CN103816482A - Traditional Chinese medicine mixture for treating thyroid enlargement as well as preparation method and application thereof - Google Patents
Traditional Chinese medicine mixture for treating thyroid enlargement as well as preparation method and application thereof Download PDFInfo
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- CN103816482A CN103816482A CN201410079317.9A CN201410079317A CN103816482A CN 103816482 A CN103816482 A CN 103816482A CN 201410079317 A CN201410079317 A CN 201410079317A CN 103816482 A CN103816482 A CN 103816482A
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Abstract
The invention provides a traditional Chinese medicine mixture for treating thyroid enlargement as well as a preparation method and application thereof. The preparation method comprises the following steps: adding rhizoma dioscoreae bulbiferae, seaweed, kelp and clinacanthus nutans into sodium carbonate, extracting for several times with water at the temperature of 80-100 DEG C, and combining the filtrate; mixing rehmannia glutinosa, radix curcumae, radix scrophulariae, bulb of thunberg fritillary, pinellia ternate, pericarpium citri reticulatae viride, honeysuckle and wild chrysanthemum flower to obtain traditional Chinese medicine to be decocted, soaking the traditional Chinese medicine to be decocted with water for 1 hour, decocting at the temperature of 180-200 DEG C for 30-60 minutes, filtering the decoction, further, adding water into filter residues and decocting at the temperature of 180-200 DEG C for 30-60 minutes, filtering the decoction, and combining the decoctions; finally, mixing the obtained filtrate with the obtained decoction, and performing reduced-pressure concentration until the volume is 1/20-1/10 of the original volume, so as to obtain the traditional Chinese medicine mixture for treating thyroid enlargement. The traditional Chinese medicine mixture can be manufactured into an oral solution, a granular preparation, a troche and a capsule, and has a good curative effect on the thyroid enlargement.
Description
Technical field
The invention belongs to Thyreoidine treatment technology field, relate in particular to a kind of herb mixture for the treatment of thyromegaly and preparation method thereof and application.
Background technology
Thyromegaly is one of a kind of multiple commonly encountered diseases, from the beginning of there is no classical symptom, and the chap gradually of later head and neck,, sometimes there is dry cough in the weak discomfort of neck area of patient, hoarseness, dysphagia, affects work and sleep.At present the medicine symptomatic treatment such as the multiplex thyroxine sheet of western medical treatment or oral potassium iodide can relief of symptoms, but western medicine can not effect a radical cure, easily recurrence, and curative effect is also not obvious.
Summary of the invention
The object of the present invention is to provide a kind of herb mixture for the treatment of thyromegaly and preparation method thereof and application, be intended to solve the problem of western medical treatment DeGrain, easy recurrence.
The present invention is achieved in that a kind of herb mixture for the treatment of thyromegaly, is followingly prepared from by mass parts raw material: 15～50 parts of Rhizoma Dioscoreae Bulbiferaes to comprise, 20～30 parts of Sargassums, 10～20 parts of Thallus Laminariae (Thallus Eckloniae)s, excellent escape grass 9～15 parts, 5～10 parts, the Radix Rehmanniae, 5～10 parts of Radix Curcumaes, 15～50 parts of Radix Scrophulariaes, 20～30 parts of Bulbus Fritillariae Thunbergii, 10～20 parts of the Rhizoma Pinelliaes, 5～10 parts, Pericarpium Citri Reticulatae Viride, 15～30 parts of Flos Loniceraes, 15～30 parts of Flos Chrysanthemi Indicis.
Preferably, described herb mixture also comprises 15～30 mass parts Fructus Forsythiaes, 9～15 mass parts Radix Platycodoniss.
Preferably, described herb mixture is followingly prepared from by mass parts raw material to comprise: 30 parts of Rhizoma Dioscoreae Bulbiferaes, 25 parts of Sargassums, 15 parts of Thallus Laminariae (Thallus Eckloniae)s, 10 parts, the Radix Rehmanniae, 8 parts of Radix Curcumaes, 20 parts of Radix Scrophulariaes, 25 parts of Bulbus Fritillariae Thunbergii, 15 parts of the Rhizoma Pinelliaes, 8 parts, Pericarpium Citri Reticulatae Viride, excellent escape grass 10 parts, 20 parts of Flos Loniceraes, 20 parts of Flos Chrysanthemi Indicis, 20 parts of Fructus Forsythiaes, 10 parts of Radix Platycodoniss.
