CN103724133B - A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer - Google Patents
A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer Download PDFInfo
- Publication number
- CN103724133B CN103724133B CN201310742817.1A CN201310742817A CN103724133B CN 103724133 B CN103724133 B CN 103724133B CN 201310742817 A CN201310742817 A CN 201310742817A CN 103724133 B CN103724133 B CN 103724133B
- Authority
- CN
- China
- Prior art keywords
- sugar refinery
- waste liquid
- phosphate fertilizer
- alcohol waste
- concentrated solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 91
- 239000007788 liquid Substances 0.000 title claims abstract description 89
- 239000002699 waste material Substances 0.000 title claims abstract description 89
- 239000002686 phosphate fertilizer Substances 0.000 title claims abstract description 78
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 238000013270 controlled release Methods 0.000 title claims abstract description 40
- 239000004021 humic acid Substances 0.000 title claims abstract description 40
- 230000001934 delay Effects 0.000 title claims abstract description 31
- 239000000470 constituent Substances 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims description 55
- 239000005760 Difenoconazole Substances 0.000 claims description 28
- BQYJATMQXGBDHF-UHFFFAOYSA-N difenoconazole Chemical group O1C(C)COC1(C=1C(=CC(OC=2C=CC(Cl)=CC=2)=CC=1)Cl)CN1N=CN=C1 BQYJATMQXGBDHF-UHFFFAOYSA-N 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 23
- 238000002360 preparation method Methods 0.000 claims description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 20
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical group O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 19
- 229930006000 Sucrose Natural products 0.000 claims description 19
- 229960004793 sucrose Drugs 0.000 claims description 19
- 238000012216 screening Methods 0.000 claims description 18
- 239000011247 coating layer Substances 0.000 claims description 16
- 238000005469 granulation Methods 0.000 claims description 15
- 230000003179 granulation Effects 0.000 claims description 15
- 235000019691 monocalcium phosphate Nutrition 0.000 claims description 15
- CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 claims description 13
- 239000001506 calcium phosphate Substances 0.000 claims description 13
- 229910000150 monocalcium phosphate Inorganic materials 0.000 claims description 13
- 229940045641 monobasic sodium phosphate Drugs 0.000 claims description 12
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000004563 wettable powder Substances 0.000 claims description 12
- 229920000742 Cotton Polymers 0.000 claims description 11
- 229910021529 ammonia Inorganic materials 0.000 claims description 10
- 239000006200 vaporizer Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000009477 fluid bed granulation Methods 0.000 claims description 5
- 210000003608 fece Anatomy 0.000 claims description 4
- 239000010871 livestock manure Substances 0.000 claims description 4
- 239000004557 technical material Substances 0.000 claims description 4
- UUVBYOGFRMMMQL-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca].OP(O)(O)=O UUVBYOGFRMMMQL-UHFFFAOYSA-N 0.000 claims description 3
- 239000003595 mist Substances 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical group [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims 1
- 239000002910 solid waste Substances 0.000 abstract description 7
- 239000000047 product Substances 0.000 description 20
- 239000003337 fertilizer Substances 0.000 description 16
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 12
- 241000219146 Gossypium Species 0.000 description 10
- 241000196324 Embryophyta Species 0.000 description 7
- 125000003636 chemical group Chemical group 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 239000010410 layer Substances 0.000 description 7
- 235000013339 cereals Nutrition 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 239000002253 acid Substances 0.000 description 4
- 230000000855 fungicidal effect Effects 0.000 description 4
- 239000000417 fungicide Substances 0.000 description 4
- 230000012010 growth Effects 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229940062672 calcium dihydrogen phosphate Drugs 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003630 growth substance Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000013379 molasses Nutrition 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- MTXSIJUGVMTTMU-JTQLQIEISA-N (S)-anabasine Chemical compound N1CCCC[C@H]1C1=CC=CN=C1 MTXSIJUGVMTTMU-JTQLQIEISA-N 0.000 description 1
- RMOGWMIKYWRTKW-UONOGXRCSA-N (S,S)-paclobutrazol Chemical compound C([C@@H]([C@@H](O)C(C)(C)C)N1N=CN=C1)C1=CC=C(Cl)C=C1 RMOGWMIKYWRTKW-UONOGXRCSA-N 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000005985 Paclobutrazol Substances 0.000 description 1
- 229930014345 anabasine Natural products 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- YWTYJOPNNQFBPC-UHFFFAOYSA-N imidacloprid Chemical compound [O-][N+](=O)\N=C1/NCCN1CC1=CC=C(Cl)N=C1 YWTYJOPNNQFBPC-UHFFFAOYSA-N 0.000 description 1
- SEOVTRFCIGRIMH-UHFFFAOYSA-N indole-3-acetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CNC2=C1 SEOVTRFCIGRIMH-UHFFFAOYSA-N 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- FFSJPOPLSWBGQY-UHFFFAOYSA-N triazol-4-one Chemical compound O=C1C=NN=N1 FFSJPOPLSWBGQY-UHFFFAOYSA-N 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310742817.1A CN103724133B (en) | 2013-12-30 | 2013-12-30 | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310742817.1A CN103724133B (en) | 2013-12-30 | 2013-12-30 | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103724133A CN103724133A (en) | 2014-04-16 |
CN103724133B true CN103724133B (en) | 2016-01-20 |
Family
ID=50448471
