CN103706142B - A kind of extraction collection device and application thereof - Google Patents
A kind of extraction collection device and application thereof Download PDFInfo
- Publication number
- CN103706142B CN103706142B CN201210370550.3A CN201210370550A CN103706142B CN 103706142 B CN103706142 B CN 103706142B CN 201210370550 A CN201210370550 A CN 201210370550A CN 103706142 B CN103706142 B CN 103706142B
- Authority
- CN
- China
- Prior art keywords
- extraction
- collection device
- receiver
- outlet
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a kind of extraction collection device, it is specifically related to a kind of volatile ingredient and extracts collection device, including extraction pot (1), extraction pot outlet (2), relief valve (3), pipeline (4), receiver (6), interlayer (11), offgas outlet (7), condensing water inlet (8) and condensation-water drain (5), pumping equipment (9).The invention has the beneficial effects as follows: simple in construction, easy to operate, receiver possesses collection and condensation function, substantially reduces condensed water consumption, improves volatile ingredient collection rate.
Description
Technical field
The invention discloses a kind of extraction collection device, be specifically related to a kind of volatile ingredient and extract collection device and answer
With.
Background technology
Volatile ingredient extracting method has decocting method, steam distillation, CO2 supercritical fluid extraction, organic solvent
Extraction methods etc., wherein the extraction effect of steam distillation is optimal.During hydrodistillation volatile ingredient, because steam carries energy
Height, as condenser can not condense the volatile ingredient distilled out in time, some volatile compounds is discharged with tail gas, causes extracting
Rate is the highest.
Summary of the invention
Instant invention overcomes existing volatile ingredient extraction and separation technology not enough, compact device, by traditional volatile composition
Extraction element, condensing plant, collecting device optimum organization, on the one hand change heat exchange method, by direct with cold by retort gas
The gas-solid heat exchange of solidifying face contact, after becoming retort gas water first and in receiver and subsequent condensation liquid heat exchange, receiver
In water and subsequent condensation liquid contact with cryosurface again, heat exchange method is that gas-liquid-solid heat exchange, beneficially retort gas are cold
Coagulate and collect, improving heat exchanger effectiveness, reducing condensed water consumption.On the other hand solve volatile ingredient condense in time because of end and
Discharge the loss caused with tail gas, improve volatile ingredient and extract yield.
For solve above-mentioned technical problem, the present invention by the following technical solutions:
A kind of extraction collection device, including extraction element, condensate collection device.Extraction element includes extraction pot 1, relief valve
3, the first pipeline 4, condensate collection device include receiver 6, interlayer 11, condensing water inlet 8, condensation-water drain 5, offgas outlet 7,
Pumping equipment 9.
Extraction pot 1 and receiver 6 is connected by the first pipeline 4, and the volatile ingredient distillated with steamed is in receiver 6
Condensation and collection.
At extraction pot 1 top equipped with relief valve 3, when extracting complete, opening the safety-valve 3, gas is discharged by relief valve, anti-
The distillate suck-back only collected in receiver 6 is in extraction pot 1.
The entrance of the first pipeline 4 is connected with extraction pot outlet 2, and the outlet 10 of the first pipeline 4 is passed through the bottom of receiver 6.
The outlet 10 of the first pipeline 4 down, is 0～90 degree of angle with horizontal line, preferably 45～90 degree.
Before extraction, adding a certain amount of water in receiver 6, water level, for exceeding pipe outlet 10 level height 5-10cm, is store
The outer wall of flow container 6 is with leading to the interlayer 11 of condensed water, and condensed water enters from condensing water inlet 8, from condensation-water drain 5.
To better implement the present invention, 2-10 receiver 6 can be through being connected in series 2-10 with second pipe 15, second pipe
The entrance of 15 is connected with the outlet of previous receiver, and the outlet of second pipe 15 is passed through the bottom of Next receiver, successively
It is connected in series.Second pipe 15 each go out mouth down, be 0～90 degree of angle with horizontal line, preferably 45～90 degree angles.Extract
In front each receiver, tank enters suitable quantity of water, exceeds level height 5-10cm of pipe outlet, can reduce volatile ingredient further
Loss, improve extract yield.
