CN103882717A - Hair product conditioner and preparation process thereof as well as method for finishing wig - Google Patents

Hair product conditioner and preparation process thereof as well as method for finishing wig Download PDF

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Publication number
CN103882717A
CN103882717A CN201410125026.9A CN201410125026A CN103882717A CN 103882717 A CN103882717 A CN 103882717A CN 201410125026 A CN201410125026 A CN 201410125026A CN 103882717 A CN103882717 A CN 103882717A
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CN
China
Prior art keywords
wig
aqueous polyurethane
acrylate modified
modified aqueous
setting agent
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CN201410125026.9A
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Chinese (zh)
Inventor
赵见栓
郭云龙
季书国
刘小东
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XUCHANG HENGYUAN HAIR PRODUCTS Inc
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XUCHANG HENGYUAN HAIR PRODUCTS Inc
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Priority to CN201410125026.9A priority Critical patent/CN103882717A/en
Publication of CN103882717A publication Critical patent/CN103882717A/en
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Abstract

The invention belongs to the technical field of cross of chemical technologies and textile technologies and in particular relates to a hair product conditioner and a preparation process thereof as well as a method for finishing wig. According to the hair product conditioner, acrylate modified waterborne polyurethane and ternary copolymer block silicon oil serve as main ingredients, Casson serves as an anti-corrosive additive, and the hair product conditioner is prepared by mixing the following raw materials in percentage by weight according to a specific formula: 30-60 percent of acrylate modified waterborne polyurethane, 3-5 percent of ternary copolymer block silicon oil, 0.3 percent of Casson and the balance of deionized water. The method for finishing wig through the hair product conditioner mainly comprises the following steps: soaking, washing, oil immersing and setting. The invention has the advantages that the finished wig product has film-forming softness and high water resistance, pungent smell can be greatly reduced, and the wig is non-toxic, nonirritant, stable in style and long in duration.

