CN103773340B - High strength consolidation type plugging agent - Google Patents

High strength consolidation type plugging agent Download PDF

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Publication number
CN103773340B
CN103773340B CN201310748470.1A CN201310748470A CN103773340B CN 103773340 B CN103773340 B CN 103773340B CN 201310748470 A CN201310748470 A CN 201310748470A CN 103773340 B CN103773340 B CN 103773340B
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China
Prior art keywords
content
high strength
plugging agent
drilling fluid
consolidation type
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Active
Application number
CN201310748470.1A
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Chinese (zh)
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CN103773340A (en
Inventor
隋跃华
关芳
张平
李兴会
刘全江
林卫东
何兴华
吕讨论
马宜超
薛龙
张帅
曹小虎
李强
高峰
刘密密
贺智
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DONGYING TAIER PETROLEUM TECHNOLOGY Co Ltd
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DONGYING TAIER PETROLEUM TECHNOLOGY Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/426Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement
    • C09K8/467Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement containing additives for specific purposes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Structural Engineering (AREA)
  • Soil Conditioners And Soil-Stabilizing Materials (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Sealing Material Composition (AREA)

Abstract

A kind of high strength consolidation type plugging agent, its composition and content are weight part: calcium carbonate 20-40; Silicon-dioxide 5-10; Calcium chloride 1-4; Polyanionic Cellulose 0.1-0.4; Drilling fluid xanthan gum 0.1-0.2; Aluminum oxide 5-10; Magnesium oxide 3-8; Oil well cement? 10-16.By above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.The present invention has that raw material sources are extensive, intensity is high, outstanding excessive ability is strong, mobility, pumpability are good, there is condense shut-off capacity and microdilatancy performance, dissolubility of holding concurrently is good, the features such as leak stopping success ratio is high, technique simple, construction safety, extensively apply in oil, geological drilling technique, special adaptation, is applied in Fractured hard formation and Caves stratum.

Description

High strength consolidation type plugging agent
Technical field
The present invention relates to drilling plugging agent, particularly a kind of high strength consolidation type plugging agent.
Background technology
The plugging agent with some strength that existing a kind of petroleum drilling uses is quick talking cement, its formula is: oil well cement 100 parts, water 40-50 part, setting accelerator 5-30 part, its leak-stopping technique being petroleum drilling has played effect, but it also exists following shortcoming or deficiency simultaneously: 1. thickening time, setting time and pumpable time are difficult to control, and grout very easily occurs and runs off fast or fast setting problem, and construction safety is difficult to ensure; 2. cement slurry density is high, and easily pressure leaks stratum, and viscous flow ability is bad; 3. viscosity is low, not easily in leakage channel remain in a standstill, solidify after easily come from water, shut-off capacity is poor; 4. setting time, set strength are uncontrollable; 5. after leak stopping, the stopper staying shaft bottom is stone, and the brill plug time is long, and easily make new advances well, or occurs again new leakage after having bored plug, and easily generation repeats leak stopping phenomenon, causes cost up.
Summary of the invention
The object of this invention is to provide a kind of high strength consolidation type plugging agent, adopt the formulated in combination with organism, inorganics and the high molecular polymer that granularity is little, intensity is high, after leak stopping, crushing resistance is high, effectively overcome or avoid the shortcoming that exists in above-mentioned prior art or deficiency, effectively improve plugging effect, shorten drilling period, improve drill speed.
High strength consolidation type plugging agent of the present invention, its composition and content, content is weight part: calcium carbonate 20-40; Silicon-dioxide 5-10; Calcium chloride 1-4; Polyanionic Cellulose 0.1-0.4; Drilling fluid xanthan gum 0.1-0.2; Aluminum oxide 5-10; Magnesium oxide 3-8; Oil well cement 10-16.
Compound method: above-mentioned substance, by its component and content, under normal temperature and pressure, adds successively in kneader with conventional formulation method, mixing and stirring, treats that it dry, pulverize into the particulate preparation of 0.05mm-1mm.
The present invention's tool compared with existing plugging agent has the following advantages or beneficial effect:
1, leakage-stop liquid has the character of consolidation after entering leakage channel, and intensity is high;
2, intensity is high, and expansion character is good, and volume does not reduce.
3, shut-off capacity is strong, can repair low pressure ravelly ground, improves the bearing resistance of absorption well section.
4, outstanding excessive ability is strong, and good fluidity, pumpability is good, can enter leakage channel deep.
5, setting time, set strength is adjustable, can form high strength lost circulation plug in leakage channel.
6, the lost circulation plug formed in annular space, moderate strength, drillability is good, not easily gets out new well, shortens and sweeps the plug time.
7, leak stopping slurry easily remains in a standstill in leakage channel deep, and multiple leakage not easily occurs the high strength leak stopping stopper formed in leakage channel after boring plug, and leak stopping success ratio is high.
8, little to environmental influence, nontoxic, pollution-free, construction safety is quick.
Embodiment:
A kind of high strength consolidation type plugging agent, its composition and content, content is weight part: calcium carbonate 20-40; Silicon-dioxide 5-10; Calcium chloride 1-4; Polyanionic Cellulose 0.1-0.4; Drilling fluid xanthan gum 0.1-0.2; Aluminum oxide 5-10; Magnesium oxide 3-8; Oil well cement 10-16.
Compound method: above-mentioned substance, by its component and content, under normal temperature and pressure, adds successively in kneader with conventional formulation method, mixing and stirring, treats that it dry, pulverize into the particulate preparation of 0.05mm-1mm.During use, in plugging drilling fluid, add the 2%-15% high strength consolidation type of the present invention plugging agent of plugging drilling fluid total amount.
Provide specific embodiment below:
1st example
Calcium carbonate 20; Silicon-dioxide 5; Calcium chloride 1; Polyanionic Cellulose 0.1; Drilling fluid xanthan gum 0.1; Aluminum oxide 5; Magnesium oxide 3; Oil well cement 10.By above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.During use, in plugging drilling fluid, add the high strength consolidation type plugging agent of the present invention of plugging drilling fluid total amount 2%.
2nd example
Calcium carbonate 27; Silicon-dioxide 7; Calcium chloride 2; Polyanionic Cellulose 0.2; Drilling fluid xanthan gum 0.12; Aluminum oxide 7; Magnesium oxide 5, oil well cement 12.By above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.During use, in plugging drilling fluid, add the high strength consolidation type plugging agent of the present invention of plugging drilling fluid total amount 8%.
3rd example
Calcium carbonate 40; Silica 10; Calcium chloride 4; Polyanionic Cellulose 0.4; Drilling fluid xanthan gum 0.2; Aluminum oxide 10; Magnesium oxide 8; Oil well cement 16.By above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.During use, in plugging drilling fluid, add the high strength consolidation type plugging agent of the present invention of plugging drilling fluid total amount 15%.
4th example
Calcium carbonate 35; Silicon-dioxide 9; Calcium chloride 3; Polyanionic Cellulose 0.34; Drilling fluid xanthan gum 0.15; Aluminum oxide 9; Magnesium oxide 7; Oil well cement 14.By above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.During use, in plugging drilling fluid, add the high strength consolidation type plugging agent of the present invention of plugging drilling fluid total amount 12%.
1st example, the 2nd example, the 3rd example are embodiment, and the 4th example is comparative example, has plugging effect very in using at the scene.