The preparation method that the present invention further provides the herb mixture of above-mentioned treatment thyromegaly, comprises the following steps:
(1) by excellent to 15～50 mass parts Rhizoma Dioscoreae Bulbiferaes, 20～30 mass parts Sargassums, 10～20 mass parts Thallus Laminariae (Thallus Eckloniae)s and 9～15 mass parts careless cutting add 1～5 mass parts sodium carbonate of escaping, at 80～100 ℃ of temperature with 60～120 mass parts water extraction for several times, merging filtrate;
(2) 5～10 mass parts Radix Rehmanniae, 5～10 mass parts Radix Curcumaes, 15～50 mass parts Radix Scrophulariaes, 20～30 mass parts Bulbus Fritillariae Thunbergii, 10～20 mass parts Rhizoma Pinelliaes, 5～10 mass parts Pericarpium Citri Reticulatae Virides, 15～30 mass parts Flos Loniceraes and 15～30 mass parts Flos Chrysanthemi Indicis are mixed to get to decocting herb, by 80～120 mass parts water soaking 1 hour for this decocting herb, 180～200 ℃ decoct 30～60min, leach decocting liquid, in filtering residue, add 180～200 ℃ of decoction 30～60min of 60～80 mass parts water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20～1/10, the herb mixture of the thyromegaly that obtains medical treatment.
Preferably, in step (2), described decocting herb also comprises 15～30 mass parts Fructus Forsythiaes, 9～15 mass parts Radix Platycodoniss.
The present invention further provides the application of above-mentioned herb mixture at treatment thyromegaly.
Preferably, the dosage form of described herb mixture is oral administration solution, granular preparation, tablet, capsule.
The present invention overcomes the deficiencies in the prior art, a kind of herb mixture for the treatment of thyromegaly and preparation method thereof and application are provided, by Rhizoma Dioscoreae Bulbiferae, Sargassum, Thallus Laminariae (Thallus Eckloniae) and the excellent grass of escaping are added to sodium carbonate, at 80～100 ℃ of temperature with water extraction for several times, merging filtrate; The Radix Rehmanniae, Radix Curcumae, Radix Scrophulariae, Bulbus Fritillariae Thunbergii, the Rhizoma Pinelliae, Pericarpium Citri Reticulatae Viride, Flos Lonicerae and Flos Chrysanthemi Indici are mixed to get to decocting herb, this decocting herb is soaked in water 1 hour, 180～200 ℃ decoct 30～60min, leach decocting liquid, decoct 30～60min toward adding water in filtering residue 180～200 ℃ again, leach decocting liquid, merge twice decocting liquid; Finally the filtrate obtaining and decocting liquid are mixed, be evaporated to original volume 1/20～1/10, the obtain medical treatment herb mixture of thyromegaly, this herb mixture can be made oral administration solution, granular preparation, tablet, capsule form, and thyromegaly is had to good curative effect.
The specific embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
Embodiment 1
The preparation method of the herb mixture for the treatment of thyromegaly, comprises the following steps:
(1) by excellent to 15g Rhizoma Dioscoreae Bulbiferae, 30g Sargassum, 10g Thallus Laminariae (Thallus Eckloniae) and the 15g careless cutting add 1g sodium carbonate of escaping, at 80～100 ℃ of temperature with 120g water extraction for several times, merging filtrate;
(2) the 5g Radix Rehmanniae, 10g Radix Curcumae, 15g Radix Scrophulariae, 30g Bulbus Fritillariae Thunbergii, the 10g Rhizoma Pinelliae, 10g Pericarpium Citri Reticulatae Viride, 15g Flos Lonicerae and 30g Flos Chrysanthemi Indici are mixed to get to decocting herb, this decocting herb is used to 80g water soaking 1 hour, 200 ℃ decoct 30min, leach decocting liquid, in filtering residue, add 180～200 ℃ of decoction 30min of 60g water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20, the herb mixture 1 of the thyromegaly that obtains medical treatment.
Embodiment 2
The preparation method of the herb mixture for the treatment of thyromegaly, comprises the following steps:
(1) by excellent to 50g Rhizoma Dioscoreae Bulbiferae, 20g Sargassum, 20g Thallus Laminariae (Thallus Eckloniae) and the 9g careless cutting add 5g sodium carbonate of escaping, at 80 ℃ of temperature with 60g water extraction for several times, merging filtrate;
(2) the 10g Radix Rehmanniae, 10g Radix Curcumae, 15g Radix Scrophulariae, 30g Bulbus Fritillariae Thunbergii, the 10g Rhizoma Pinelliae, 10g Pericarpium Citri Reticulatae Viride, 15g Flos Lonicerae and 30g Flos Chrysanthemi Indici are mixed to get to decocting herb, this decocting herb is used to 120g water soaking 1 hour, 200 ℃ decoct 60min, leach decocting liquid, in filtering residue, add 200 ℃ of decoction 60min of 60g water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20, the herb mixture 2 of the thyromegaly that obtains medical treatment.
