CN103815459B - Spiced can of a kind of Jack-fruit seeds and preparation method thereof - Google Patents
Spiced can of a kind of Jack-fruit seeds and preparation method thereof Download PDFInfo
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- CN103815459B CN103815459B CN201410093910.9A CN201410093910A CN103815459B CN 103815459 B CN103815459 B CN 103815459B CN 201410093910 A CN201410093910 A CN 201410093910A CN 103815459 B CN103815459 B CN 103815459B
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- 244000025352 Artocarpus heterophyllus Species 0.000 title claims abstract description 71
- 235000008725 Artocarpus heterophyllus Nutrition 0.000 title claims abstract description 71
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
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- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 9
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- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims abstract description 9
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- 241000134253 Lanka Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
- A23L25/20—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof consisting of whole seeds or seed fragments
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/269—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of microbial origin, e.g. xanthan or dextran
- A23L29/27—Xanthan not combined with other microbial gums
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Dispersion Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to food processing field, disclose spiced can of a kind of Jack-fruit seeds and preparation method thereof.Preparation method of the present invention takes the Jack-fruit seeds after water, anise, Chinese prickly ash, cassia bark, good slurry, salt, dark soy sauce, monosodium glutamate, white granulated sugar and process, mix and carry out infusion, then cool, add stabilizing agent, tinning, exhaust sealing, sterilization cooling, smear tank and put in storage and get final product.The present invention is from the feature of Jack-fruit seeds self, selected suitable batching, optimizing machining technology technology is prepared into a kind of sweet mouthfeel, unique flavor, containing rich in protein, starch and dietary fiber, can body immunity be improved simultaneously, alleviate agitation, the Jack-fruit seeds can of the multiple health care such as treatment diarrhoea, improves the utilization rate of Jack-fruit seeds.
Description
Technical field
The present invention relates to food processing field, be specifically related to spiced can of a kind of Jack-fruit seeds and preparation method thereof.
Background technology
Jackfruit (ArtocarpusheterophyllsLam.) has another name called jackfruit, artocarpus heterophyllus, belong to Moraceae Artocarpus aiphyllium, catchment fruit, grain and preciousness material in the tropical tree species of one, originate in the India of Tropical Asia, extensively cultivate in tropic tides Humid Area, be mainly distributed in country in Southeast Asia as Sri Lanka, Burma, Indonesia, China etc.Mainly be distributed in Hainan, Guangdong, Guangxi, Yunnan, Fujian and Sichuan at home, wherein with Hainan Province's plantation at most.
Jackfruit is world-renowned tropical fruit (tree), the seed containing 13%-20% in fruit, seed ovalize, large as Chinese chestnut, be rich in starch, usual pulp eats rear remaining seed except utilizing it to carry out choose seeds, introduce a fine variety except mostly all do not utilized, this kind of wasting of resources beyond doubt.Research shows in Jack-fruit seeds containing abundant starch, account for more than 60% of whole kernel, its crude protein content is also higher simultaneously, account for more than 7% of kernel, heat 160 kilocalories, fatty 0.3g, vitamin C 16mg, dietary fiber 2.3g, simultaneously also containing calcium 18mg, magnesium 27mg, iron 1.6mg etc., there is higher nutritive value, can allay one's hunger on a small quantity, to the normal physiological function maintaining body, there is important function.Meanwhile, the effects such as the symptoms such as Jack-fruit seeds has can treat women's milk deficiency in postpartum, promote digestion, treatment diarrhoea, treatment are irritated depressed, anti-oxidant, immunological regulation, Jack-fruit seeds no matter boiling, stew in clear soup, still burn halogen, frying, all local flavor is aromatic, nutritious, there is higher diet therapy nutritional and be worth.