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310742817.1A Active CN103724133B (en) | 2013-12-30 | 2013-12-30 | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103724133B (en) |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3136268B2 (en) * | 1996-06-18 | 2001-02-19 | 電気化学工業株式会社 | Manufacturing method of granular fertilizer |
CN101041600A (en) * | 2007-03-16 | 2007-09-26 | 阴高鹏 | Humic acid composite material and preparation method thereof |
CN102795946A (en) * | 2012-07-27 | 2012-11-28 | 山东农大肥业科技有限公司 | Formulation and preparation method of humic acid sustained release fertilizer for double-activity and double-effect cotton |
CN102850140A (en) * | 2012-09-29 | 2013-01-02 | 广西力源肥业科技农化有限公司 | Anti-blocking compound fertilizer and preparation method thereof |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH06172075A (en) * | 1992-12-02 | 1994-06-21 | Honen Corp | Slow-acting solid fertilizer |
-
2013
- 2013-12-30 CN CN201310742817.1A patent/CN103724133B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3136268B2 (en) * | 1996-06-18 | 2001-02-19 | 電気化学工業株式会社 | Manufacturing method of granular fertilizer |
CN101041600A (en) * | 2007-03-16 | 2007-09-26 | 阴高鹏 | Humic acid composite material and preparation method thereof |
CN102795946A (en) * | 2012-07-27 | 2012-11-28 | 山东农大肥业科技有限公司 | Formulation and preparation method of humic acid sustained release fertilizer for double-activity and double-effect cotton |
CN102850140A (en) * | 2012-09-29 | 2013-01-02 | 广西力源肥业科技农化有限公司 | Anti-blocking compound fertilizer and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
CN103724133A (en) | 2014-04-16 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103664384B (en) | Humid acid type organic water-retaining agent containing wastes in sugar refinery and alcohol plant | |
CN103626593B (en) | Humic acid type organic-inorganic soil conditioner prepared from wastes of sugar mills and alcohol plants | |
CN104823826A (en) | Greenhouse selenium-enriched herba houttuyniae soilless culture method | |
CN103664383B (en) | Humid acid type organic-inorganic water-retaining agent containing wastes in sugar refinery and alcohol plant | |
CN103664420B (en) | Humic acid water-retention sustained and controlled release organic-inorganic fertilizer made from waste of sugar refineries and alcohol plants | |
CN103724134B (en) | A kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste | |
CN103772068B (en) | A kind of Humic acid type organic-inorganic medicine fertilizer composition comprising neires toxin and nicotinic insecticide utilizing sugar refinery, grain distillery's waste | |
CN107586205A (en) | A kind of coated fertilizer for improveing acid soil and preparation method thereof | |
CN103626594B (en) | Humic acid type water-retaining slow-release controlled-release organic fertilizer prepared from wastes of sugar mills and alcohol plants | |
CN106396860A (en) | Agricultural organic fertilizer | |
CN1242962C (en) | Nimbic coating slow release granular fertilizer | |
CN103739385B (en) | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled-release fertilizer | |
CN103724133B (en) | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays controlled release phosphate fertilizer | |
CN104892312A (en) | High-nutrient organic compound fertilizer | |
CN103708965B (en) | A kind of humic acid type sustained/controlled release urea utilizing alcohol waste liquid for sugar refinery | |
CN103724132B (en) | A kind of humic acid type of alcohol waste liquid for sugar refinery that utilizes delays Controlled Release Nitrogen Fertilizer | |
CN109997649B (en) | Rice seedling raising substrate and application thereof | |
CN106588180A (en) | Disease-resistant potato fertilizer | |
CN104860784A (en) | High-nutrition organic compound fertilizer | |
CN105110884A (en) | Organic base fertilizer and preparation method therefor | |
CN103964923A (en) | Method for preparing organic/inorganic controlled-release fertilizer for maize through secondary spraying technology | |
CN105000953B (en) | A kind of organic composite fertilizer suitable for clayed soil | |
CN103964944B (en) | A kind of method utilizing flat mushroom waste-material-preparing seedling raising ground substance | |
CN103420709B (en) | A kind of Natural mineral matter composite fertilizer | |
CN102219592A (en) | Special organic fertilizer for greenhouse vegetables and preparation method thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200117 Address after: 530007, B-2 building, headquarter of China ASEAN enterprise, No. 1, headquarters Road, Nanning hi tech Zone, the Guangxi Zhuang Autonomous Region Patentee after: GUANGXI QINDE TECHNOLOGY CO.,LTD. Address before: 530007, B-2 building, headquarter of China ASEAN enterprise, No. 1, headquarters Road, Nanning hi tech Zone, the Guangxi Zhuang Autonomous Region Patentee before: Ye Changdong |
|
TR01 | Transfer of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Humic Acid Type Slow and Controlled Release Phosphate Fertilizer Utilizing Alcohol Waste Liquid from Sugar Factory Effective date of registration: 20221122 Granted publication date: 20160120 Pledgee: Nanning United Innovation Financing Guarantee Co.,Ltd. Pledgor: GUANGXI QINDE TECHNOLOGY CO.,LTD. Registration number: Y2022450000204 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231109 Granted publication date: 20160120 Pledgee: Nanning United Innovation Financing Guarantee Co.,Ltd. Pledgor: GUANGXI QINDE TECHNOLOGY CO.,LTD. Registration number: Y2022450000204 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A humic acid type slow-release phosphate fertilizer utilizing alcohol waste liquid from a sugar factory Effective date of registration: 20231120 Granted publication date: 20160120 Pledgee: Nanning United Innovation Financing Guarantee Co.,Ltd. Pledgor: GUANGXI QINDE TECHNOLOGY CO.,LTD. Registration number: Y2023450000145 |