CN103790006A - Method for preparing flame-retardant fabric finishing agent - Google Patents
Method for preparing flame-retardant fabric finishing agent Download PDFInfo
- Publication number
- CN103790006A CN103790006A CN201310622317.4A CN201310622317A CN103790006A CN 103790006 A CN103790006 A CN 103790006A CN 201310622317 A CN201310622317 A CN 201310622317A CN 103790006 A CN103790006 A CN 103790006A
- Authority
- CN
- China
- Prior art keywords
- parts
- mass
- weight parts
- finishing agent
- flame
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Detergent Compositions (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a method for preparing a flame-retardant fabric finishing agent. The method comprises the following steps: (1) grinding 2-3 weight parts of diammonium hydrogen phosphate, 15-17 weight parts of borax, 8-9 weight parts of trimethylol tripolyamide , 2-3 weight parts of tetrakis hydroxyethyl phosphorus chloride and 6-7 weight parts of sodium silicate, and uniformly mixing; (2) simultaneously adding 2-3 weight parts of dodecyl trimethyl ammonium sulfate, 5-6 weight parts of magnesium chloride, 150-180 weight parts of deionized water and 10-15 weight parts of tricresyl phosphate, finishing batching within 15-20 minutes, and uniformly stirring and mixing at the temperature of 60-65 DEG C; and (3) cooling to room temperature, sequentially adding 2-3 weight parts of hydroxypropyl methyl cellulose, 12-14 weight parts of triethanolamine and 8-9 weight parts of urea, uniformly stirring and mixing to obtain the flame-retardant fabric finishing agent. The invention provides a method for preparing the flame-retardant fabric finishing agent, and the fabric finished by the flame-retardant fabric finishing agent has high fire resistance and hidden combustion property, can prevent molten drops and is resistant to washing and dry cleaning.
Description
Technical field
The present invention relates to the preparation method of fabric fire-retardant finishing agent.
Background technology
Current fabric fire-retardant finishing agent effect is not on the market very desirable, and anti-flammable and the smouldering of the fabric after arrangement do not reach requirement, not water-fastness and dry-cleaning.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of fabric fire-retardant finishing agent, the fabric after arranging with this fabric fire-retardant finishing agent has good anti-flammable and smouldering, can prevent molten drop, water-fastness and dry-cleaning.
For achieving the above object, technical scheme of the present invention is the preparation method of a kind of fabric fire-retardant finishing agent of design, comprises the steps:
1) get 2-3 parts by mass diammonium hydrogen phosphate, 15-17 parts by mass borax, 8-9 parts by mass trihydroxy methyl three polyamide, 2-3 parts by mass four ethoxy phosphorus chloride, 6-7 parts by mass sodium metasilicate porphyrize, mix;
2) then add 2-3 parts by mass dodecyl trimethyl ammonium sulfate, 5-6 parts by mass magnesium chloride, 150-180 parts by mass deionized water, 10-15 parts by mass tricresyl phosphate simultaneously, in 15-20 minute, feed intake complete, be uniformly mixed at 60-65 ℃;
3) be cooled to room temperature, add successively 2-3 parts by mass hydroxypropyl methylcellulose, 12-14 parts by mass triethanolamine, 8-9 parts by mass urea, be uniformly mixed, obtain fabric fire-retardant finishing agent.
Advantage of the present invention and beneficial effect are: a kind of preparation method of fabric fire-retardant finishing agent is provided, and the fabric after arranging with this fabric fire-retardant finishing agent has good anti-flammable and smouldering, can prevent molten drop, water-fastness and dry-cleaning.
The specific embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples are only for technical scheme of the present invention is more clearly described, and can not limit the scope of the invention with this.
The concrete technical scheme of implementing of the present invention is:
Embodiment 1
A preparation method for fabric fire-retardant finishing agent, comprises the steps:
1) get 3 parts by mass diammonium hydrogen phosphates, 17 parts by mass boraxs, 9 parts by mass trihydroxy methyl three polyamide, 3 parts by mass four ethoxy phosphorus chloride, 7 parts by mass sodium metasilicate porphyrizes, mix;
2) then add 3 parts by mass dodecyl trimethyl ammonium sulfate, 6 parts by mass magnesium chlorides, 180 parts by mass deionized waters, 15 parts by mass tricresyl phosphates simultaneously, in 20 minutes, feed intake complete, be uniformly mixed at 65 ℃;
3) be cooled to room temperature, add successively 3 parts by mass hydroxypropyl methylcelluloses, 14 parts by mass triethanolamines, 9 parts by mass urea, be uniformly mixed, obtain fabric fire-retardant finishing agent.