Embodiment 3
The preparation method of the herb mixture for the treatment of thyromegaly, comprises the following steps:
(1) by excellent to 50g Rhizoma Dioscoreae Bulbiferae, 20g Sargassum, 20g Thallus Laminariae (Thallus Eckloniae) and the 9g careless cutting add 5g sodium carbonate of escaping, at 80 ℃ of temperature with 60g water extraction for several times, merging filtrate;
(2) the 5g Radix Rehmanniae, 10g Radix Curcumae, 15g Radix Scrophulariae, 30g Bulbus Fritillariae Thunbergii, the 10g Rhizoma Pinelliae, 10g Pericarpium Citri Reticulatae Viride, 15g Flos Lonicerae and 30g Flos Chrysanthemi Indici, 15g Fructus Forsythiae and 15g Radix Platycodonis are mixed to get to decocting herb, this decocting herb is used to 80g water soaking 1 hour, 200 ℃ decoct 60min, leach decocting liquid, in filtering residue, add 200 ℃ of decoction 60min of 80g water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20, the herb mixture 3 of the thyromegaly that obtains medical treatment.
Embodiment 4
The preparation method of the herb mixture for the treatment of thyromegaly, comprises the following steps:
(1) by excellent to 15～50 mass parts Rhizoma Dioscoreae Bulbiferaes, 20～30 mass parts Sargassums, 10～20 mass parts Thallus Laminariae (Thallus Eckloniae)s and 9～15 mass parts careless cutting add 1～5 mass parts sodium carbonate of escaping, at 80～100 ℃ of temperature with 60～120 mass parts water extraction for several times, merging filtrate;
(2) by 5～10 mass parts Radix Rehmanniae, 5～10 mass parts Radix Curcumaes, 15～50 mass parts Radix Scrophulariaes, 20～30 mass parts Bulbus Fritillariae Thunbergii, 10～20 mass parts Rhizoma Pinelliaes, 5～10 mass parts Pericarpium Citri Reticulatae Virides, 15～30 mass parts Flos Loniceraes and 15～30 mass parts Flos Chrysanthemi Indicis, 15～30 mass parts Fructus Forsythiaes and 9～15 mass parts Radix Platycodoniss are mixed to get decocting herb, by 80～120 mass parts water soaking 1 hour for this decocting herb, 180～200 ℃ decoct 30～60min, leach decocting liquid, in filtering residue, add 180～200 ℃ of decoction 30～60min of 60～80 mass parts water again, leach decocting liquid, merge decocting liquid twice,
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20～1/10, the herb mixture 4 of the thyromegaly that obtains medical treatment.
Embodiment 5
The preparation method of the herb mixture for the treatment of thyromegaly, comprises the following steps:
(1) by excellent to 30g Rhizoma Dioscoreae Bulbiferae, 25g Sargassum, 15g Thallus Laminariae (Thallus Eckloniae) and the 10g careless cutting add 4g sodium carbonate of escaping, at 90 ℃ of temperature with 100g water extraction for several times, merging filtrate;
(2) the 10g Radix Rehmanniae, 8g Radix Curcumae, 20g Radix Scrophulariae, 25g Bulbus Fritillariae Thunbergii, the 15g Rhizoma Pinelliae, 8g Pericarpium Citri Reticulatae Viride, 20g Flos Lonicerae and 20g Flos Chrysanthemi Indici, 20g Fructus Forsythiae and 10g Radix Platycodonis are mixed to get to decocting herb, this decocting herb is used to 100g water soaking 1 hour, 200 ℃ decoct 40min, leach decocting liquid, in filtering residue, add 180～200 ℃ of decoction 60min of 70g water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/15, the herb mixture 5 of the thyromegaly that obtains medical treatment.
Embodiment 6
The preparation of the granular preparation of Sugarless type, detailed process is as follows:
Toward 5% dextrin, 5% lactose that add its quality in the herb mixture 1 of the treatment thyromegaly of 1kg embodiment 1 gained, and the ethanol that is 60～70% by 1kg volumetric concentration is as binding agent, is mixed and made into soft material in trough type mixing machine.
