CN103830965B - Toughness reinforcing composite ceramic filter core of a kind of monkey grass and preparation method thereof - Google Patents
Toughness reinforcing composite ceramic filter core of a kind of monkey grass and preparation method thereof Download PDFInfo
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- CN103830965B CN103830965B CN201410074020.3A CN201410074020A CN103830965B CN 103830965 B CN103830965 B CN 103830965B CN 201410074020 A CN201410074020 A CN 201410074020A CN 103830965 B CN103830965 B CN 103830965B
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Abstract
The invention discloses the toughness reinforcing composite ceramic filter core of a kind of monkey grass, it is characterized in that, be made up of the raw material of following weight portion: cordierite 13-15, medical stone 10-13, aluminium titanates 4-6, vermiculite power 6-9, calcium sulfate 4-6, zirconia 5-7, silica 8-10, pulverize levant cotton exocarp 3-5, monkey grass 4-6, ammonium chloride 2-3, starch 3-6, atoleine 6-8, modification cocoanut active charcoal 5-7, water are appropriate; The present invention adds pulverizing levant cotton exocarp, monkey grass, adds the toughness of filter core, has the performance of porous simultaneously, improve filtration absorption property; Add modification cocoanut active charcoal, space be flourishing, absorption property is good, intensity is high, easy regeneration, economy and durability; Raw material is simple and easy to get, and cost is low, and purification efficiency is high, corrosion-resistant, can be used as air adsorption and filters.
Description
Technical field
The present invention relates to a kind of filtering material and preparation method thereof, particularly toughness reinforcing composite ceramic filter core of a kind of monkey grass and preparation method thereof.
Background technology
Filtering material purposes is very extensive, is mainly used in each fields such as coating, ink, dyestuff, plastics, pharmacy, plating, beverage, cosmetics, rubber, printing, electron tube production, wiring board production, waste incineration, Chemical Manufacture.Modal have filtering material for air handling system, present ambient air pollutes very serious, haze weather has brought great harm, air adsorption filtering material can by the various deleterious particle things of air, as PM2.5 absorption, prevent the life or the working environment that enter people, reduce human lung to the suction of the harmful substances such as particle, improve the quality of life of people, reduce the generation of disease.Existing filtering material mainly contains ceramic honey comb, filter paper, active carbon, steel wire etc.Existing honeycomb ceramic filter material feedstock, formula, function are all more single, can not meet the requirement of technology development.
Summary of the invention
The object of this invention is to provide toughness reinforcing composite ceramic filter core of a kind of monkey grass and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
The toughness reinforcing composite ceramic filter core of a kind of monkey grass, is made up of the raw material of following weight portion: cordierite 13-15, medical stone 10-13, aluminium titanates 4-6, vermiculite power 6-9, calcium sulfate 4-6, zirconia 5-7, silica 8-10, pulverizing levant cotton exocarp 3-5, monkey grass 4-6, ammonium chloride 2-3, starch 3-6, atoleine 6-8, modification cocoanut active charcoal 5-7, water are appropriate;
Described modification cocoanut active charcoal is made up of the raw material of following weight portion: pulverize coconut husk 20-25, zirconia 5-8, superfine silica gel powder 3-5; Preparation method is by the hot wash of pulverizing coconut husk, then soaks 1-2 hour with 50-60% phosphoric acid solution at normal temperatures; Filter, getting filter residue in the retort of 550-600 DEG C carbonizes 1.5-2 hour, takes out; Mix with zirconia, superfine silica gel powder when temperature is down to room temperature, then add 60% NaOH stirring 1-1.5 hour, then filter taking-up; With distilled water cleaning 3-4 time, dry and get final product.
