CN103740341B - The agent of leak stopping pressure-bearing - Google Patents

The agent of leak stopping pressure-bearing Download PDF

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Publication number
CN103740341B
CN103740341B CN201310748479.2A CN201310748479A CN103740341B CN 103740341 B CN103740341 B CN 103740341B CN 201310748479 A CN201310748479 A CN 201310748479A CN 103740341 B CN103740341 B CN 103740341B
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China
Prior art keywords
pressure
bearing
content
agent
leak stopping
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Active
Application number
CN201310748479.2A
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Chinese (zh)
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CN103740341A (en
Inventor
隋跃华
关芳
刘全江
何立成
张喜民
邱光源
顾法钊
谢海龙
孙秀鹏
曹文学
王宏超
池占福
张艳
马玉峥
曹小虎
刘智杰
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DONGYING TAIER PETROLEUM TECHNOLOGY Co Ltd
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DONGYING TAIER PETROLEUM TECHNOLOGY Co Ltd
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Priority to CN201310748479.2A priority Critical patent/CN103740341B/en
Publication of CN103740341A publication Critical patent/CN103740341A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/426Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement

Abstract

The agent of a kind of leak stopping pressure-bearing, its composition and content are weight part: calcium carbonate 20-30, perlite powder 10-15, G level oil well cement 2-5, quartz sand 10-15; Calucium Silicate powder 10-20, oyster shell whiting 10-15, calcium hydroxide 1-4, drilling fluid xanthan gum 0.1-0.4, Polyacrylamide 0.1-0.4, Polyanionic Cellulose 0.1-0.4; Above-mentioned substance, by its component and content, under normal temperature and pressure, adds in molten device successively with conventional formulation method, mixing and stirring, treats that it dry, pulverize into the particulate preparation of 0.05mm – 0.8mm.It is high that the present invention has sealing ratiod, suspension property is good, there is after condensation very high setting strength, enter leakage channel deep, in the crack of difference leakage type, bearing capacity according to the leakage degree of depth, lithology, intensity adjustment, after pressurization sealing liquid solidifies, can have very high condensation performance and pressure-bearing effect.Extensively apply in oil, geological drilling technique, special adaptation, is applied in Fractured hard formation and Caves stratum.