Description

Hair products setting agent and preparation technology thereof and the method that wig is arranged
Technical field
The invention belongs to chemical technology, the mutual interleaving techniques of textile technology field, relate in particular to a kind of for wig curly hair goods, film forming softness, water-fastness, manufacture craft is simple, nontoxic, non-stimulated hair products setting agent and preparation technology thereof and the method that wig is arranged.
Background technology
Hair products curly hair setting agent adopts polyacrylate for the composition of mainly shaping more at present, be equipped with simple silicone oil, or silicone body, or using polyaminoester emulsion is main sizing composition, be equipped with silicone oil or silicone body, wherein adopting polyacrylate is that mainly the shape hair products curly hair setting agent of composition exists following defect: (1), polyacrylate are high molecular polymer, have unpleasant chemicals taste; (2), polyacrylate belongs to acrylate copolymer, and human body is had to corrosiveness; (3), polyacrylate when sizing, film forming is harder, affects the feel of hair products softness; Be while mainly shaping the hair products curly hair setting agent of composition, to have that film forming poor mechanical property, hardness are low, the defect of poor heat stability and adopt polyaminoester emulsion.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art and a kind of film forming softness is provided, water-fastness, can reduce in a large number penetrating odor simultaneously, nontoxic, non-stimulated, the simple hair products setting agent of manufacture craft and preparation technology thereof and the method that wig is arranged.
The technical solution adopted in the present invention is:
A kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of percentage by weight: Acrylate Modified Aqueous Polyurethane 30%~60%, ternary polymerization block silicone oil 3%~5%, Kathon CG 0.3%, surplus are deionized water.
Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A preparation technology for hair products setting agent described above, its preparation technology is as follows:
Step 1), be respectively according to percentage by weight: the proportionate relationship that Acrylate Modified Aqueous Polyurethane 30%~60%, ternary polymerization block silicone oil 3%~5%, Kathon CG 0.3%, surplus are deionized water, get Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, Kathon CG, deionized water for subsequent use;
Step 2), under the temperature conditions of 18~25 DEG C, by Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, Kathon CG, ionized water adds in container, stir 10 minutes, after the dilution of Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, obtain arranging after required curly hair the hair products setting agent of use.
A kind of method that hair products setting agent described above arranges wig:
Step 1), immersion: get wig curly hair clockwork spring, the wig curly hair clockwork spring of reserving type is put into 40~50 DEG C of water, soak 5~10 minutes, until wig curly hair clockwork spring bubbles open, clockwork spring curtain head no longer hardens, and can rub with the hands open, curtain also no longer hardens, and keeps the curtain moulding can not turmoil when immersion;
Step 2), washing: use clear water to rinse on the wig curly hair clockwork spring that bubbles open, the temperature of cleaning institute's water is 30~50 DEG C, rinses three to four times with clear water, can not destroy the moulding of wig curly hair clockwork spring in the process of washing;
Step 3), immersion oil: by step 2) in clean complete wig curly hair clockwork spring put in the silicone oil mixed liquor preparing, described silicone oil mixed liquor main component comprises: hexadecyltrimethylammonium chloride, amido silicon oil, dimethicone, quaternary ammonium salt and deionized water, when dipping wig curly hair clockwork spring, keeping the temperature of silicone oil mixed liquor is 40~50 DEG C, flood 30 minutes, wig curly hair clockwork spring is taken out, for subsequent use;
Step 4), sizing: the hair products setting agent preparing is placed in container, by adding the proportionate relationship of 2g polyisocyanates to add polyisocyanates in 1000g hair products setting agent in container, and stirs 10 minutes, the two is mixed, obtain mixed liquor A; Get mixed liquor A 6~7g, join in 1000g water, controlling water temperature is 40~50 DEG C, stirs 5 minutes, obtains mixed liquid B; Wig curly hair clockwork spring after treatment in step 3) is carried out to kiss-coating processing by obtained mixed liquid B, kiss-coating wig curly hair after treatment clockwork spring is carried out to moulding, then in being the drying baker of 80~120 DEG C, Temperature Setting dries, drying time is 2 hours, the wig curly hair goods after obtaining heat treatment after having dried and completing.
Beneficial effect of the present invention is: because Acrylate Modified Aqueous Polyurethane used is except having film forming water-tolerant, hardness is high, mechanical strength is high, pliability is good, low temperature resistant, endurance, high gloss, high-adhesion, colour retention is good, outside the features such as photostability is strong, also have anti-flaming, explosion-proof, nontoxic, the advantage such as free from environmental pollution, make hair products setting agent provided by the present invention there is film forming softness, water-fastness, colour retention is good, photostability is strong, in preparation process, can reduce in a large number the generation of penetrating odor, nontoxic, non-stimulated advantage, be used on artificial hair product, make wig curly hair goods keep the good moulding while, can keep excellent feel, make the curly hair also can be soft, smooth, promote the quality of wig product, and can save great amount of cost, the product of the same type that contrast existing market is sold can be saved approximately 38.7% production cost, in addition, in the fixating shape step of method wig being arranged at this hair products setting agent of use provided by the invention, in this hair products setting agent, add by a certain percentage polyisocyanates, due to polyisocyanates can be in water self-emulsifying, there is the good water compatibility that has, can accelerate film forming speed, make institute's film forming softness, mechanical strength is high, also makes to use that the wig curly hair goods of hair products setting agent sizing provided by the invention have advantages of that sizing is fast, good hand touch, wig curly hair goods softness, smooth, it is simple that the preparation technology of this hair products setting agent provided by the invention and the method for utilizing this hair products setting agent to arrange wig have technique, convenient operation, be applicable at present common on the market various curly hair types, do not affect feel and perception that curly hair arranges, and do not need the manufacture craft of current curly hair goods to carry out the advantage of larger change.
Detailed description of the invention
