Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird do not stand all over the body, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci with the weight ratio of water be: each 0.5 gram～0.7 gram Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, the whole body are warming, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird are not stood, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci be than 1000 grams～3000 grams water.
The weight ratio of Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae and water is: each 0.5 gram～0.7 gram Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae are than 1000 grams～3000 grams water.
Above-mentioned little seeds of a tung oil tree bacteriostatic extractive is little seeds of a tung oil tree tree slurry crude extract or above-mentioned little seeds of a tung oil tree branch and leaf extractum.
Claims (10)
1. a little seeds of a tung oil tree branch and leaf extractum extracting method, comprises the steps:
S1, little seeds of a tung oil tree leaves and/or branch are pulverized;
S2, the little seeds of a tung oil tree leaves of pulverizing and/or branch are added in extracting solution and extracted, extraction time is 3～20 hours, and extracting temperature is that room temperature is to 100 ℃ Celsius;
S3, will after extracting liquid filtering, carry out concentrating under reduced pressure, dry at 50 ℃～70 ℃ Celsius, obtain little seeds of a tung oil tree branch and leaf extractum.
2. little seeds of a tung oil tree branch and leaf extractum extracting method as claimed in claim 1, is characterized in that, described extracting solution is water or ethanol water or ethanol.
3. little seeds of a tung oil tree branch and leaf extractum extracting method as claimed in claim 2, is characterized in that, described extraction time is 10～15 hours.
4. little seeds of a tung oil tree branch and leaf extractum extracting method as claimed in claim 2, is characterized in that, described extraction temperature is 30 ℃ Celsius; In described step S2, the little seeds of a tung oil tree leaves of pulverizing and/or the solid-liquid ratio of branch and extracting solution are 1:15.
5. little seeds of a tung oil tree branch and leaf extractum extracting method as claimed in claim 2, is characterized in that, described extracting solution is the ethanol water that water or alcoholic strength are less than 50%, and described step S3 comprises: by Powdered by being milled into the little seeds of a tung oil tree branch and leaf extractum obtaining.
6. the little seeds of a tung oil tree branch and leaf extractum extracting method as described in one of claim 1 to 5, is characterized in that, in step S3, comprise precipitate with ethanol processing: after extracting liquid filtering, add the ethanol of two volumes, at 4 ℃ Celsius, leave standstill 6～12 hours, then remove by filter precipitate; Extracting solution, after precipitate with ethanol is processed, then carries out concentrating under reduced pressure and oven dry, obtains little seeds of a tung oil tree branch and leaf extractum.
7. a foot bath formula, is characterized in that, comprises little seeds of a tung oil tree bacteriostatic extractive, the water-soluble foot bath liquid that makes of this foot bath formula medicament; The weight ratio of this little seeds of a tung oil tree bacteriostatic extractive and water is: 0.2 gram～1.2 grams little seeds of a tung oil tree bacteriostatic extractives are than 1000 grams～3000 grams water.
8. foot bath formula as claimed in claim 7, is characterized in that, the weight ratio of described little seeds of a tung oil tree bacteriostatic extractive and water is: 0.5 gram～1.0 grams little seeds of a tung oil tree bacteriostatic extractives are than 1000 grams～3000 grams water.
9. foot bath formula as claimed in claim 7, it is characterized in that, comprise Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci, described Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, the weight ratio of Herba Lysimachiae foenum-graeci and water is: each 0.5 gram～0.7 gram Radix Rumicis Crispi, Cortex Dictamni, Cortex Meliae, Cortex Pseudolaricis, Herba Pogostemonis, warming all over the body, Rhizoma Homalomenae, Millettia Speciosa, copper sunshade, Flos Carthami pouring curtain, Caulis Polygoni Multiflori, bird does not stand, Radix Clematidis, Herba Lobeliae Chinensis, Herba Lysimachiae foenum-graeci is than 1000 grams～3000 grams water,
Or comprise Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae, described Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, the weight ratio of Radix Achyranthis Bidentatae and water is: each 0.5 gram～0.7 gram Stigma Croci, Herba Agrimoniae, Radix Ginseng, CAIFUZI, Fructus Xanthii, Herba Cistanches, Herba Lycopodii, Herba speranskiae tuberculatae, Fructus Liquidambaris, Folium Artemisiae Argyi, Fructus Ligustri Lucidi, Rhizoma Cibotii, Flos Magnoliae, Radix Achyranthis Bidentatae is than 1000 grams～3000 grams water.
10. the foot bath formula as described in one of claim 7 to 9, is characterized in that, described little seeds of a tung oil tree bacteriostatic extractive is little seeds of a tung oil tree tree slurry crude extract or little seeds of a tung oil tree branch and leaf extractum as claimed in claim 1.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410142536.7A CN103893243A (en) | 2014-02-07 | 2014-04-10 | Method for extracting jatropha curcas branch and leaf extract and foot bath formula |
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| CN201410045144.9 | 2014-02-07 | ||
| CN201410045144 | 2014-02-07 | ||
| CN201410142536.7A CN103893243A (en) | 2014-02-07 | 2014-04-10 | Method for extracting jatropha curcas branch and leaf extract and foot bath formula |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106866693A (en) * | 2017-04-12 | 2017-06-20 | 武汉兴旺生物技术发展有限公司 | A kind of application of the preparation method, molluscicide and molluscicide of numb Folium Evodiae trichotomae extract |
| CN110693768A (en) * | 2019-10-30 | 2020-01-17 | 凉山德农生物能源股份有限公司 | Jatropha curcas seed purified oil-based washing and protecting two-in-one shampoo and preparation method thereof |
-
2014
- 2014-04-10 CN CN201410142536.7A patent/CN103893243A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106866693A (en) * | 2017-04-12 | 2017-06-20 | 武汉兴旺生物技术发展有限公司 | A kind of application of the preparation method, molluscicide and molluscicide of numb Folium Evodiae trichotomae extract |
| CN110693768A (en) * | 2019-10-30 | 2020-01-17 | 凉山德农生物能源股份有限公司 | Jatropha curcas seed purified oil-based washing and protecting two-in-one shampoo and preparation method thereof |
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Application publication date: 20140702 |