At present along with the day by day maturation of jackfruit production technology, the seed amount of discarding increases gradually, because its content of starch is higher, is need the starch resource needing to be developed badly.Jack-fruit seeds can not directly eat, nutriment wherein could be absorbed after finished product after must pass through processing, along with the progress of society, the raising of people's living standard, people require also more and more higher to name alkene fruit, not only need the fruit-like flavour with Hainan characteristic, also require to possess certain health-care efficacy.Therefore, the feature of Jack-fruit seeds can be made full use of to carry out deep processing.But report less to the research utilizing Jack-fruit seeds to carry out food processing both at home and abroad, and market there is no the product of shaping.
Summary of the invention
In view of this, the object of the present invention is to provide spiced can of a kind of Jack-fruit seeds and preparation method thereof, make described can sense organ fragrant and sweet, unique flavor;
Another object of the present invention makes described can contain rich in protein, starch and dietary fiber;
The multiple health care such as another object of the present invention described can is had improve body immunity, alleviates agitation, treatment diarrhoea.
For realizing above goal of the invention, the invention provides following technical scheme:
A preparation method for the spiced can of Jack-fruit seeds, comprising:
Take the Jack-fruit seeds after water, anise, Chinese prickly ash, cassia bark, good slurry, salt, dark soy sauce, monosodium glutamate, white granulated sugar and process, mix and carry out infusion, then cool, add stabilizing agent, tinning, exhaust sealing, sterilization cooling, smear tank and put in storage and get final product.
As preferably, described each raw material with parts by weight is:
Water 80-100 part, anistree 0.1-1.0 part, Chinese prickly ash 0.1-1.0 part, cassia bark 0.1-1.0 part, galingal 0.1-1.0 part, salt 1.0-2.0 part, dark soy sauce 0.5-2.0 part, monosodium glutamate 0.1-1.0 part, white granulated sugar 0.5-2.0 part, the Jack-fruit seeds 90-200 part after process, stabilizing agent 0.2-0.5 part.It should be noted that, in the present invention, above-mentioned each raw material weight mark independently can be selected from any one point value in respective scope, and can be combined with the raw material of other weight portions.Such as:
Water, it can be 80,85,90,95 or 100 weight portions;
Anise, it can be 0.1,0.11,0.12,0.13......0.50,0.51......0.98,0.99 or 1.0 weight portions;
Chinese prickly ash, it can be 0.1,0.11,0.12,0.13......0.50,0.51......0.98,0.99 or 1.0 weight portions;
Cassia bark, it can be 0.1,0.11,0.12,0.13......0.50,0.51......0.98,0.99 or 1.0 weight portions;
Galingal, it can be 0.1,0.11,0.12,0.13......0.50,0.51......0.98,0.99 or 1.0 weight portions;
Jack-fruit seeds after process, it can be 90,91,92......125,126......198,199 or 200 weight portions;
Stabilizing agent, it can be 0.20,0.21,0.22......0.33,0.34,0.35......0.48,0.49 or 0.50 weight portion;
Salt, it can be 1.0,1.1,1.2,1.3,1.4,1.5,1.6,1.7,1.8,1.9 or 2.0 weight portions;
Dark soy sauce, it can be 0.5,0.6......1.7,1.8,1.9 or 2.0 weight portions;
Monosodium glutamate, it can be 0.1,0.11,0.12,0.13......0.50,0.51......0.98,0.99 or 1.0 weight portions;
White granulated sugar, it can be 0.5,0.6......1.7,1.8,1.9 or 2.0 weight portions.
For the problem that Jack-fruit seeds resource utilization is not high, the present invention utilizes the feature of Jack-fruit seeds, selected batching, make sweet mouthfeel, unique flavor, have concurrently salty fragrant and sweet, containing rich in protein, starch and dietary fiber, can body immunity be improved simultaneously, alleviate agitation, the spiced can of Jack-fruit seeds of the multiple health care such as treatment diarrhoea.
As preferably, described stabilizing agent is xanthans.
As preferably, the described infusion time is 20-30min.
As preferably, the treatment step of the Jack-fruit seeds after described process is specially:
Get in maturation, disease-free Jack-fruit seeds soaking disinfection liquid, clean seed appearance pectin, with salt poach 15-20min, cooling, removes seed coat and plants clothing to complete process.According to preferred scheme, applicant considers local flavor and the mouthfeel of product, adopts salt poach in processing procedure, can realize pre-gelatinized, is conducive to follow-up local flavor infiltration, and the mouthfeel after infusion.