It is a further object to provide the extracting method of a kind of volatile ingredient, volatility provided by the present invention
The extracting method of composition, is to utilize device of the present invention to decoct volatile component of plant or steam distillation carries
Take；The method of described decoction or water vapour distillation is addition suitable quantity of water in device receiver of the present invention, and water level is high
Go out pipe outlet 10 level height 5-10cm and open condensed water, carry out decocting or distillation extraction.
The invention has the beneficial effects as follows: simple in construction, easy to operate, receiver possesses condensation and collecting function, significantly subtracts
Few condensed water consumption, improves volatile ingredient collection rate.
Accompanying drawing explanation
Fig. 1 is the structural representation of the embodiment of the present invention one
Fig. 2 is the structural representation of the embodiment of the present invention two
Fig. 3 is the extraction of traditional handicraft, condensation, collection device schematic diagram
Detailed description of the invention
The present invention is further elaborated below in conjunction with the accompanying drawings:
Embodiment one: as it is shown in figure 1,
Fig. 1 show a kind of extraction collection device that the present invention provides, including extraction element, condensate collection device.Extract
Device includes extraction pot 1, relief valve the 3, first pipeline 4, condensate collection device include receiver 6, interlayer 11, condensing water inlet 8,
Condensation-water drain 5, offgas outlet 7, pumping equipment 9.
Extraction pot 1 is connected by the first pipeline 4 with receiver 6, and during extracting, the volatility distillated with steamed becomes
Divide to be entered into by the first pipeline 4 and receiver 6 condenses and collects.
At extraction pot 1 top equipped with relief valve 3, when extracting complete, opening the safety-valve 3, gas is discharged by relief valve, with
Prevent the distillate suck-back collected in receiver 6 in extraction pot 1.
The entrance of the first pipeline 4 is connected with extraction pot outlet 2, and the outlet 10 of the first pipeline 4 is passed through the bottom of receiver 6.
The outlet 10 of the first pipeline 4 down, is 75 degree of angles with horizontal line.
Before extraction, adding a certain amount of water in receiver 6, water level, for exceeding pipe outlet 10 level height 5-10cm, is store
The outer wall of flow container 6 is with leading to the interlayer 11 of condensed water, and condensed water enters from condensing water inlet 8, discharges from condensation-water drain 5.
Embodiment two: as in figure 2 it is shown,
Fig. 2 show a kind of extraction collection device that the present invention provides, including extraction element, condensate collection device.Extract
Device includes extraction pot 1, relief valve the 3, first pipeline 4, second pipe 15, and condensate collection device includes receiver 6, receiver
16, receiver 17, interlayer 11, condensing water inlet 8, condensation-water drain 5, offgas outlet 7, pumping equipment 9, pumping equipment 91, row
Liquid device 92.
Extraction pot 1 is connected by the first pipeline 4 and second pipe 15 with receiver 6, receiver 16 and receiver 17, and first
The entrance of pipeline 4 is connected with extraction pot outlet 2, and the volatile ingredient extracted tank outlet 2 distilled out in extraction pot, through the first pipe
The outlet 10 in road 4 enters receiver 6 and completes condense and collect for the first time, and the volatile ingredient that receiver 6 is collected the most completely is from storage
The outlet 13 of flow container 6, enters receiver 16 through the outlet 101 of second pipe 15 and completes second time and condense and collect, receiver 16
The volatile ingredient collected the most completely from the outlet 14 of receiver 16, enters basin 17 through the outlet 102 of second pipe 15 and completes
Third time condensation and collection, tail gas is from outlet 7 discharge, and when volatile ingredient has extracted, open the safety-valve (3).Before extraction, storage
In flow container 6, receiver 16 and receiver 17, tank enters a certain amount of water 12, exceeds the outlet 10 of the first pipeline 4, the going out of second pipe 15
Mouthfuls 101, level height 5-10cm of the outlet 102 of second pipe 15, opens condensed water, cold by bottom receiver 17 of condensed water
Solidifying water inlet 8 enters, and through receiver interlayer 11, discharges from condensation-water drain 5.