Embodiment 1, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: the deionized water that Acrylate Modified Aqueous Polyurethane 500g, ternary polymerization block silicone oil 40g, Kathon CG 3g, surplus are 457g.The each component total amount using is 1000g.Wherein Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
As a preparation technology for above-mentioned hair products setting agent, its preparation technology is as follows:
Step 1), get 500g Acrylate Modified Aqueous Polyurethane, 40g ternary polymerization block silicone oil, 3g Kathon CG, 457g deionized water is for subsequent use;
Step 2), under the temperature conditions of 18~25 DEG C, Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, Kathon CG, deionized water are added in container, stir 10 minutes dilution after, obtain required hair products setting agent.
A kind of method that as above-mentioned hair products setting agent arranges wig:
Step 1), immersion: get wig curly hair clockwork spring, the wig curly hair clockwork spring of reserving type is put into 40~50 DEG C of water, soak 5~10 minutes, until wig curly hair clockwork spring bubbles open, clockwork spring curtain head no longer hardens, and can rub with the hands open, curtain also no longer hardens, and keeps the curtain moulding can not turmoil when immersion;
Step 2), washing: use clear water to rinse on the wig curly hair clockwork spring that bubbles open, the temperature of cleaning institute's water is 30~50 DEG C, rinses three to four times with clear water, can not destroy the moulding of wig curly hair clockwork spring in the process of washing;
Step 3), immersion oil: by step 2) in clean complete wig curly hair clockwork spring put in the silicone oil mixed liquor preparing, described silicone oil mixed liquor main component comprises: hexadecyltrimethylammonium chloride, amido silicon oil, dimethicone, quaternary ammonium salt and deionized water, when dipping wig curly hair clockwork spring, keeping the temperature of silicone oil mixed liquor is 40~50 DEG C, flood 30 minutes, wig curly hair clockwork spring is taken out, for subsequent use;
Step 4), sizing: the hair products setting agent preparing is placed in container, in 1000g hair products setting agent, adds 2g polyisocyanates, stir 10 minutes, the two is mixed, obtain mixed liquor A; Get mixed liquor A 6~7g, join in 1000g water, controlling water temperature is 40~50 DEG C, stirs 5 minutes, obtains mixed liquid B; Wig curly hair clockwork spring after treatment in step 3) is carried out to kiss-coating processing by obtained mixed liquid B, kiss-coating wig curly hair after treatment clockwork spring is carried out to moulding, then in being the drying baker of 80~120 DEG C, Temperature Setting dries, drying time is 2 hours, the wig curly hair goods after obtaining heat treatment after having dried and completing.
Embodiment 2, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: the deionized water that Acrylate Modified Aqueous Polyurethane 600g, ternary polymerization block silicone oil 35g, Kathon CG 3g, surplus are 362g.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 3, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: the deionized water that Acrylate Modified Aqueous Polyurethane 400g, ternary polymerization block silicone oil 50g, Kathon CG 3g, surplus are 557g.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 4, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: the deionized water that Acrylate Modified Aqueous Polyurethane 550g, ternary polymerization block silicone oil 30g, Kathon CG 3g, surplus are 417g.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 5, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 600g, ternary polymerization block silicone oil 30g, Kathon CG 3g, surplus are 367g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 6, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 300g, ternary polymerization block silicone oil 30g, Kathon CG 3g, surplus are 667g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 7, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 400g, ternary polymerization block silicone oil 30g, Kathon CG 3g, surplus are 567g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 8, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 500g, ternary polymerization block silicone oil 30g, Kathon CG 3g, surplus are 467g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 9, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 300g, ternary polymerization block silicone oil 35g, Kathon CG 3g, surplus are 662g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 10, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 400g, ternary polymerization block silicone oil 35g, Kathon CG 3g, surplus are 562g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 11, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 500g, ternary polymerization block silicone oil 35g, Kathon CG 3g, surplus are 462g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 12, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 300g, ternary polymerization block silicone oil 40g, Kathon CG 3g, surplus are 657g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 13, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 400g, ternary polymerization block silicone oil 40g, Kathon CG 3g, surplus are 557g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 14, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 600g, ternary polymerization block silicone oil 40g, Kathon CG 3g, surplus are 357g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 15, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 300g, ternary polymerization block silicone oil 45g, Kathon CG 3g, surplus are 652g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 16, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 400g, ternary polymerization block silicone oil 45g, Kathon CG 3g, surplus are 552g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 17, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 500g, ternary polymerization block silicone oil 45g, Kathon CG 3g, surplus are 452g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 18, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 600g, ternary polymerization block silicone oil 45g, Kathon CG 3g, surplus are 352g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 19, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 300g, ternary polymerization block silicone oil 50g, Kathon CG 3g, surplus are 647g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 20, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 500g, ternary polymerization block silicone oil 50g, Kathon CG 3g, surplus are 447g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 21, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 600g, ternary polymerization block silicone oil 50g, Kathon CG 3g, surplus are 347g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.
Embodiment 22, a kind of hair products setting agent, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of weight grams: Acrylate Modified Aqueous Polyurethane 450g, ternary polymerization block silicone oil 40g, Kathon CG 3g, surplus are 507g deionized water.The each component total amount using is 1000g.Described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
A kind of preparation technology of above-mentioned hair products setting agent and a kind of method of utilizing above-mentioned hair products setting agent to arrange wig are identical with embodiment 1, no longer repeat.