As preferably, the salt solution of described salt solution to be mass percent be 0.1-0.3%.
As preferably, described sterilization is sterilized for soaking 10-20min with 80-150ppm liquor natrii hypochloritis.
As preferably, sterilization temperature 121 DEG C, sterilizing time 30min is 0.5-1.0 hour from sealing to sterilizing time.
The spiced can of Jack-fruit seeds prepared by the present invention meets enterprise-quality standard and national food hygienic standard, every 100g heat content 1400 ~ 1800 kilojoule, protein 6 ~ 12g, fat 1 ~ 4g, dietary fiber 5 ~ 10g(wherein soluble dietary fiber 0.5 ~ 1.5g, soluble dietary fiber 5 ~ 9g after testing), ash content 5g ~ 8g, carbohydrate 70g ~ 80g, carry out different crowd taste flavor experimental investigation simultaneously, result shows, the spiced can sweet mouthfeel of Jack-fruit seeds of the present invention, unique flavor, have concurrently salty fragrant and sweet, high by approval rate.Meanwhile, the food General Requirements such as can have certain solid content, and therefore in preparation process, the present invention has certain deposited phenomenon and belongs to normal, keeps solid content in the present invention more than 35%, and ensure the stability of sample.
In addition, the present invention also investigates the health-care efficacy that hypoimmunity, disposition surveyee that is irritated, diarrhoea of often suffering from indiestion eat product of the present invention, result shows, the often surveyee of edible product of the present invention, immunity improves, the time decreased of mood agitation, stomach situation improves, and is not easy diarrhoea.
Thus, the present invention also provides a kind of Jack-fruit seeds prepared by preparation method of the present invention spiced can.
From above technical scheme, the present invention is from the feature of Jack-fruit seeds self, selected suitable batching, optimizing machining technology technology is prepared into a kind of sweet mouthfeel, unique flavor, containing rich in protein, starch and dietary fiber, body immunity can be improved simultaneously, alleviate agitation, the Jack-fruit seeds can of the multiple health care such as treatment diarrhoea, improves the utilization rate of Jack-fruit seeds.
Detailed description of the invention
The invention discloses spiced can of a kind of Jack-fruit seeds and preparation method thereof, those skilled in the art can use for reference present disclosure, and suitable improving technique parameter realizes.Special needs to be pointed out is, all similar replacements and change apparent to those skilled in the art, they are all deemed to be included in the present invention.Product of the present invention and preparation method are described by preferred embodiment, related personnel obviously can not depart from content of the present invention, spirit and scope methods and applications as herein described are changed or suitably change with combination, realize and apply the technology of the present invention.
Just spiced can of a kind of Jack-fruit seeds provided by the present invention and preparation method thereof is described further below.
Embodiment 1: prepare the spiced can of Jack-fruit seeds of the present invention
Jack-fruit seeds is sterilized: liquor natrii hypochloritis Jack-fruit seeds being immersed in 100ppm sterilizes 10min;
Precook: take Jack-fruit seeds 100Kg, with cold water 200L, add salt 0.3Kg, boil 20min, slightly split shell to seed coat, cooling, remove seed coat and plant clothing, obtain the seed cleaned standby seam after processing;
Batch mixing: take 90 parts of pure water, 0.2 part of anise, 0.1 portion of Chinese prickly ash, 0.1 part of cassia bark, 0.1 part of galingal, 1.5 portions of salt, 1 portion of dark soy sauce, 0.1 portion of monosodium glutamate, 1 portion of white granulated sugar, mix, adds the seed after 100 parts of process;
The xanthans adding 0.4 part, as stabilizing agent, in 121 DEG C of sterilization 30min after exhaust, sealing, refrigerates in-4 DEG C of sealings after cooling.
