CN103756453A - Water soluble damping antirust coating and preparation method thereof - Google Patents
Water soluble damping antirust coating and preparation method thereof Download PDFInfo
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- CN103756453A CN103756453A CN201310732264.1A CN201310732264A CN103756453A CN 103756453 A CN103756453 A CN 103756453A CN 201310732264 A CN201310732264 A CN 201310732264A CN 103756453 A CN103756453 A CN 103756453A
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Abstract
The invention relates to a water soluble damping antirust coating and a preparation method thereof. The coating comprises the following raw materials in parts by weight: 20-30 parts of styrene-acrylic ester, 10-15 parts of vinyl acetate-butyl acrylate, 2-4 parts of tributyl phosphate, 6-10 parts of polyvinyl alcohol, 0.5-2 parts of polyaspartic acid, 3-5 parts of lignosulfonate, 0.5-3 parts of nanometer titania, 0.2-0.6 parts of nanometer ceria, 50-70 parts of bentonite, 0.4-1 part of dispersant, 0.5-1.5 parts of thickener and 40-50 parts of water. The water soluble damping antirust coating disclosed by the invention is simple in preparation method, and the prepared waterborne damping antirust coating is good in damping and noise-reduction performances, and strong in adhesive force on a substrate, not only can protect the substrate and play an antirust role, but also has good bactericidal performance, and meanwhile, the water soluble damping antirust coating disclosed by the invention takes water as a solvent, so that pollution to the environment caused by a solvent coating is overcome, and the water soluble damping antirust coating is a green and environmental coating.
Description
Technical field
The invention belongs to technical field of coatings, be specifically related to a kind of aqueous damping rust proof paint and preparation method thereof.
Background technology
Damping paint by macromolecule resin add appropriate filler and subsidiary material formulated, that one can be coated on various metal plate-like structure surface, there is the speciality coating of vibration damping, thermal insulation and certain sealing property, can be widely used in the vibration damping of aircraft, boats and ships, vehicle and various machineries.Because coating can be painted on body structure surface, thus easy construction, especially to baroque surface as naval vessels, aircraft etc., more embody its superiority.
Current damping paint adopts organic solvent mostly, after these paint spay-coatings, can discharge a large amount of VOC gas, and not only the healthy of end user arrived in serious harm, also can pollute atmosphere, damages ecotope.Meanwhile, the damping paint function on market is comparatively single, does not have antibacterial and antirust function, and therefore how overcoming the deficiencies in the prior art is problems that current technical field of coatings is needed solution badly.
Summary of the invention
The object of the invention is in order to solve the deficiencies in the prior art, a kind of aqueous damping rust proof paint and preparation method thereof is provided, the method is simple, and the aqueous damping rust proof paint making has damping noise reduction, antibacterial and antirust effect, is a kind of environmental type coating.
The technical solution used in the present invention is as follows:
A kind of aqueous damping rust proof paint, comprises the following raw material according to parts by weight meter: 20 ~ 30 parts of cinnamic acrylic ester emulsions, 10 ~ 15 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 2 ~ 4 parts of tributyl phosphates, 6 ~ 10 parts of polyvinyl alcohol, 0.5 ~ 2 part of poly aspartic acid, 3 ~ 5 parts of sulfonated lignin, 0.5 ~ 3 part of nano titanium oxide, 0.2 ~ 0.6 part of nano ceric oxide, 50 ~ 70 parts of wilkinites, 0.4 ~ 1 part of dispersion agent, 0.5 ~ 1.5 part of thickening material, 40 ~ 50 parts, water.
Further preferably described dispersion agent is dioctyl phthalate (DOP) or Sodium hexametaphosphate 99.
Further preferably described thickening material is Xylo-Mucine.