Embodiment 2
A preparation method for fabric fire-retardant finishing agent, comprises the steps:
1) get 2 parts by mass diammonium hydrogen phosphates, 15 parts by mass boraxs, 8 parts by mass trihydroxy methyl three polyamide, 2 parts by mass four ethoxy phosphorus chloride, 6 parts by mass sodium metasilicate porphyrizes, mix;
2) then add 2 parts by mass dodecyl trimethyl ammonium sulfate, 5 parts by mass magnesium chlorides, 150 parts by mass deionized waters, 10 parts by mass tricresyl phosphates simultaneously, in 15 minutes, feed intake complete, be uniformly mixed at 60 ℃;
3) be cooled to room temperature, add successively 2 parts by mass hydroxypropyl methylcelluloses, 12 parts by mass triethanolamines, 8 parts by mass urea, be uniformly mixed, obtain fabric fire-retardant finishing agent.
Embodiment 3
A preparation method for fabric fire-retardant finishing agent, comprises the steps:
1) get 2.3 parts by mass diammonium hydrogen phosphates, 16 parts by mass boraxs, 8.9 parts by mass trihydroxy methyl three polyamide, 2.3 parts by mass four ethoxy phosphorus chloride, 6.7 parts by mass sodium metasilicate porphyrizes, mix;
2) then add 2.3 parts by mass dodecyl trimethyl ammonium sulfate, 5.6 parts by mass magnesium chlorides, 170 parts by mass deionized waters, 13 parts by mass tricresyl phosphates simultaneously, in 17 minutes, feed intake complete, be uniformly mixed at 63 ℃;
3) be cooled to room temperature, add successively 2.3 parts by mass hydroxypropyl methylcelluloses, 13 parts by mass triethanolamines, 8.9 parts by mass urea, be uniformly mixed, obtain fabric fire-retardant finishing agent.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, do not departing under the prerequisite of the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (1)
1. the preparation method of fabric fire-retardant finishing agent, is characterized in that, comprises the steps:
1) get 2-3 parts by mass diammonium hydrogen phosphate, 15-17 parts by mass borax, 8-9 parts by mass trihydroxy methyl three polyamide, 2-3 parts by mass four ethoxy phosphorus chloride, 6-7 parts by mass sodium metasilicate porphyrize, mix;
2) then add 2-3 parts by mass dodecyl trimethyl ammonium sulfate, 5-6 parts by mass magnesium chloride, 150-180 parts by mass deionized water, 10-15 parts by mass tricresyl phosphate simultaneously, in 15-20 minute, feed intake complete, be uniformly mixed at 60-65 ℃;
3) be cooled to room temperature, add successively 2-3 parts by mass hydroxypropyl methylcellulose, 12-14 parts by mass triethanolamine, 8-9 parts by mass urea, be uniformly mixed, obtain fabric fire-retardant finishing agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310622317.4A CN103790006A (en) | 2013-11-30 | 2013-11-30 | Method for preparing flame-retardant fabric finishing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310622317.4A CN103790006A (en) | 2013-11-30 | 2013-11-30 | Method for preparing flame-retardant fabric finishing agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103790006A true CN103790006A (en) | 2014-05-14 |
Family
ID=50666032
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310622317.4A Pending CN103790006A (en) | 2013-11-30 | 2013-11-30 | Method for preparing flame-retardant fabric finishing agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103790006A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104047092A (en) * | 2014-06-27 | 2014-09-17 | 江苏金宏针纺织有限公司 | Flame-retardant knitted fabric |
| CN104060478A (en) * | 2014-06-27 | 2014-09-24 | 江苏金宏针纺织有限公司 | Anti-cutting corrosion-resistant fabric |
| CN104328661A (en) * | 2014-11-28 | 2015-02-04 | 何庆堃 | Ramie cotton fabric finishing agent with water proof function |
| CN105239374A (en) * | 2015-11-27 | 2016-01-13 | 常熟市通惠织造有限公司 | Production process for antifouling cloth |
| CN105332279A (en) * | 2015-12-07 | 2016-02-17 | 常熟市永新印染有限公司 | After-finishing technology of wool fabric |
| CN105350311A (en) * | 2015-12-18 | 2016-02-24 | 苏州富美纺织科技有限公司 | Preparation method of plush fabric finishing liquid |
| CN105350289A (en) * | 2015-12-16 | 2016-02-24 | 常熟市华博毛纺织有限公司 | Finishing process for wool fabric |
| CN105369593A (en) * | 2015-12-16 | 2016-03-02 | 常熟绣珀纤维有限公司 | Preparation method of ultrahigh molecular weight polyethylene protofilament |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102352560A (en) * | 2011-07-28 | 2012-02-15 | 吴江征明纺织有限公司 | Textile flame-retardant finishing agent and preparation method thereof |