The toughness reinforcing composite ceramic filter core of a kind of monkey grass of the present invention, be made up of following concrete steps:
(1) monkey grass is put into pulverizer to pulverize, all the other residual components except atoleine, water are put into ball mill, ball milling 3-4 hour, mix with the monkey grass pulverized and obtain mixed-powder;
(2) mixed-powder is added appropriate water to stir, obtain mixed slurry, by the slurry vacuum de-soak 2-3 hour of mixing;
(3) slurry of de-soak is injected mould, at room temperature transpiring moisture, the demoulding after automatic drying, obtain the raw embryo of filter core;
(4) sinter in life embryo feeding car tunnel furnace under normal pressure, first roasting 10-12 hour at 200-260 DEG C, then roasting 4-5 hour at being slowly warming up to 500-550 DEG C, then, again with 6-8 DEG C/min of ramp to 1070-1140 DEG C, sintering 3-4 hour, cooling after take out, put into after clear water soaks 1-2 days, take out and dry.
The invention has the beneficial effects as follows: the present invention adds pulverizing levant cotton exocarp, monkey grass, adds the toughness of filter core, has the performance of porous simultaneously, improve filtration absorption property; Add modification cocoanut active charcoal, space be flourishing, absorption property is good, intensity is high, easy regeneration, economy and durability; Raw material is simple and easy to get, and cost is low, and purification efficiency is high, corrosion-resistant, can be used as air adsorption and filters.
Specific embodiments
Below by instantiation, the present invention is described in detail.
The toughness reinforcing composite ceramic filter core of a kind of monkey grass, is made up of the raw material of following weight portion (kilogram): cordierite 13, medical stone 10, aluminium titanates 4, vermiculite power 6, calcium sulfate 4, zirconia 5, silica 8, pulverizing levant cotton exocarp 3, monkey grass 4, ammonium chloride 2, starch 3, atoleine 6, modification cocoanut active charcoal 5, water are appropriate;
Described modification cocoanut active charcoal is made up of the raw material of following weight portion (kilogram): pulverize coconut husk 20, zirconia 5, superfine silica gel powder 3; Preparation method is by the hot wash of pulverizing coconut husk, then soaks 1-2 hour with 50-60% phosphoric acid solution at normal temperatures; Filter, getting filter residue in the retort of 550-600 DEG C carbonizes 1.5-2 hour, takes out; Mix with zirconia, superfine silica gel powder when temperature is down to room temperature, then add 60% NaOH stirring 1-1.5 hour, then filter taking-up; With distilled water cleaning 3-4 time, dry and get final product.
The toughness reinforcing composite ceramic filter core of a kind of monkey grass of the present invention, be made up of following concrete steps:
(1) monkey grass is put into pulverizer to pulverize, all the other residual components except atoleine, water are put into ball mill, ball milling 3-4 hour, mix with the monkey grass pulverized and obtain mixed-powder;
(2) mixed-powder is added appropriate water to stir, obtain mixed slurry, by the slurry vacuum de-soak 2-3 hour of mixing;
(3) slurry of de-soak is injected mould, at room temperature transpiring moisture, the demoulding after automatic drying, obtain the raw embryo of filter core;
(4) sinter in life embryo feeding car tunnel furnace under normal pressure, first roasting 10-12 hour at 200-260 DEG C, then roasting 4-5 hour at being slowly warming up to 500-550 DEG C, then, again with 6-8 DEG C/min of ramp to 1070-1140 DEG C, sintering 3-4 hour, cooling after take out, put into after clear water soaks 1-2 days, take out and dry.
Inventive samples important technological parameters is: the technical indicator of exhaust gas purification and treatment device is: the dust granules minimum grain size scope 0.5-10 μm caught; Process maximum gas temperature 550 DEG C; Trapping micronic dust efficiency>=99%; Outlet drain soot dust granule substrate concentration≤30mg/m
3.
Claims (2)
1. the toughness reinforcing composite ceramic filter core of monkey grass, it is characterized in that, be made up of the raw material of following weight portion: cordierite 13-15, medical stone 10-13, aluminium titanates 4-6, vermiculite power 6-9, calcium sulfate 4-6, zirconia 5-7, silica 8-10, pulverize levant cotton exocarp 3-5, monkey grass 4-6, ammonium chloride 2-3, starch 3-6, atoleine 6-8, modification cocoanut active charcoal 5-7, water are appropriate; Described modification cocoanut active charcoal is made up of the raw material of following weight portion: pulverize coconut husk 20-25, zirconia 5-8, superfine silica gel powder 3-5; Preparation method is by the hot wash of pulverizing coconut husk, then soaks 1-2 hour with 50-60% phosphoric acid solution at normal temperatures; Filter, getting filter residue in the retort of 550-600 DEG C carbonizes 1.5-2 hour, takes out; Mix with zirconia, superfine silica gel powder when temperature is down to room temperature, then add 60% NaOH stirring 1-1.5 hour, then filter taking-up; With distilled water cleaning 3-4 time, dry and get final product.
2. the toughness reinforcing composite ceramic filter core of a kind of monkey grass according to claim 1, is characterized in that, be made up of following concrete steps:
(1) monkey grass is put into pulverizer to pulverize, all the other residual components except monkey grass, water are put into ball mill, ball milling 3-4 hour, mix with the monkey grass pulverized and obtain mixed-powder;
(2) mixed-powder is added appropriate water to stir, obtain mixed slurry, by the slurry vacuum de-soak 2-3 hour of mixing;
(3) slurry of de-soak is injected mould, at room temperature transpiring moisture, the demoulding after automatic drying, obtain the raw embryo of filter core;
(4) sinter in life embryo feeding car tunnel furnace under normal pressure, first roasting 10-12 hour at 200-260 DEG C, then roasting 4-5 hour at being slowly warming up to 500-550 DEG C, then, again with 6-8 DEG C/min of ramp to 1070-1140 DEG C, sintering 3-4 hour, cooling after take out, put into after clear water soaks 1-2 days, take out and dry.
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Families Citing this family (4)
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CN105986525A (en) * | 2016-01-29 | 2016-10-05 | 蚌埠首创滤清器有限公司 | Hydraulic filter filtering paper with ceramic materials for improving pollutant capacity |
CN105920922A (en) * | 2016-06-30 | 2016-09-07 | 郑伟阳 | Ceramic filter element with filter and purifying effects and preparation method thereof |
CN109111936B (en) * | 2018-08-01 | 2021-08-10 | 湖南工业大学 | Biochar processed by in-situ evaporation and preparation method thereof |
CN115074090A (en) * | 2022-07-25 | 2022-09-20 | 深圳市中黄实业有限公司 | High-temperature composite phase-change heat storage material and preparation method thereof |
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CN1349839A (en) * | 2000-10-24 | 2002-05-22 | 邱文亮 | Composite for producing macroporous ceramic filter element |
CN1548402A (en) * | 2003-05-14 | 2004-11-24 | 广东省枫溪陶瓷工业研究所 | Making process of porous ceraimc filter element |
CN103381326A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Carbon crystal composite microporous ceramic filter core and preparation method thereof |
CN103382096A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Anti-microbial ceramic filter core and preparation method thereof |
CN103505944A (en) * | 2013-09-06 | 2014-01-15 | 安徽国电能源设备工程有限公司 | Composite ceramic filter core containing diatomite and active carbon and preparation method thereof |
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JPS58159825A (en) * | 1982-03-19 | 1983-09-22 | Inoue Japax Res Inc | Production of filter element |
JPH0819717A (en) * | 1994-07-08 | 1996-01-23 | Toyobo Co Ltd | Sheet type filter medium for water purification |
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1349839A (en) * | 2000-10-24 | 2002-05-22 | 邱文亮 | Composite for producing macroporous ceramic filter element |
CN1548402A (en) * | 2003-05-14 | 2004-11-24 | 广东省枫溪陶瓷工业研究所 | Making process of porous ceraimc filter element |
CN103381326A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Carbon crystal composite microporous ceramic filter core and preparation method thereof |
CN103382096A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Anti-microbial ceramic filter core and preparation method thereof |
CN103505944A (en) * | 2013-09-06 | 2014-01-15 | 安徽国电能源设备工程有限公司 | Composite ceramic filter core containing diatomite and active carbon and preparation method thereof |
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