Description

The agent of leak stopping pressure-bearing
Technical field
The present invention relates to drilling plugging agent material, particularly a kind of leak stopping pressure-bearing agent.
Background technology
The leak stopping slurry adopted in petroleum drilling, be generally the nut-shell of different-grain diameter, cotton seed hull, single material such as envelope, diesel oil bentonite slurry, mica, husk, at the scene as the agent of leak stopping pressure-bearing, realize the construction of pressurization sealing, these plugging agents are that petroleum drilling stoppage engineering aspect has played effect.But it also exists following shortcoming or deficiency simultaneously: 1. above-mentioned plugging agent only small-sized leakage and bearing requirements not high time play a role, still do not reach the requirement of pressure-bearing, leak stopping is repeatedly caused on the stratum that the large bearing requirements in, crack large to hole is higher; What 2. plugging agent particle diameter was large enters less than in crack, and what particle diameter was little is detained incessantly in leakage channel; 3. pressure-bearing agent dose hour, can not be detained, frame does not play bridge, holds incessantly pressure, when dosage is large, poor fluidity, Portability is bad, and easily sealing is difficult to pump into, and easily causes high pump pressure, is destroyed further by drop ply again and form new crack during pump pressure height; 4. pressurization sealing slurry enter leakage stratum after because of performance of not condensing, turn on pump circulating pressure excitement time can miss again, do not reach the object of pressure-bearing; 5. bad with formation rock adsorptivity, there is no cementation and cementation, cause a large amount of pressure-bearing material to return out well head, cause a large amount of wastes; 6. pressure-bearing material usage is large, and pressure-bearing repeatedly, the pressure-bearing time is long, pressure-bearing weak effect, causes down-hole situation complicated, does not finally reach pressure-bearing object.
Summary of the invention
The object of this invention is to provide the agent of a kind of leak stopping pressure-bearing, adopt inorganic, organic multiple pressure-bearing material, through different compatibility, make pressure-bearing agent, its sealing ratiod is high, and suspending, it is good to carry performance, can enter leakage channel deep, pressure-bearing shut-off capacity is high, engineering time is short, and pump pressure is low, avoids causing secondary injury to leakage stratum, bearing capacity can be missed in the crack of type in difference and be adjusted according to the leakage degree of depth, lithology, intensity, has very high ultimate compression strength and pressure-bearing effect.Effectively overcome or avoid the shortcoming that exists in above-mentioned prior art or deficiency.
Leak stopping pressure-bearing of the present invention agent, its composition and content, content is weight part: calcium carbonate 20-30; Perlite powder 10-15; G level oil well cement 2-5; Quartz sand 10-15; Calucium Silicate powder 10-20; Oyster shell whiting 10-15; Calcium hydroxide 1-4; Drilling fluid xanthan gum 0.1-0.4; Polyacrylamide 0.1-0.4; Polyanionic Cellulose 0.1-0.4.
Compound method: by above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
The present invention compared with prior art tool has the following advantages or beneficial effect:
1, bearing capacity is strong, and existing physical clogging performance, has again chemical coagulation effect;
2, good fluidity, suspension carrying capacity is strong, and can enter deep, low-pressure stratum crack, plugging effect is good;
3, with formation lithology excellent adsorption, connect, cementation characteristic is good, and there is performance of well condensing, low pressure ravelly ground bearing capacity can be improved;
4, performance is even, easily pumps into open-ended, the secondary crack that the formation damage that high pump pressure can not be caused to cause is formed, and pressurization sealing success ratio is high;
5, technique is simple, and the shove time is short, and rate of set is fast, and sealing ratiod is high, pressurization sealing Be very effective, significantly shortens the pressurization sealing cycle;
6, compatibility is good, can with other multiple leak stopping starch with the use of, matched performance is good, has good compatibility performance;
7, use range is wide, pressure-bearing can construct, all have good pressurization sealing effect in dissimilar formation lithology well section;
8, little to environmental influence, nontoxic, pollution-free, easy and safe to operate.
Embodiment:
The agent of a kind of leak stopping pressure-bearing, its composition and content, content is weight part: calcium carbonate 20-30; Perlite powder 10-15; G level oil well cement 2-5; Quartz sand 10-15; Calucium Silicate powder 10-20; Oyster shell whiting 10-15; Calcium hydroxide 1-4; Drilling fluid xanthan gum 0.1-0.4; Polyacrylamide 0.1-0.4; Polyanionic Cellulose 0.1-0.4.
Compound method: by above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
During use, in plugging drilling fluid, add the 2%-15% leak stopping pressure-bearing of the present invention agent of plugging drilling fluid total amount.
Provide specific embodiment below:
1st example
Calcium carbonate 20; Perlite powder 10; G level oil well cement 2; Quartz sand 10; Calucium Silicate powder 10; Oyster shell whiting 10; Calcium hydroxide 1; Drilling fluid xanthan gum 0.1; Polyacrylamide 0.1; Polyanionic Cellulose 0.1; By above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
During use, in plugging drilling fluid, add the leak stopping pressure-bearing of the present invention agent of plugging drilling fluid total amount 2%.
2nd example
Calcium carbonate 23; Perlite powder 12; G level oil well cement 3; Quartz sand 12; Calucium Silicate powder 13; Oyster shell whiting 13; Calcium hydroxide 2; Drilling fluid xanthan gum 0.2; Polyacrylamide 0.2; Polyanionic Cellulose 0.2; By above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.During use, in plugging drilling fluid, add the leak stopping pressure-bearing of the present invention agent of plugging drilling fluid total amount 8%.
3rd example
Calcium carbonate 30; Perlite powder 15; G level oil well cement 5; Quartz sand 15; Calucium Silicate powder 20; Oyster shell whiting 15; Calcium hydroxide 4; Drilling fluid xanthan gum 0.4; Polyacrylamide 0.4; Polyanionic Cellulose 0.4; By above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
During use, in plugging drilling fluid, add the leak stopping pressure-bearing of the present invention agent of plugging drilling fluid total amount 15%.
4th example
Calcium carbonate 27; Perlite powder 13; G level oil well cement 4; Quartz sand 14; Calucium Silicate powder 17; Oyster shell whiting 14; Calcium hydroxide 3; Drilling fluid xanthan gum 0.3; Polyacrylamide 0.3; Polyanionic Cellulose 0.3; By above-mentioned substance by its component and content, under normal temperature and pressure, add in molten device successively with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
During use, in plugging drilling fluid, add the leak stopping pressure-bearing of the present invention agent of plugging drilling fluid total amount 12%.
1st example, the 2nd example, the 3rd example are embodiment, and the 4th example is comparative example, has good plugging effect in using at the scene.