Soft material is granulated with granulator, granule, after hot air circulation drying oven is dry at 60～75 ℃ of temperature, is used to shaking screen granulate, finally by automatic particle packaging machine subpackage, obtain 2kg granular preparation 1.
Embodiment 7
The preparation of the capsule preparations of Sugarless type, detailed process is as follows:
In the herb mixture 4 of the treatment thyromegaly obtaining toward 1kg embodiment 4, spray into its quality 60～70% hydroxypropyl methylcellulose solution; successively through high-speed mixing granulating machine granulate, HighefficientFluidbeddrier is dry, after shaking screen granulate; and add 0.5% micropowder silica gel of herb mixture 4 quality; pass through mixer mix homogeneously, the filling of hard capsule filling machine, obtaining content is 1.3kg capsule preparations 1 again.
Wherein, the hydroxypropyl methylcellulose solution ethanol that to refer to hydroxypropyl methylcellulose and volumetric concentration be 40% is mixed with the solution that mass volume ratio (kg/ml) is 3%.
Embodiment 8
The preparation of the tablet of Sugarless type, detailed process is as follows:
Toward 3% dextrin, 3% starch that add its quality in the herb mixture 5 of the melancholy treatment thyromegaly of 1kg embodiment 5 gained; the ethanol that is 60～70% by volumetric concentration after mix homogeneously is binding agent; process high-speed mixing granulating machine is granulated successively, HighefficientFluidbeddrier is dry, shaking screen granulate; and add 0.1% Pulvis Talci of herb mixture 5 quality; pass through again mixer mix homogeneously, tablet machine tabletting, obtain 1.1kg tablet 1.
Effect embodiment
The herb mixture 5 of preparing with embodiment 5 carries out toxicity test and clinical treatment observation to West Germany rabbit, and process of the test and result are as follows:
1, animal toxicity test
Get 20 of West Germany rabbits, male and female dual-purpose, body weight 2～2.5kg, divide two groups, 10 every group, wherein one group is overdose test group, two groups is normal amount test group, overdose group is 30ml/kg, and normal amount is 10ml/kg, and administering mode is administration by gavage administration, twice of every day, serve on seven days, observe administration reaction every day, result shows that the movable diet of two groups of rabbit is normal.
2, clinical observation
(1) physical data
Accept out-patient's 30 examples for medical treatment, wherein male 19 examples, female's 11 examples, 10～20 years old age, 6 examples, 21～30 years old 8 example, 31～40 years old 10 example, 40 years old above 6 example.
(2) diagnostic criteria
At the ill initial stage, patient feels off color, discomfort of neck area, loss of appetite, poor appetite, dry cough sometimes, hoarseness, the progressively chap of later cervical region, dysphagia.
(3) Therapeutic Method
Every day is oral twice, and sooner or later respectively once, according to the above-mentioned mode decoction of boiling medicine, ten days is a course for the treatment of, serve on three courses for the treatment of.
(4) efficacy assessment standard
Effective: patient's spirit, diet recover normal, observe 1 year without recidivist;
Take a turn for the better: patient's spirit and diet recover normal, cervical region is subsided a swelling gradually and is recovered normal;
Invalid: not reach improvement standard person.
(5) therapeutic outcome is as shown in table 1 below:
Table 1 therapeutic outcome
In three courses for the treatment of, with Drug therapy thyromegaly patient of the present invention 30 examples, effective 21 examples of result, 8 examples that take a turn for the better, invalid 1 example, obvious effective rate 70%, improvement rate 27%, total effective rate is 97%
Compare and the shortcoming and defect of prior art, the present invention has following beneficial effect: the herb mixture for the treatment of thyromegaly of the present invention is remarkable to thyromegaly therapeutic effect, and raw materials is simple and easy to get, cost is low, and preparation method is simple.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (7)
1. a herb mixture for the treatment of thyromegaly, is characterized in that, is followingly prepared from by mass parts raw material: 15～50 parts of Rhizoma Dioscoreae Bulbiferaes to comprise, 20～30 parts of Sargassums, 10～20 parts of Thallus Laminariae (Thallus Eckloniae)s, excellent escape grass 9～15 parts, 5～10 parts, the Radix Rehmanniae, 5～10 parts of Radix Curcumaes, 15～50 parts of Radix Scrophulariaes, 20～30 parts of Bulbus Fritillariae Thunbergii, 10～20 parts of the Rhizoma Pinelliaes, 5～10 parts, Pericarpium Citri Reticulatae Viride, 15～30 parts of Flos Loniceraes, 15～30 parts of Flos Chrysanthemi Indicis.