Product meets enterprise-quality standard and national food hygienic standard after testing, every 100g butt heat content 1546 kilojoule, protein 9.61g, fatty 1.35g, dietary fiber 7.56g(wherein soluble dietary fiber 0.83g, soluble dietary fiber 6.73g), ash content 6.66g, carbohydrate 74.82g.
Embodiment 2: prepare the spiced can of Jack-fruit seeds of the present invention
Jack-fruit seeds is sterilized: liquor natrii hypochloritis Jack-fruit seeds being immersed in 120ppm sterilizes 10min;
Precook: take Jack-fruit seeds 150Kg, with cold water 450L, add salt 0.6Kg, boil 20min, slightly split shell to seed coat, cooling, remove seed coat and plant clothing, obtain the seed cleaned standby seam after processing;
Batch mixing: take 92 parts of pure water, 0.3 part of anise, 0.2 portion of Chinese prickly ash, 0.3 part of cassia bark, 0.2 part of galingal, 1.8 portions of salt, 1.5 portions of dark soy sauce, 0.2 portion of monosodium glutamate, 1.2 portions of white granulated sugars, mix, adds the seed after 120 parts of process;
The xanthans adding 0.4 part, as stabilizing agent, in 121 DEG C of sterilization 30min after exhaust, sealing, refrigerates in-4 DEG C of sealings after cooling.
Product meets enterprise-quality standard and national food hygienic standard after testing, and every 100g heat content 1522 kilojoule, protein 10.64g, fatty 1.48g, dietary fiber 8.64g(be soluble dietary fiber 0.96g, soluble dietary fiber 7.68g wherein), ash content 7.62g, carbohydrate 71.62g.
Embodiment 3: prepare the spiced can of Jack-fruit seeds of the present invention
Jack-fruit seeds is sterilized: liquor natrii hypochloritis Jack-fruit seeds being immersed in 100ppm sterilizes 10min;
Precook: take Jack-fruit seeds 50Kg, with cold water 100L, add salt 0.15Kg, boil 20min, slightly split shell to seed coat, cooling, remove seed coat and plant clothing, obtain the seed cleaned standby seam after processing;
Batch mixing: take 87 parts of pure water, 0.1 part of anise, 0.1 portion of Chinese prickly ash, 0.1 part of cassia bark, 0.1 part of galingal, 0.8 portion of salt, 0.8 portion of dark soy sauce, 0.1 portion of monosodium glutamate, 0.8 portion of white granulated sugar, mix, adds the seed after 90 parts of process;
The xanthans adding 0.4 part, as stabilizing agent, in 121 DEG C of sterilization 30min after exhaust, sealing, refrigerates in-4 DEG C of sealings after cooling.
Product meets enterprise-quality standard and national food hygienic standard after testing, and every 100g heat content 1563 kilojoule, protein 8.26g, fatty 1.21g, dietary fiber 6.60g(be soluble dietary fiber 0.71g, soluble dietary fiber 5.89g wherein), ash content 5.98g, carbohydrate 77.95g.
Embodiment 4: mouthfeel experimental investigation
Respectively in Harbin, Hefei, Shanghai, Qinghai and each random investigation 300 people in city, 5, Haikou, respectively comprehensive grading evaluation is carried out to the color and luster of spiced Jack-fruit seeds can prepared by embodiment 1-3, soup juice, structural state, fragrance, hardness, flavour and other indexs: well for 90-100 divides, preferably 80-90 divides, mediumly to divide for 70-80, poor 60-70 divides, and difference is less than 60 points.Surveyee unanimously approves that described can sense organ is fragrant and sweet, unique flavor.
Wherein, statistics be 90% people think that the color and luster of described spiced Jack-fruit seeds can is good or better; The people of 89% thinks that the soup juice of described spiced Jack-fruit seeds can is good or better; The people of 91% thinks that the structural state of described spiced Jack-fruit seeds can is good or better; The people of 88% thinks that the fragrance of described spiced Jack-fruit seeds can is good or better; The people of 95% thinks that the hardness of described spiced Jack-fruit seeds can is good or better; The people of 88% thinks that the flavour of described spiced Jack-fruit seeds can is good or better; The people of 93% thinks that other indexs of described spiced Jack-fruit seeds can are good or better; .
