CN103788790A - Fireproof coating and preparation method thereof - Google Patents

Fireproof coating and preparation method thereof Download PDF

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Publication number
CN103788790A
CN103788790A CN201410030163.4A CN201410030163A CN103788790A CN 103788790 A CN103788790 A CN 103788790A CN 201410030163 A CN201410030163 A CN 201410030163A CN 103788790 A CN103788790 A CN 103788790A
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Prior art keywords
parts
retardant coating
frie retardant
solvent
aluminum silicate
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CN201410030163.4A
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Chinese (zh)
Inventor
曹伟
葛锦妹
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Nantong Haiou Lift-Saving & Protection Equipment Co Ltd
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Nantong Haiou Lift-Saving & Protection Equipment Co Ltd
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Priority to CN201410030163.4A priority Critical patent/CN103788790A/en
Publication of CN103788790A publication Critical patent/CN103788790A/en
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Abstract

The invention provides a fireproof coating and a preparation method thereof. The fireproof coating comprises the following components in parts by weight (100 parts in total): 10-20 parts of aluminum silicate fibers, 5-15 parts of expanded perlite, 5-10 parts of ammonium polyphosphate, 3-8 parts of a curing agent, 25-30 parts of acrylic resin, 3-8 parts of pentaerythritol, and the balance of a solvent. The preparation method comprises the following steps: (1) adding expanded perlite, ammonium polyphosphate, the curing agent, and pentaerythritol in the solvent in proportion in a mixed mode, and after the added mixture is uniformly stirred, carrying out high-speed grinding on the obtained mixture until the fineness is 15-20 mu m; (2) adding aluminum silicate fibers and acrylic resin in a solution obtained in the step (1) in proportion, and after the added mixture is uniformly stirred, carrying out high-speed dispersing on the obtained mixture 15-20 min. The fireproof coating provided by the invention is not easy to crack under a large temperature difference condition, and also not easy to crack under a dry or wet condition, therefore, the fireproof coating is better in fireproof performance, and wider in application range.