Claims (1)

1. a pressure-bearing agent, its composition and content, content is weight part:
Calcium carbonate 20-30;
Perlite powder 10-15;
G level oil well cement 2-5;
Quartz sand 10-15;
Calucium Silicate powder 10-20;
Oyster shell whiting 10-15;
Calcium hydroxide 1-4;
Drilling fluid xanthan gum 0.1-0.4;
Polyacrylamide 0.1-0.4;
Polyanionic Cellulose 0.1-0.4;
Compound method: by above-mentioned substance by its component and content, under normal temperature and pressure, add successively in container with conventional formulation method, mixing and stirring, treat that it dry, pulverize or be screened into the powdered preparations that particle diameter is 0.05mm – 0.8mm.
CN201310748479.2A 2013-12-31 2013-12-31 The agent of leak stopping pressure-bearing Active CN103740341B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310748479.2A CN103740341B (en) 2013-12-31 2013-12-31 The agent of leak stopping pressure-bearing

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Application Number Priority Date Filing Date Title
CN201310748479.2A CN103740341B (en) 2013-12-31 2013-12-31 The agent of leak stopping pressure-bearing

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CN103740341A CN103740341A (en) 2014-04-23
CN103740341B true CN103740341B (en) 2016-01-13

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108690581A (en) * 2017-04-06 2018-10-23 中国石油化工股份有限公司 A kind of high-efficiency water-base drilling fluid sealing agent

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CN104312559A (en) * 2014-11-14 2015-01-28 天津大港油田滨港集团博弘石油化工有限公司 Silicate plugging agent for water plugging in oilfields
CN104987856B (en) * 2015-07-31 2018-07-13 山东盛海科贸有限公司 Offshore drilling fluid pressurization sealing agent and its application process
CN106566501B (en) * 2016-08-18 2020-09-15 盘锦鸿鼎油气技术服务有限公司 Flexible plugging agent and preparation method and application thereof
CN106336861A (en) * 2016-08-30 2017-01-18 董晓 Preparation method of novel plugging agent
CN106497526A (en) * 2016-09-27 2017-03-15 任丘市力科节能材料有限公司 A kind of plugging while drilling pressure-bearing retaining wall agent and preparation method thereof of drilling fluid
CN106675538A (en) * 2016-12-22 2017-05-17 上海三瑞高分子材料股份有限公司 Plugging-type shield mud
CN107880862B (en) * 2017-11-07 2018-08-10 西南石油大学 A kind of sealing agent and preparation method thereof improving bearing capacity
MY197237A (en) 2019-02-01 2023-06-07 Halliburton Energy Services Inc Compatible low crystalline silica spacers
US11760913B2 (en) 2019-06-14 2023-09-19 King Fahd University Of Petroleum And Minerals Perlite containing drilling fluids and uses thereof
CN110938413A (en) * 2019-09-26 2020-03-31 霍尔果斯弗莱瑟逆向石油科技有限公司 Reverse plugging material for stratum
CN110903815A (en) * 2019-12-20 2020-03-24 东营泰尔石油技术有限公司 High-strength leakage-stopping slurry
CN110951471A (en) * 2019-12-20 2020-04-03 山东华越天成石油技术有限责任公司 Coagulation plugging slurry
CN111040748B (en) * 2019-12-20 2022-05-17 东营泰尔石油技术有限公司 Low-density high-bridge plug plugging slurry
CN110734748A (en) * 2019-12-20 2020-01-31 山东华越天成石油技术有限责任公司 leak-proof plugging filling agent
CN111607366B (en) * 2020-06-09 2021-05-04 山东科兴化工有限责任公司 Plugging agent for drilling fluid and preparation method thereof

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