In addition, in 60 people in Harbin, 93% thinks that the overall evaluation of described spiced Jack-fruit seeds can is good or better; In 60 people in Hefei, 96% thinks that the overall evaluation of described spiced Jack-fruit seeds can is good or better; In 60 people in Shanghai, 94% thinks that the overall evaluation of described spiced Jack-fruit seeds can is good or better; In 60 people in Qinghai, 99% thinks that the overall evaluation of described spiced Jack-fruit seeds can is good or better; In 60 people at Haikou, 98% thinks that the overall evaluation of described spiced Jack-fruit seeds can is good or better.As can be seen here, northern territory, middle part, west area, eastern region and southern areas all obtain good evaluation to spiced Jack-fruit seeds can of the present invention at home.
Embodiment 5: health-care efficacy is tested
1, Dong so-and-so, all day feels powerless in work, and daily thing is many, easily produces irritated mood, operating pressure causes greatly spiritual high-pressure, and cause frequent flu because body immunity declines to a great extent, eating spiced Jack-fruit seeds can continuously after 8 months, the state of mind is significantly better than before half a year, be in a cheerful frame of mind, irritated mood is little, and immunity improves, and physical function is improved;
2, Zhang, owing to suffering from indiestion, careless slightly will diarrhoea of eating, and indigestion, eating spiced Jack-fruit seeds can after 5 months, diarrhoea obviously reduces, digestion function of stomach and intestine is greatly improved, and feels gasteremphraxis, indigestible symptom never again.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (7)
1. a preparation method for the spiced can of Jack-fruit seeds, is characterized in that, comprising:
Take the Jack-fruit seeds after water, anise, Chinese prickly ash, cassia bark, galingal, salt, dark soy sauce, monosodium glutamate, white granulated sugar and process, mix and carry out infusion, then cool, add stabilizing agent, tinning, exhaust sealing, sterilization cooling, smear tank and put in storage and get final product;
The treatment step of described Jack-fruit seeds is specially:
Get in maturation, disease-free Jack-fruit seeds soaking disinfection liquid, clean seed appearance pectin, with salt poach 15-20min, cooling, removes seed coat and plants clothing to complete process.
2. preparation method according to claim 1, it is characterized in that, each raw material with parts by weight is:
Water 80-100 part, anistree 0.1-1.0 part, Chinese prickly ash 0.1-1.0 part, cassia bark 0.1-1.0 part, galingal 0.1-1.0 part, salt 1.0-2.0 part, dark soy sauce 0.5-2.0 part, monosodium glutamate 0.1-1.0 part, white granulated sugar 0.5-2.0 part, the Jack-fruit seeds 90-200 part after process, stabilizing agent 0.2-0.5 part.
3. preparation method according to claim 1, it is characterized in that, described stabilizing agent is xanthans.
4. preparation method according to claim 1, it is characterized in that, the described infusion time is 20-30min.
5. preparation method according to claim 1, is characterized in that, described sterilization is sterilized for soaking 10-20min with 80-150ppm liquor natrii hypochloritis.
6. preparation method according to claim 1, is characterized in that, the salt solution of described salt solution to be mass percent be 0.1-0.3%.
7. the spiced can of the Jack-fruit seeds that described in claim 1-6 any one prepared by preparation method.
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CN103333260A (en) * | 2013-07-17 | 2013-10-02 | 中国热带农业科学院香料饮料研究所 | Method for extracting starch from jack fruit seed |
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CN103333260A (en) * | 2013-07-17 | 2013-10-02 | 中国热带农业科学院香料饮料研究所 | Method for extracting starch from jack fruit seed |
CN103461746A (en) * | 2013-09-18 | 2013-12-25 | 中国热带农业科学院香料饮料研究所 | Jack fruit seed kernel rice dumplings as well as preparation method thereof |
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