The preparation method of above-mentioned aqueous damping rust proof paint, comprises the steps:
Step (1): cinnamic acrylic ester emulsion, vinyl acetate between to for plastic-polybutylacrylate latex, tributyl phosphate, polyvinyl alcohol, poly aspartic acid, sulfonated lignin, nano titanium oxide, nano ceric oxide and dispersion agent are added to the water and are stirred at normal temperatures, obtain slurries;
Step (2): wilkinite is ground to form to fine powder, and granularity is 150 ~ 200 orders;
Step (3): the wilkinite fine powder that step (2) is obtained joins in the slurries that step (1) obtains, and adds thickening material simultaneously, is stirred to and mixes, and obtains aqueous damping rust proof paint of the present invention.
compared with prior art, its beneficial effect is in the present invention:(1) product damping noise reduction performance of the present invention is good, to the strong adhesion of base material, not only can protect base material, plays antirust effect, also has good bactericidal properties; (2) product of the present invention, take water as solvent, has overcome the pollution of solvent based coating to environment; (3) preparation method of the present invention is simple, is easy to promote.
Specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
A kind of aqueous damping rust proof paint, comprises the following raw material according to parts by weight meter: 20 parts of cinnamic acrylic ester emulsions, 10 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 2 parts of tributyl phosphates, 6 parts of polyvinyl alcohol, 0.5 part of poly aspartic acid, 3 parts of sulfonated lignin, 0.5 part of nano titanium oxide, 0.2 part of nano ceric oxide, 50 parts of wilkinites, 0.4 part of dioctyl phthalate (DOP), 0.5 part of Xylo-Mucine, 400 parts, water.
The preparation method of the aqueous damping rust proof paint of the present embodiment, comprises the steps:
Step (1): cinnamic acrylic ester emulsion, vinyl acetate between to for plastic-polybutylacrylate latex, tributyl phosphate, polyvinyl alcohol, poly aspartic acid, sulfonated lignin, nano titanium oxide, nano ceric oxide and dioctyl phthalate (DOP) are added to the water and are stirred at normal temperatures, obtain slurries;
Step (2): wilkinite is ground to form to fine powder, and granularity is 150 ~ 200 orders;
Step (3): the wilkinite fine powder that step (2) is obtained joins in the slurries that step (1) obtains, and adds Xylo-Mucine simultaneously, is stirred to and mixes, and obtains the aqueous damping rust proof paint of the present embodiment.
Embodiment 2
A kind of aqueous damping rust proof paint, comprises the following raw material according to parts by weight meter: 30 parts of cinnamic acrylic ester emulsions, 15 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 4 parts of tributyl phosphates, 10 parts of polyvinyl alcohol, 2 parts of poly aspartic acids, 5 parts of sulfonated lignin, 3 parts of nano titanium oxides, 0.6 part of nano ceric oxide, 70 parts of wilkinites, 1 part of dioctyl phthalate (DOP), 1.5 parts of Xylo-Mucines, 50 parts, water.
The preparation method of the aqueous damping rust proof paint of the present embodiment is identical with embodiment 1.
Embodiment 3
A kind of aqueous damping rust proof paint, comprises the following raw material according to parts by weight meter: 22 parts of cinnamic acrylic ester emulsions, 12 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 3 parts of tributyl phosphates, 7 parts of polyvinyl alcohol, 1 part of poly aspartic acid, 4 parts of sulfonated lignin, 1 part of nano titanium oxide, 0.5 part of nano ceric oxide, 58 parts of wilkinites, 0.9 part of dioctyl phthalate (DOP), 1 part of Xylo-Mucine, 44 parts, water.
The preparation method of the aqueous damping rust proof paint of the present embodiment is identical with embodiment 1.
Embodiment 4
A kind of aqueous damping rust proof paint, comprises the following raw material according to parts by weight meter: 27 parts of cinnamic acrylic ester emulsions, 13 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 3.5 parts of tributyl phosphates, 9 parts of polyvinyl alcohol, 1.5 parts of poly aspartic acids, 4.5 parts of sulfonated lignin, 2 parts of nano titanium oxides, 0.4 part of nano ceric oxide, 64 parts of wilkinites, 0.7 part of Sodium hexametaphosphate 99,0.8 part of Xylo-Mucine, 48 parts, water.