The outlet 10 of the first pipeline 4, the outlet 101 of second pipe 15, second pipe 15 outlet 102 down, with level
Line is 80 degree of angles.
Embodiment three: collect with the extraction of paeonol in Cortex Moutan and apparatus of the present invention and using method thereof and effect are described
By Cortex Moutan 20.0kg, being placed in the extraction pot 1 extracting collection device described in embodiment 2, receiver 6,16,17 add
Entering suitable quantity of water, water level exceeds pipe outlet 10,101,102 level height 5cm, opens water vapour and condensed water, distillation, extracts,
Collect.Steam pressure 0.10-0.12Mpa, condensate flow is 1.0 ton hour.
Distillation collects distillate 200kg after terminating.
Distillate is placed 4 DEG C of cold rooms and is carried out paeonol crystallization, there are paeonol crystal 0.42kg, calculates paeonol and obtains
Rate, formula is paeonol yield=(paeonol crystal/Cortex Moutan weight) * 100%, extracts Cortex Moutan with device in embodiment 2
Middle paeonol, its yield is 2.10%
Use traditional volatile ingredient to extract collection device and Cortex Moutan is carried out the contrast experiment of steam distillation.
Take Cortex Moutan 20.0kg and put into the extraction pot 1 shown in Fig. 3, open water vapour, the condensed water of open cold condenser 5, steam
Evaporate, extract, collect.Steam pressure 0.10-0.12Mpa, condensate flow is 1.5 ton hour.
Distillation collects distillate 200.0kg after terminating
Distillate is placed 4 DEG C of cold rooms and is carried out paeonol crystallization, there are paeonol crystal 0.35kg, calculates paeonol and obtains
Rate, formula is paeonol yield=(paeonol crystal/Cortex Moutan weight) * 100%, extracts Cortex Moutan with device in embodiment 2
Middle paeonol, its yield is 1.75%.
Claims (7)
1. extract a collection device, including extraction element, condensate collection device；It is characterized in that: described extraction element bag
Including extraction pot (1), relief valve (3), the first pipeline (4), described condensate collection device includes receiver (6), interlayer (11), cold
Solidifying water inlet (8), condensation-water drain (5), offgas outlet (7), pumping equipment (9), extraction pot (1) and receiver (6) are by the
One pipeline (4) connects, and the entrance of the first pipeline (4) is connected with extraction pot outlet (2), and the outlet (10) of the first pipeline (4) is passed through
The bottom of receiver (6).
Extraction collection device the most according to claim 1, it is characterised in that: the outlet (10) of the first pipeline (4) down, with
Horizontal line is 0～90 degree of angle.
Extraction collection device the most according to claim 2, it is characterised in that: the outlet (10) of the first pipeline (4) down, with
Horizontal line is 45～90 degree of angles.
4. according to the arbitrary described extraction collection device of claim 1-3, it is characterised in that: 2-10 receiver (6) can be through the
Two pipelines (15) are connected in series.
Extraction collection device the most according to claim 4, it is characterised in that: second pipe (15) go out mouth down, with water
Horizontal line is 0～90 degree of angle.
Extraction collection device the most according to claim 5, it is characterised in that: second pipe (15) go out mouth down, with water
Horizontal line is 45～90 degree of angles.