2. the herb mixture for the treatment of thyromegaly as claimed in claim 1, is characterized in that, described herb mixture also comprises 15～30 mass parts Fructus Forsythiaes, 9～15 mass parts Radix Platycodoniss.
3. the herb mixture for the treatment of thyromegaly as claimed in claim 2, is characterized in that, described herb mixture is followingly prepared from by mass parts raw material to comprise:
30 parts of Rhizoma Dioscoreae Bulbiferaes, 25 parts of Sargassums, 15 parts of Thallus Laminariae (Thallus Eckloniae)s, 10 parts, the Radix Rehmanniae, 8 parts of Radix Curcumaes, 20 parts of Radix Scrophulariaes, 25 parts of Bulbus Fritillariae Thunbergii, 15 parts of the Rhizoma Pinelliaes, 8 parts, Pericarpium Citri Reticulatae Viride, excellent escape grass 10 parts, 20 parts of Flos Loniceraes, 20 parts of Flos Chrysanthemi Indicis, 20 parts of Fructus Forsythiaes, 10 parts of Radix Platycodoniss.
4. the preparation method of the herb mixture for the treatment of thyromegaly claimed in claim 1, is characterized in that, comprises the following steps:
(1) by excellent to 15～50 mass parts Rhizoma Dioscoreae Bulbiferaes, 20～30 mass parts Sargassums, 10～20 mass parts Thallus Laminariae (Thallus Eckloniae)s and 9～15 mass parts careless cutting add 1～5 mass parts sodium carbonate of escaping, at 80～100 ℃ of temperature with 60～120 mass parts water extraction for several times, merging filtrate;
(2) 5～10 mass parts Radix Rehmanniae, 5～10 mass parts Radix Curcumaes, 15～50 mass parts Radix Scrophulariaes, 20～30 mass parts Bulbus Fritillariae Thunbergii, 10～20 mass parts Rhizoma Pinelliaes, 5～10 mass parts Pericarpium Citri Reticulatae Virides, 15～30 mass parts Flos Loniceraes and 15～30 mass parts Flos Chrysanthemi Indicis are mixed to get to decocting herb, by 80～120 mass parts water soaking 1 hour for this decocting herb, 180～200 ℃ decoct 30～60min, leach decocting liquid, in filtering residue, add 180～200 ℃ of decoction 30～60min of 60～80 mass parts water again, leach decocting liquid, merge twice decocting liquid;
(3) decocting liquid that filtrate step (1) being obtained and step (2) obtain mixes, and is evaporated to original volume 1/20～1/10, the herb mixture of the thyromegaly that obtains medical treatment.
5. the preparation method of the herb mixture for the treatment of thyromegaly as claimed in claim 4, is characterized in that, in step (2), described decocting herb also comprises 15～30 mass parts Fructus Forsythiaes, 9～15 mass parts Radix Platycodoniss.
6. the herb mixture described in claim 1～3 any one is in the application for the treatment of thyromegaly.
7. herb mixture as claimed in claim 6, in the application for the treatment of thyromegaly, is characterized in that, the dosage form of described herb mixture is oral administration solution, granular preparation, tablet, capsule.
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| CN104800781A (en) * | 2015-05-26 | 2015-07-29 | 柴秀平 | Traditional Chinese medicine preparation for treating chronic lymphocytic thyroiditis and preparation method of traditional Chinese medicine preparation |
| CN105267605A (en) * | 2015-10-26 | 2016-01-27 | 赖坤流 | Medicine for treating Proteus syndrome |
| CN105833111A (en) * | 2016-02-17 | 2016-08-10 | 青岛市中心医院 | Drug for treating goiter |
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| CN101152538A (en) * | 2007-09-15 | 2008-04-02 | 尹克华 | Traditional Chinese medicine for treating thyroid tumor |
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| CN101152538A (en) * | 2007-09-15 | 2008-04-02 | 尹克华 | Traditional Chinese medicine for treating thyroid tumor |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104800781A (en) * | 2015-05-26 | 2015-07-29 | 柴秀平 | Traditional Chinese medicine preparation for treating chronic lymphocytic thyroiditis and preparation method of traditional Chinese medicine preparation |
| CN105267605A (en) * | 2015-10-26 | 2016-01-27 | 赖坤流 | Medicine for treating Proteus syndrome |
| CN105833111A (en) * | 2016-02-17 | 2016-08-10 | 青岛市中心医院 | Drug for treating goiter |
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Application publication date: 20140528 |