Claims (1)

1. a high strength consolidation type plugging agent, its composition and content, content is weight part:
Calcium carbonate 20-40
Silicon-dioxide 5-10
Calcium chloride 1-4
Polyanionic Cellulose 0.1-0.4
Drilling fluid xanthan gum 0.1-0.2
Aluminum oxide 5-10
Magnesium oxide 3-8
Oil well cement 10-16;
Compound method: by above-mentioned substance by its component and content, under normal temperature and pressure, add successively in kneader with conventional formulation method, mixing and stirring, treat that it dry, pulverize into the powder that particle diameter is 0.01mm – 0.2mm.
CN201310748470.1A 2013-12-31 2013-12-31 High strength consolidation type plugging agent Active CN103773340B (en)

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Application Number Priority Date Filing Date Title
CN201310748470.1A CN103773340B (en) 2013-12-31 2013-12-31 High strength consolidation type plugging agent

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CN103773340A CN103773340A (en) 2014-05-07
CN103773340B true CN103773340B (en) 2016-02-24

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108300435A (en) * 2018-02-08 2018-07-20 陕西海睿能源技术服务有限公司 A kind of embedded high pressure-bearing sealing agent

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105131922B (en) * 2015-07-31 2018-08-07 山东盛海科贸有限公司 Workover treatment borehole wall resistance to compression stabilizer and its application process
CN110903815A (en) * 2019-12-20 2020-03-24 东营泰尔石油技术有限公司 High-strength leakage-stopping slurry
CN110872500A (en) * 2019-12-20 2020-03-10 山东华越天成石油技术有限责任公司 Asphalt layer leakage plugging slurry
CN112341065B (en) * 2020-12-01 2021-12-24 中国石油大学(北京) Non-cementing leaking stoppage cement slurry and preparation method thereof
CN114196387A (en) * 2021-07-16 2022-03-18 中国石油天然气集团有限公司 Shear-dilution type acid-soluble inorganic curing plugging agent, and preparation method and application thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5749418A (en) * 1997-04-14 1998-05-12 Halliburton Energy Services, Inc. Cementitious compositions and methods for use in subterranean wells
CN101353570A (en) * 2008-09-03 2009-01-28 中国石油新疆油田分公司采油工艺研究院 Heavy crude thermal recovery steamed well slag plugging agent
CN102277145A (en) * 2011-06-03 2011-12-14 西南石油大学 Magnesium-oxygen cement slurry used for reservoir water plugging, leak plugging and temporary-closure plugging in oil and gas well and preparation method thereof
CN102719232A (en) * 2012-06-15 2012-10-10 中国石油化工股份有限公司 Bridging particle for shallow casing blind hole

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060167133A1 (en) * 2005-01-24 2006-07-27 Jan Gromsveld Sealant composition comprising a crosslinkable material and a reduced amount of cement for a permeable zone downhole

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5749418A (en) * 1997-04-14 1998-05-12 Halliburton Energy Services, Inc. Cementitious compositions and methods for use in subterranean wells
CN101353570A (en) * 2008-09-03 2009-01-28 中国石油新疆油田分公司采油工艺研究院 Heavy crude thermal recovery steamed well slag plugging agent
CN102277145A (en) * 2011-06-03 2011-12-14 西南石油大学 Magnesium-oxygen cement slurry used for reservoir water plugging, leak plugging and temporary-closure plugging in oil and gas well and preparation method thereof
CN102719232A (en) * 2012-06-15 2012-10-10 中国石油化工股份有限公司 Bridging particle for shallow casing blind hole

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108300435A (en) * 2018-02-08 2018-07-20 陕西海睿能源技术服务有限公司 A kind of embedded high pressure-bearing sealing agent
CN108300435B (en) * 2018-02-08 2021-09-07 陕西海睿能源技术服务有限公司 Embedded high-pressure-bearing plugging agent

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