Description

A kind of frie retardant coating and preparation method thereof
Technical field
The present invention relates to paint field, be specifically related to a kind of frie retardant coating and preparation method thereof.
Background technology
Frie retardant coating refers to and is applied to flammable substrates surface, in order to change material surface combustioncharacteristics, blocks fire rapid spread; Or be applied on building slab, in order to improve the speciality coating of the fire endurance building.By the surface at those inflammable materials by paint brush, improve the refractory ability of material, slow down propagation of flame velocity of propagation, or can stop burning within a certain period of time.
It is poor that current some frie retardant coatings on the market often have weathering resistance, and As time goes on, fire resistance declines, the shortcoming of functional defect face.
Summary of the invention
In view of above-mentioned information, it is a kind of with low cost that one of object of the present invention is to provide, excellent performance, the frie retardant coating of complete function.
The invention provides a kind of frie retardant coating, 100 parts of meters comprise following component by weight: 10~20 parts of aluminum silicate fibers, 5~15 parts of pearlstones, 5~10 parts of ammonium polyphosphates, 3~8 parts, solidifying agent, 25~30 parts of acrylic resins, 3~8 parts of tetramethylolmethanes, all the other are solvent.
Preferably, 100 parts of meters comprise following component by weight: 10~15 parts of aluminum silicate fibers, and 5~12 parts of pearlstones, 5~8 parts of ammonium polyphosphates, 5~8 parts, solidifying agent, 25~28 parts of acrylic resins, 3~6 parts of tetramethylolmethanes, all the other are solvent.
Most preferably, 100 parts of meters comprise following component by weight: 12 parts of aluminum silicate fibers, and 10 parts of pearlstones, 6 parts of ammonium polyphosphates, 6 parts, solidifying agent, 25 parts of acrylic resins, 5 parts of tetramethylolmethanes, all the other are solvent.
Described solvent is selected from one or more in pimelinketone, propyl carbinol, butyl glycol ether.
Described solidifying agent is xylidine or 2,4-dihydroxy-benzene ketone.
The preparation method who another object of the present invention is to provide a kind of frie retardant coating, comprises the steps:
(1), by pearlstone, ammonium polyphosphate, solidifying agent, tetramethylolmethane is mixed to join in solvent by proportioning, after stirring, carries out speed lapping, to fineness 15-20 μ m;
(2), aluminium silicate fiber peacekeeping acrylic resin is joined in solution obtained in the previous step by proportioning,, after stirring, high speed dispersion 15~20min, obtains frie retardant coating of the present invention.
A kind of frie retardant coating provided by the invention, adopts aluminium silicate fiber peacekeeping acrylic resin to coordinate, and has obtained good effect, and also not easy to crack under huge temperature difference condition, also not easy to crack under dry or wet condition, fire resistance is better, and range of application is wider.
Embodiment
The following examples can make the present invention of those skilled in the art comprehend, but do not limit the present invention in any way.
Embodiment 1
Get 5 parts of pearlstones, 5 parts of ammonium polyphosphates, 3 parts of xylidines, 3 parts of tetramethylolmethanes are mixed to join in pimelinketone by proportioning, after stirring, carry out speed lapping, to fineness 15-20 μ m; 10 parts of aluminum silicate fibers are joined in solution obtained in the previous step by proportioning with 20 parts of acrylic resins, and after stirring, high speed dispersion 15~20min, obtains frie retardant coating 1, and its performance test results is in table 1.
Table 1 frie retardant coating 1 aptitude test result
Figure BDA0000460113270000021
Embodiment 2
Get 12 parts of pearlstones, 8 parts of ammonium polyphosphates, 5 parts of 2,4-dihydroxy-benzene ketones, 6 parts of tetramethylolmethanes are mixed to join in propyl carbinol by proportioning, after stirring, carry out speed lapping, to fineness 15-20 μ m; 15 parts of aluminum silicate fibers are joined in solution obtained in the previous step by proportioning with 28 parts of acrylic resins, and after stirring, high speed dispersion 15~20min, obtains frie retardant coating 2, and its performance test results is in table 2.
Table 2 frie retardant coating 2 aptitude test results
Figure BDA0000460113270000022
Figure BDA0000460113270000031
Embodiment 3
Get 15 parts of pearlstones, 10 parts of ammonium polyphosphates, 8 parts of xylidines, 8 parts of tetramethylolmethanes are mixed to join in propyl carbinol by proportioning, after stirring, carry out speed lapping, to fineness 15-20 μ m; 20 parts of aluminum silicate fibers are joined in solution obtained in the previous step by proportioning with 30 parts of acrylic resins, and after stirring, high speed dispersion 15~20min, obtains frie retardant coating 3, and its performance test results is in table 3.
Table 3 frie retardant coating 3 aptitude test results
Embodiment 4
Get 10 parts of pearlstones, 6 parts of ammonium polyphosphates, 6 parts of xylidines, 5 parts of tetramethylolmethanes are mixed to join in butyl glycol ether by proportioning, after stirring, carry out speed lapping, to fineness 15-20 μ m; 12 parts of aluminum silicate fibers are joined in solution obtained in the previous step by proportioning with 25 parts of acrylic resins, and after stirring, high speed dispersion 15~20min, obtains frie retardant coating 4, and its performance test results is in table 4.
Table 4 frie retardant coating 4 aptitude test results
Figure BDA0000460113270000033

Claims (6)