7. extract the method collecting volatile ingredient, be to utilize the device described in claim 1-6 any one to plant
Volatile ingredient carries out decocting or water vapour distillation；The method of described decoction or water vapour distillation is right to be wanted
Asking in 1-6 and to add suitable quantity of water in the device receiver described in any one, water level exceeds pipe outlet (10) level height 5-
10cm opens condensed water, carries out decocting or distillation extraction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210370550.3A CN103706142B (en) | 2012-09-29 | 2012-09-29 | A kind of extraction collection device and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210370550.3A CN103706142B (en) | 2012-09-29 | 2012-09-29 | A kind of extraction collection device and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103706142A CN103706142A (en) | 2014-04-09 |
| CN103706142B true CN103706142B (en) | 2016-12-21 |
Family
ID=50399706
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210370550.3A Active CN103706142B (en) | 2012-09-29 | 2012-09-29 | A kind of extraction collection device and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103706142B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108261797A (en) * | 2016-12-31 | 2018-07-10 | 九芝堂股份有限公司 | A kind of distillation automaton and its application |
| CN107625437B (en) * | 2017-11-03 | 2021-03-19 | 珠海格力电器股份有限公司 | Electric cooker and distillation method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4334962A (en) * | 1977-12-28 | 1982-06-15 | Fmc Corporation | Apparatus for stripping immiscible materials |
| US5178734A (en) * | 1990-02-16 | 1993-01-12 | International Water Technologies, Inc. | Water distilling apparatus with vertically stacked components |
| CN2869023Y (en) * | 2005-12-29 | 2007-02-14 | 华南师范大学 | Plant volatile oil extractor |
| CN201692682U (en) * | 2010-06-08 | 2011-01-05 | 湖北中烟工业有限责任公司 | Novel volatile oil extraction equipment |
| CN102512839B (en) * | 2011-12-24 | 2015-06-17 | 吉安市林业科学研究所 | Natural d-borneol extraction equipment |
| CN202892957U (en) * | 2012-09-29 | 2013-04-24 | 九芝堂股份有限公司 | Extraction and collection device |
-
2012
- 2012-09-29 CN CN201210370550.3A patent/CN103706142B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN103706142A (en) | 2014-04-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103923748B (en) | A kind of volatile oil extracts collects separation equipment | |
| CN106010790A (en) | Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil | |
| CN107057857A (en) | Agilawood essential oil equipment and process are extracted in a kind of efficiently distillation | |
| CN103706142B (en) | A kind of extraction collection device and application thereof | |
| CN206127245U (en) | Distillation edulcoration device of raw oil | |
| CN204395516U (en) | The dual extraction element of a kind of Chinese herbal medicine effective ingredients | |
| CN201454122U (en) | Extraction solution concentration device | |
| CN202892957U (en) | Extraction and collection device | |
| CN103007572B (en) | Medicine extraction device and technique thereof | |
| CN204550508U (en) | A kind of volatile oil extractor of ultrasonic assistant | |
| CN106281701A (en) | Essential oil extraction device and plants essential oil extracting method | |
| CN202401042U (en) | Volatile oil extraction equipment | |
| CN206881177U (en) | A kind of modified form ethanol refinery system | |
| CN210251253U (en) | Traditional chinese medicine purification solvent recovery system | |
| CN202671521U (en) | Honeysuckle distillation extraction device | |
| CN205088156U (en) | Can improve natural borneol extraction system who receives yield | |
| CN105237358B (en) | Natural borneol extraction system and method capable of increasing yield | |
| CN205216227U (en) | Alcohol extract collecting system | |
| CN205556137U (en) | Distilled water generater | |
| CN201208517Y (en) | Natural herbals light-oil heavy-oil extraction device | |
| CN103834473A (en) | Taxus chinensis volatile oil extracting device | |
| CN204951680U (en) | Equipment is drawed in processing of blumea balsamifera | |
| CN205683639U (en) | Hot reflux extracting-concentration machine | |
| CN208308821U (en) | A kind of traditional medicine volatile oil condensing unit | |
| CN102586025B (en) | Device for extracting and measuring essential oil of ligusticum chuanxiong and use method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C53 | Correction of patent for invention or patent application | ||
| CB02 | Change of applicant information |
Address after: 410205 Changsha high tech Zone, Tongzi, west slope road, No. 339, No. Applicant after: Jiuzhitang Co., Ltd. Address before: 410008 Hunan province Changsha Kaifu District, Furong Road No. 129 Applicant before: Jiuzhitang Co., Ltd. |
|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |