CN103820246A - Glass cleaning agent and preparation method - Google Patents
Glass cleaning agent and preparation method Download PDFInfo
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- CN103820246A CN103820246A CN201310643965.8A CN201310643965A CN103820246A CN 103820246 A CN103820246 A CN 103820246A CN 201310643965 A CN201310643965 A CN 201310643965A CN 103820246 A CN103820246 A CN 103820246A
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Abstract
The invention discloses a glass cleaning agent and a preparation method thereof. The glass cleaning agent comprises the following ingredients in parts by weight: 8-12 parts of oxalic acid, 0.2-0.6 parts of sodium alkylarysulfonate, 2-5 parts of glycerol, 0.5-1 part of anhydrous calcium oxide, 0.5-1 part of magnesium sulfate, 0.1-0.5 parts of sodium-ethylenediamine-tetra-acetic acid, 1-4 parts of sodium pyrophosphate, 0.5-2 parts of tween 80, and 40-50 parts of deionized water. The preparation method comprises the steps of adding sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, sodium-ethylenediamine-tetra-acetic acid, sodium pyrophosphate and tween 80 into the deionized water, heating to 60-70 DEG C, stirring to produce colloidal micel suspension, continuing to stir for 10-20min, adding oxalic acid and glycerol into the obtained suspension, heating to 80-90 DEG C and stirring for 15-30min. The glass cleaning agent can well clean dirt on the surface of glass and has no influence on the glass.
Description
Technical field
The invention belongs to chemical industry clean-out system field, be specifically related to a kind of glass cleaner and preparation method thereof.
Background technology
In its molecule of glass cleaner, there is hydrophilic polar group and the non-polar group of oleophylic simultaneously, in the time that its add-on is little, can greatly reduce surface tension and the light-liquid interfacial tension of solvent, and there is the effects such as lubricated, solubilising, emulsification, dispersion and washing.Glass cleaner, in family life and industrial cleaning, has been widely used.Traditional glass cleaner contains alcohol, ethers composition; not only jeopardize user; but also pollute the environment; some composition life-time service in existing glass cleaner can carry out slow reaction with glass surface; make glass surface coarse; transparency reduces, and therefore needs to develop a kind of dirt that can clean efficiently glass surface, can produce to glass the glass cleaner of provide protection simultaneously.
Summary of the invention
The object of the invention is to provides a kind of glass cleaner and preparation method thereof in order to overcome above the deficiencies in the prior art.
This law is bright to be realized by following technique means:
A kind of glass cleaner, comprises in components by weight percent: oxalic acid 8-12 part, sodium alkylarysulfonate 0.2-0.6 part, glycerine 2-5 part, anhydrous calcium oxide 0.5-1 part, magnesium sulfate 0.5-1 part, ethylene dinitrilotetra-acetic acid sodium 0.1-0.5 part, trisodium phosphate 1-4 part, tween 80 0.5-2 part, deionized water 40-50 part.
Described glass cleaner, can be preferably in components by weight percent and comprise: oxalic acid 10-12 part, sodium alkylarysulfonate 0.3-0.5 part, glycerine 3-4 part, anhydrous calcium oxide 0.6-0.8 part, magnesium sulfate 0.8-1 part, ethylene dinitrilotetra-acetic acid sodium 0.2-0.4 part, trisodium phosphate 1-3 part, tween 80 1.5-1.8 part, deionized water 46-48 part.
The preparation method of the glass cleaner described in more than one, can be prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 60-70 ℃, be stirred to and produce micell suspension, continue to stir 10-20 minute;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 80-90 ℃, stir 15-30 minute.
Glass cleaner provided by the invention can be removed the greasy dirt of glass surface after tested well, the assorted point of nothing after washing, corrosion-free to glass, water droplet angle has reached 30 degree, after continuous 100 washings, glass surface is still without assorted point, corrosion-free, and surface shows that this glass cleaner does not have corrosive nature to glass surface.
Embodiment:
Embodiment 1
A kind of glass cleaner, comprises in components by weight percent: 8 parts of oxalic acid, 0.2 part of sodium alkylarysulfonate, 2 parts of glycerine, 0.5 part of anhydrous calcium oxide, 0.5 part, magnesium sulfate, 0.1 part, ethylene dinitrilotetra-acetic acid sodium, 1 part of trisodium phosphate, 0.5 part of tween 80,40 parts of deionized waters.
Described glass cleaner is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 60 ℃, be stirred to and produce micell suspension, continue to stir 10 minutes;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 80 ℃, stir 15 minutes.
Embodiment 2
A kind of glass cleaner, comprises in components by weight percent: 10 parts of oxalic acid, 0.3 part of sodium alkylarysulfonate, 3 parts of glycerine, 0.6 part of anhydrous calcium oxide, 0.8 part, magnesium sulfate, 0.2 part, ethylene dinitrilotetra-acetic acid sodium, 1 part of trisodium phosphate, 1.5 parts of tween 80s, 46 parts of deionized waters.
Described glass cleaner is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 65 ℃, be stirred to and produce micell suspension, continue to stir 12 minutes;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 82 ℃, stir 18 minutes.
Embodiment 3
A kind of glass cleaner, comprises in components by weight percent: 11 parts of oxalic acid, 0.4 part of sodium alkylarysulfonate, 3.5 parts of glycerine, 0.7 part of anhydrous calcium oxide, 0.9 part, magnesium sulfate, 0.3 part, ethylene dinitrilotetra-acetic acid sodium, 2 parts of trisodium phosphates, 1.6 parts of tween 80s, 47 parts of deionized waters.
Described glass cleaner is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 65 ℃, be stirred to and produce micell suspension, continue to stir 18 minutes;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 85 ℃, stir 20 minutes.
Embodiment 4
A kind of glass cleaner, comprises in components by weight percent: 12 parts of oxalic acid, 0.5 part of sodium alkylarysulfonate, 4 parts of glycerine, 0.8 part of anhydrous calcium oxide, 1 part, magnesium sulfate, 0.4 part, ethylene dinitrilotetra-acetic acid sodium, 3 parts of trisodium phosphates, 1.8 parts of tween 80s, 48 parts of deionized waters.
Described glass cleaner is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 68 ℃, be stirred to and produce micell suspension, continue to stir 18 minutes;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 90 ℃, stir 25 minutes.
Embodiment 5
A kind of glass cleaner, comprises in components by weight percent: 12 parts of oxalic acid, 0.6 part of sodium alkylarysulfonate, 5 parts of glycerine, 1 part of anhydrous calcium oxide, 1 part, magnesium sulfate, 0.5 part, ethylene dinitrilotetra-acetic acid sodium, 4 parts of trisodium phosphates, 2 parts of tween 80s, 50 parts of deionized waters.
Described glass cleaner is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 70 ℃, be stirred to and produce micell suspension, continue to stir 20 minutes;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 90 ℃, stir 30 minutes.
The glass cleaner preparing is above carried out to glass cleaning test, the results are shown in following table:
Can find out from above testing data, glass cleaner provided by the invention can carry out the washing of oil stain on glass surface well, and long-term use does not continuously have infection to glass.
Claims (3)
1. a glass cleaner, it is characterized in that, comprise in components by weight percent: oxalic acid 8-12 part, sodium alkylarysulfonate 0.2-0.6 part, glycerine 2-5 part, anhydrous calcium oxide 0.5-1 part, magnesium sulfate 0.5-1 part, ethylene dinitrilotetra-acetic acid sodium 0.1-0.5 part, trisodium phosphate 1-4 part, tween 80 0.5-2 part, deionized water 40-50 part.
2. glass cleaner according to claim 1, it is characterized in that, comprise in components by weight percent: oxalic acid 10-12 part, sodium alkylarysulfonate 0.3-0.5 part, glycerine 3-4 part, anhydrous calcium oxide 0.6-0.8 part, magnesium sulfate 0.8-1 part, ethylene dinitrilotetra-acetic acid sodium 0.2-0.4 part, trisodium phosphate 1-3 part, tween 80 1.5-1.8 part, deionized water 46-48 part.
3. a preparation method for the glass cleaner described in claim 1 or 2, is characterized in that, is prepared according to following steps:
(1) take each component according to weight part;
(2) sodium alkylarysulfonate, anhydrous calcium oxide, magnesium sulfate, ethylene dinitrilotetra-acetic acid sodium, trisodium phosphate and tween 80 are joined in deionized water, be heated to 60-70 ℃, be stirred to and produce micell suspension, continue to stir 10-20 minute;
(3) oxalic acid and glycerine are joined in the suspension that step (2) obtains, continue to be warming up to 80-90 ℃, stir 15-30 minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643965.8A CN103820246B (en) | 2013-12-03 | 2013-12-03 | A kind of glass cleaner and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643965.8A CN103820246B (en) | 2013-12-03 | 2013-12-03 | A kind of glass cleaner and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103820246A true CN103820246A (en) | 2014-05-28 |
| CN103820246B CN103820246B (en) | 2016-10-05 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310643965.8A Active CN103820246B (en) | 2013-12-03 | 2013-12-03 | A kind of glass cleaner and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110846147A (en) * | 2019-11-28 | 2020-02-28 | 维达力实业(深圳)有限公司 | Cleaning agent for removing polishing powder on glass surface and preparation method and application thereof |
Citations (5)
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| WO2003016452A1 (en) * | 2001-08-20 | 2003-02-27 | Tani Co., Ltd. | Detergent for vehicle, method for cleaning vehicle and device for cleaning vehicle |
| CN101144050A (en) * | 2006-09-12 | 2008-03-19 | 长葛市天润有色金属研究所 | Method for manufacturing bath tub ceramic tile cleaning agent |
| CN101838595A (en) * | 2010-05-22 | 2010-09-22 | 湖南嘉业达电子有限公司 | Water-soluble recyclable cleaning liquid and preparation method thereof |
| CN101993786A (en) * | 2009-08-14 | 2011-03-30 | 上海和黄白猫有限公司 | Cleanser essence capable of removing odors of kitchen utensils |
| CN102124091A (en) * | 2008-08-14 | 2011-07-13 | 荷兰联合利华有限公司 | Builder composition |
-
2013
- 2013-12-03 CN CN201310643965.8A patent/CN103820246B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003016452A1 (en) * | 2001-08-20 | 2003-02-27 | Tani Co., Ltd. | Detergent for vehicle, method for cleaning vehicle and device for cleaning vehicle |
| CN101144050A (en) * | 2006-09-12 | 2008-03-19 | 长葛市天润有色金属研究所 | Method for manufacturing bath tub ceramic tile cleaning agent |
| CN102124091A (en) * | 2008-08-14 | 2011-07-13 | 荷兰联合利华有限公司 | Builder composition |
| CN101993786A (en) * | 2009-08-14 | 2011-03-30 | 上海和黄白猫有限公司 | Cleanser essence capable of removing odors of kitchen utensils |
| CN101838595A (en) * | 2010-05-22 | 2010-09-22 | 湖南嘉业达电子有限公司 | Water-soluble recyclable cleaning liquid and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 唐育民: "《合成洗涤剂及其应用》", 31 May 2006, 中国纺织出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110846147A (en) * | 2019-11-28 | 2020-02-28 | 维达力实业(深圳)有限公司 | Cleaning agent for removing polishing powder on glass surface and preparation method and application thereof |
| CN110846147B (en) * | 2019-11-28 | 2021-04-13 | 维达力实业(深圳)有限公司 | Cleaning agent for removing polishing powder on glass surface and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103820246B (en) | 2016-10-05 |
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Effective date of registration: 20210428 Address after: 226300 WuJie central bridge, Tongzhou District, Nantong City, Jiangsu Province Patentee after: Nantong Tongzhou District WuJie agricultural electromechanical management station Address before: 226300, Jiangsu Nantong hi tech Zone, Century Road, No. 788 East Science Park, building of excellence Patentee before: NEOVOLTAIC ENERGY NANTONG Co.,Ltd. |