Claims (4)

1. a hair products setting agent, it is characterized in that, taking Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil as major ingredient composition, taking Kathon CG as anticorrosive additive, above-mentioned each raw material is as follows according to the concrete formula of percentage by weight: Acrylate Modified Aqueous Polyurethane 30%~60%, ternary polymerization block silicone oil 3%~5%, Kathon CG 0.3%, surplus are deionized water.
2. hair products setting agent according to claim 1, is characterized in that: described Acrylate Modified Aqueous Polyurethane is to use the KH550 end-sealed type Acrylate Modified Aqueous Polyurethane of KH550 silane coupler as end-capping reagent.
3. a preparation technology for hair products setting agent as claimed in claim 1 or 2, is characterized in that, its preparation technology is as follows:
Step 1), be respectively according to percentage by weight: the proportionate relationship that Acrylate Modified Aqueous Polyurethane 30%~60%, ternary polymerization block silicone oil 3%~5%, Kathon CG 0.3%, surplus are deionized water, get Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, Kathon CG, deionized water for subsequent use;
Step 2), under the temperature conditions of 18~25 DEG C, by Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, Kathon CG, ionized water adds in container, stir 10 minutes, after the dilution of Acrylate Modified Aqueous Polyurethane, ternary polymerization block silicone oil, obtain arranging after required curly hair the hair products setting agent of use.
4. the method that hair products setting agent as claimed in claim 3 arranges wig, is characterized in that:
Step 1), immersion: get wig curly hair clockwork spring, the wig curly hair clockwork spring of reserving type is put into 40~50 DEG C of water, soak 5~10 minutes, until wig curly hair clockwork spring bubbles open, clockwork spring curtain head no longer hardens, and can rub with the hands open, curtain also no longer hardens, and keeps the curtain moulding can not turmoil when immersion;
Step 2), washing: use clear water to rinse on the wig curly hair clockwork spring that bubbles open, the temperature of cleaning institute's water is 30~50 DEG C, rinses three to four times with clear water, can not destroy the moulding of wig curly hair clockwork spring in the process of washing;
Step 3), immersion oil: by step 2) in clean complete wig curly hair clockwork spring put in the silicone oil mixed liquor preparing, described silicone oil mixed liquor main component comprises: hexadecyltrimethylammonium chloride, amido silicon oil, dimethicone, quaternary ammonium salt and deionized water, when dipping wig curly hair clockwork spring, keeping the temperature of silicone oil mixed liquor is 40~50 DEG C, flood 30 minutes, wig curly hair clockwork spring is taken out, for subsequent use;
Step 4), sizing: the hair products setting agent preparing is placed in container, by adding the proportionate relationship of 2g polyisocyanates to add polyisocyanates in 1000g hair products setting agent in container, and stirs 10 minutes, the two is mixed, obtain mixed liquor A; Get mixed liquor A 6~7g, join in 1000g water, controlling water temperature is 40~50 DEG C, stirs 5 minutes, obtains mixed liquid B; Wig curly hair clockwork spring after treatment in step 3) is carried out to kiss-coating processing by obtained mixed liquid B, kiss-coating wig curly hair after treatment clockwork spring is carried out to moulding, then in being the drying baker of 80~120 DEG C, Temperature Setting dries, drying time is 2 hours, the wig curly hair goods after obtaining heat treatment after having dried and completing.
CN201410125026.9A 2014-03-31 2014-03-31 Hair product conditioner and preparation process thereof as well as method for finishing wig Pending CN103882717A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106758260A (en) * 2017-02-19 2017-05-31 邵阳阳光发品有限公司 A kind of hair products processing after-treating auxiliary
CN107164959A (en) * 2016-03-07 2017-09-15 邵阳阳光发品有限公司 A kind of human hair chemical fiber hairs processing slipping agent and its application
CN108236155A (en) * 2018-01-19 2018-07-03 安徽富泰发饰文化股份有限公司 A kind of heat-setting method of wig curly hair

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Publication number Priority date Publication date Assignee Title
CN1236783A (en) * 1998-05-14 1999-12-01 Basf公司 Crosslinked, water-soluble or water-dispersible polyurethanes
CN1305366A (en) * 1998-05-14 2001-07-25 Basf公司 Cosmetic product
CN101966019A (en) * 2010-10-14 2011-02-09 许昌恒源发制品股份有限公司 Process for preparing easy-finishing curly hair four-piece wig product
CN101424041B (en) * 2007-10-30 2011-07-13 河南瑞贝卡发制品股份有限公司 Method for preparing isolated hair finishing auxiliaries after frizzy hair and use
CN103214676A (en) * 2013-04-11 2013-07-24 浙江捷发科技有限公司 Synthesis method for terpolymer block silicone oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1236783A (en) * 1998-05-14 1999-12-01 Basf公司 Crosslinked, water-soluble or water-dispersible polyurethanes
CN1305366A (en) * 1998-05-14 2001-07-25 Basf公司 Cosmetic product
CN101424041B (en) * 2007-10-30 2011-07-13 河南瑞贝卡发制品股份有限公司 Method for preparing isolated hair finishing auxiliaries after frizzy hair and use
CN101966019A (en) * 2010-10-14 2011-02-09 许昌恒源发制品股份有限公司 Process for preparing easy-finishing curly hair four-piece wig product
CN103214676A (en) * 2013-04-11 2013-07-24 浙江捷发科技有限公司 Synthesis method for terpolymer block silicone oil

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107164959A (en) * 2016-03-07 2017-09-15 邵阳阳光发品有限公司 A kind of human hair chemical fiber hairs processing slipping agent and its application
CN106758260A (en) * 2017-02-19 2017-05-31 邵阳阳光发品有限公司 A kind of hair products processing after-treating auxiliary
CN108236155A (en) * 2018-01-19 2018-07-03 安徽富泰发饰文化股份有限公司 A kind of heat-setting method of wig curly hair

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Application publication date: 20140625