1. a frie retardant coating, is characterized in that, 100 parts of meters comprise following component by weight: 10 ~ 20 parts of aluminum silicate fibers, 5 ~ 15 parts of pearlstones, 5 ~ 10 parts of ammonium polyphosphates, 3 ~ 8 parts, solidifying agent, 25 ~ 30 parts of acrylic resins, 3 ~ 8 parts of tetramethylolmethanes, all the other are solvent.
2. a kind of frie retardant coating according to claim 1, is characterized in that, 100 parts of meters comprise following component by weight: 10 ~ 15 parts of aluminum silicate fibers, 5 ~ 12 parts of pearlstones, 5 ~ 8 parts of ammonium polyphosphates, 5 ~ 8 parts, solidifying agent, 25 ~ 28 parts of acrylic resins, 3 ~ 6 parts of tetramethylolmethanes, all the other are solvent.
3. a kind of frie retardant coating according to claim 1, is characterized in that, 100 parts of meters comprise following component by weight: 12 parts of aluminum silicate fibers, 10 parts of pearlstones, 6 parts of ammonium polyphosphates, 6 parts, solidifying agent, 25 parts of acrylic resins, 5 parts of tetramethylolmethanes, all the other are solvent.
4. a kind of frie retardant coating according to claim 1, is characterized in that, described solvent is selected from one or more in pimelinketone, propyl carbinol, butyl glycol ether.
5. a kind of frie retardant coating according to claim 1, is characterized in that, described solidifying agent is xylidine or 2,4-dihydroxy-benzene ketone.
6. the preparation method based on a kind of frie retardant coating claimed in claim 1, is characterized in that, comprises the steps:
(1), by pearlstone, ammonium polyphosphate, solidifying agent, tetramethylolmethane is mixed to join in solvent by proportioning, after stirring, carries out speed lapping, to fineness 15-20 μ m;
(2), aluminium silicate fiber peacekeeping acrylic resin is joined in solution obtained in the previous step by proportioning,, after stirring, high speed dispersion 15 ~ 20min, obtains frie retardant coating of the present invention.
CN201410030163.4A 2014-01-22 2014-01-22 Fireproof coating and preparation method thereof Withdrawn CN103788790A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106752580A (en) * 2016-12-16 2017-05-31 芜湖天鸿汽车零部件有限公司 A kind of automobile fireproof coating and preparation method thereof
CN107141947A (en) * 2017-05-31 2017-09-08 安庆永大体育用品有限公司 A kind of plank fireproof coating and preparation method thereof
CN108059909A (en) * 2017-11-24 2018-05-22 惠水县凡趣创意科技有限公司 A kind of fireproof coating and preparation method thereof
CN109266128A (en) * 2018-09-17 2019-01-25 佛山市禅城区诺高环保科技有限公司 A kind of steel structure surface fireproof coating
CN109988534A (en) * 2019-03-13 2019-07-09 河南诚信密封材料有限公司 A kind of anti-oxidation edge sealing adhesive of TBS and preparation method thereof

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CN101344006A (en) * 2008-08-20 2009-01-14 厦门大学 Tunnel fire-proof slab and preparation method thereof
CN102173691A (en) * 2011-02-22 2011-09-07 山西省交通科学研究院 Single-component tunnel fire-retardant coating and preparation method thereof
CN102559054A (en) * 2011-12-28 2012-07-11 四川汉邦石化有限责任公司 High-efficiency fireproof corrosionproof paint of steel structure
CN103087601A (en) * 2011-10-31 2013-05-08 亚士创能科技(上海)股份有限公司 Fireproof composition and fireproof heat insulation plate

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EP1616924A1 (en) * 2004-07-13 2006-01-18 Huntsman Advanced Materials (Switzerland) GmbH Fire retardant composition
CN101323719A (en) * 2007-06-15 2008-12-17 上海金力泰化工股份有限公司 Construction curtain wall ceramic
CN101344006A (en) * 2008-08-20 2009-01-14 厦门大学 Tunnel fire-proof slab and preparation method thereof
CN102173691A (en) * 2011-02-22 2011-09-07 山西省交通科学研究院 Single-component tunnel fire-retardant coating and preparation method thereof
CN103087601A (en) * 2011-10-31 2013-05-08 亚士创能科技(上海)股份有限公司 Fireproof composition and fireproof heat insulation plate
CN102559054A (en) * 2011-12-28 2012-07-11 四川汉邦石化有限责任公司 High-efficiency fireproof corrosionproof paint of steel structure

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106752580A (en) * 2016-12-16 2017-05-31 芜湖天鸿汽车零部件有限公司 A kind of automobile fireproof coating and preparation method thereof
CN107141947A (en) * 2017-05-31 2017-09-08 安庆永大体育用品有限公司 A kind of plank fireproof coating and preparation method thereof
CN108059909A (en) * 2017-11-24 2018-05-22 惠水县凡趣创意科技有限公司 A kind of fireproof coating and preparation method thereof
CN109266128A (en) * 2018-09-17 2019-01-25 佛山市禅城区诺高环保科技有限公司 A kind of steel structure surface fireproof coating
CN109988534A (en) * 2019-03-13 2019-07-09 河南诚信密封材料有限公司 A kind of anti-oxidation edge sealing adhesive of TBS and preparation method thereof

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Application publication date: 20140514