The preparation method of the aqueous damping rust proof paint of the present embodiment, comprises the steps:
Step (1): cinnamic acrylic ester emulsion, vinyl acetate between to for plastic-polybutylacrylate latex, tributyl phosphate, polyvinyl alcohol, poly aspartic acid, sulfonated lignin, nano titanium oxide, nano ceric oxide and Sodium hexametaphosphate 99 are added to the water and are stirred at normal temperatures, obtain slurries;
Step (2): wilkinite is ground to form to fine powder, and granularity is 150 ~ 200 orders;
Step (3): the wilkinite fine powder that step (2) is obtained joins in the slurries that step (1) obtains, and adds Xylo-Mucine simultaneously, is stirred to and mixes, and obtains the aqueous damping rust proof paint of the present embodiment.
performance test
Performance to the embodiment of the present invention 1 ~ 4 product is tested, and test result is in Table 1, and wherein damping test detects according to GB/T 16406-1996.
The performance test data of table 1 embodiment 1 ~ 4 product
Meanwhile, the anti-microbial property that this has been implemented to 1 ~ 4 product is tested, and its data results is as shown in table 2.
The antibacterial effect of table 2 embodiment of the present invention 1 ~ 4 product detects data
Claims (4)
1. an aqueous damping rust proof paint, is characterized in that comprising the following raw material according to parts by weight meter: 20 ~ 30 parts of cinnamic acrylic ester emulsions, 10 ~ 15 parts of vinyl acetate between to for plastic-polybutylacrylate latexes, 2 ~ 4 parts of tributyl phosphates, 6 ~ 10 parts of polyvinyl alcohol, 0.5 ~ 2 part of poly aspartic acid, 3 ~ 5 parts of sulfonated lignin, 0.5 ~ 3 part of nano titanium oxide, 0.2 ~ 0.6 part of nano ceric oxide, 50 ~ 70 parts of wilkinites, 0.4 ~ 1 part of dispersion agent, 0.5 ~ 1.5 part of thickening material, 40 ~ 50 parts, water.
2. aqueous damping rust proof paint according to claim 1, is characterized in that described dispersion agent is dioctyl phthalate (DOP) or Sodium hexametaphosphate 99.
3. aqueous damping rust proof paint according to claim 1, is characterized in that described thickening material is Xylo-Mucine.
4. the preparation method of aqueous damping rust proof paint claimed in claim 1, is characterized in that comprising the steps:
Step (1): cinnamic acrylic ester emulsion, vinyl acetate between to for plastic-polybutylacrylate latex, tributyl phosphate, polyvinyl alcohol, poly aspartic acid, sulfonated lignin, nano titanium oxide, nano ceric oxide and dispersion agent are added to the water and are stirred at normal temperatures, obtain slurries;
Step (2): wilkinite is ground to form to fine powder, and granularity is 150 ~ 200 orders;
Step (3): the wilkinite fine powder that step (2) is obtained joins in the slurries that step (1) obtains, and adds thickening material simultaneously, is stirred to and mixes, and obtains aqueous damping rust proof paint of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201310732264.1A CN103756453A (en) | 2013-12-27 | 2013-12-27 | Water soluble damping antirust coating and preparation method thereof |
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| CN201310732264.1A CN103756453A (en) | 2013-12-27 | 2013-12-27 | Water soluble damping antirust coating and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104513578A (en) * | 2014-11-28 | 2015-04-15 | 蚌埠南自仪表有限公司 | Lasting antifouling antirusting paint and preparation method thereof |
| CN105419544A (en) * | 2015-12-31 | 2016-03-23 | 优链新材料科技（上海）有限公司 | Water-based damping coating and preparation method thereof |
| JP2016069574A (en) * | 2014-09-30 | 2016-05-09 | 株式会社日本触媒 | Resin composition for vibration control |
| CN105885603A (en) * | 2016-06-12 | 2016-08-24 | 铜陵青铜时代雕塑有限公司 | Coating for polyaspartic acid-glycidyl methacrylate composite urban cast copper sculpture and preparation method of coating |
| CN106281030A (en) * | 2016-08-08 | 2017-01-04 | 凡音环保科技（苏州）有限公司 | A kind of environment-friendly type multiple-effect high-molecular damping material |
| CN106349780A (en) * | 2016-08-30 | 2017-01-25 | 无锡益联机械有限公司 | Rust prevention painting for bead ring and preparing method thereof |
| JP2017179144A (en) * | 2016-03-30 | 2017-10-05 | 株式会社日本触媒 | Resin composition for heating and drying |
| CN107384094A (en) * | 2017-08-03 | 2017-11-24 | 合肥泓定科技有限公司 | Aqueous damping coating and preparation method thereof |
| CN108822661A (en) * | 2018-05-29 | 2018-11-16 | 芜湖市元奎新材料科技有限公司 | Waterborne flame retardant damping paint |
| CN111534170A (en) * | 2019-12-30 | 2020-08-14 | 阜阳师范大学 | CeO2Application in water-based acrylic paint |
| CN114395300A (en) * | 2022-02-28 | 2022-04-26 | 扬州一诺新材料有限公司 | Water-based noise reduction coating for aluminum plate and preparation method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016069574A (en) * | 2014-09-30 | 2016-05-09 | 株式会社日本触媒 | Resin composition for vibration control |
| US11053408B2 (en) | 2014-09-30 | 2021-07-06 | Nippon Shokubai Co., Ltd. | Resin composition for damping material |
| EP3202854A4 (en) * | 2014-09-30 | 2018-06-06 | Nippon Shokubai Co., Ltd. | Resin composition for damping material |
| CN104513578A (en) * | 2014-11-28 | 2015-04-15 | 蚌埠南自仪表有限公司 | Lasting antifouling antirusting paint and preparation method thereof |
| CN105419544A (en) * | 2015-12-31 | 2016-03-23 | 优链新材料科技（上海）有限公司 | Water-based damping coating and preparation method thereof |
| CN105419544B (en) * | 2015-12-31 | 2018-06-26 | 优链新材料科技（上海）有限公司 | A kind of aqueous damping coating and preparation method thereof |
| JP2017179144A (en) * | 2016-03-30 | 2017-10-05 | 株式会社日本触媒 | Resin composition for heating and drying |
| CN105885603A (en) * | 2016-06-12 | 2016-08-24 | 铜陵青铜时代雕塑有限公司 | Coating for polyaspartic acid-glycidyl methacrylate composite urban cast copper sculpture and preparation method of coating |
| CN106281030A (en) * | 2016-08-08 | 2017-01-04 | 凡音环保科技（苏州）有限公司 | A kind of environment-friendly type multiple-effect high-molecular damping material |
| CN106349780A (en) * | 2016-08-30 | 2017-01-25 | 无锡益联机械有限公司 | Rust prevention painting for bead ring and preparing method thereof |
| CN107384094A (en) * | 2017-08-03 | 2017-11-24 | 合肥泓定科技有限公司 | Aqueous damping coating and preparation method thereof |
| CN108822661A (en) * | 2018-05-29 | 2018-11-16 | 芜湖市元奎新材料科技有限公司 | Waterborne flame retardant damping paint |
| CN111534170A (en) * | 2019-12-30 | 2020-08-14 | 阜阳师范大学 | CeO2Application in water-based acrylic paint |
| CN114395300A (en) * | 2022-02-28 | 2022-04-26 | 扬州一诺新材料有限公司 | Water-based noise reduction coating for aluminum plate and preparation method thereof |
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Application publication date: 20140430 |