| CN102720060A (en) * | 2012-06-28 | 2012-10-10 | 华纺股份有限公司 | Method for performing flame-retardant finish on fabric in printing and dyeing process |
| CN102965923A (en) * | 2012-12-04 | 2013-03-13 | 海泰纺织（苏州）有限公司 | Flame-retardant finishing agent for textiles and preparation method of agent |
-
2013
- 2013-11-30 CN CN201310622317.4A patent/CN103790006A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102352560A (en) * | 2011-07-28 | 2012-02-15 | 吴江征明纺织有限公司 | Textile flame-retardant finishing agent and preparation method thereof |
| CN102720060A (en) * | 2012-06-28 | 2012-10-10 | 华纺股份有限公司 | Method for performing flame-retardant finish on fabric in printing and dyeing process |
| CN102965923A (en) * | 2012-12-04 | 2013-03-13 | 海泰纺织（苏州）有限公司 | Flame-retardant finishing agent for textiles and preparation method of agent |
Non-Patent Citations (1)
| Title |
|---|
| 周学良: "《精细化工产品手册.橡塑助剂》", 30 April 2002, 化学工业出版社 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104047092A (en) * | 2014-06-27 | 2014-09-17 | 江苏金宏针纺织有限公司 | Flame-retardant knitted fabric |
| CN104060478A (en) * | 2014-06-27 | 2014-09-24 | 江苏金宏针纺织有限公司 | Anti-cutting corrosion-resistant fabric |
| CN104328661A (en) * | 2014-11-28 | 2015-02-04 | 何庆堃 | Ramie cotton fabric finishing agent with water proof function |
| CN105239374A (en) * | 2015-11-27 | 2016-01-13 | 常熟市通惠织造有限公司 | Production process for antifouling cloth |
| CN105332279A (en) * | 2015-12-07 | 2016-02-17 | 常熟市永新印染有限公司 | After-finishing technology of wool fabric |
| CN105350289A (en) * | 2015-12-16 | 2016-02-24 | 常熟市华博毛纺织有限公司 | Finishing process for wool fabric |
| CN105369593A (en) * | 2015-12-16 | 2016-03-02 | 常熟绣珀纤维有限公司 | Preparation method of ultrahigh molecular weight polyethylene protofilament |
| CN105350311A (en) * | 2015-12-18 | 2016-02-24 | 苏州富美纺织科技有限公司 | Preparation method of plush fabric finishing liquid |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103790006A (en) | Method for preparing flame-retardant fabric finishing agent | |
| CN104072805B (en) | A kind of preparation method of composite flame-retardant agent based on Vermiculitum | |
| CN102965923A (en) | Flame-retardant finishing agent for textiles and preparation method of agent | |
| CN102992786A (en) | Preparation method and usage method for foundry silicate binder | |
| CN103643501A (en) | Process for preparing soft fabric finishing agent | |
| CN103789999A (en) | Flame-retardant finishing method for polyester fabric | |
| CN102965939A (en) | Fire-proof flame retardant specially used for curtain and preparation method thereof | |
| CN102604575B (en) | Modified urea formaldehyde adhesive and preparation method thereof | |
| CN109081628A (en) | A kind of high-performance composite cement grinding aid and preparation method thereof | |
| CN103074082A (en) | Potent flame retardant | |
| CN103773393B (en) | Composite type flame retardant containing modified zeolite powder | |
| CN104163600B (en) | A kind of environment-friendly insulating mortar and preparation method thereof | |
| CN103741461B (en) | A kind of acrylic fibers material treatment agent and its preparation method | |
| CN103790005A (en) | Method for producing fireproof mildew-proof shell fabric | |
| CN105386303A (en) | High-temperature-resistant blended yarn | |
| CN103790018A (en) | Method for preparing durable fabric water repellent finishing agent | |
| CN103757898B (en) | A kind of polyester fiber finishing agent and preparation method thereof | |
| CN106049786A (en) | Elastic fireproof wallboard | |
| CN105968602A (en) | Flame retardant foamed polystyrene resin and preparation method thereof | |
| CN109456627A (en) | A kind of fireproof flame-retardant coating and preparation method thereof | |
| CN104497361A (en) | New environmentally-friendly rubber flame retardant | |
| CN105506976A (en) | Dyeing and finishing process for composite fabric | |
| CN105421072A (en) | Dyeing and finishing process of polar fleece | |
| CN105085969A (en) | Composite inorganic foaming agent and preparation method thereof | |
| CN105332279A (en) | After-finishing technology of wool fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20140514 |