CN103694875A - Peelable antibacterial protection slurry and preparation method thereof - Google Patents
Peelable antibacterial protection slurry and preparation method thereof Download PDFInfo
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- CN103694875A CN103694875A CN201310654884.8A CN201310654884A CN103694875A CN 103694875 A CN103694875 A CN 103694875A CN 201310654884 A CN201310654884 A CN 201310654884A CN 103694875 A CN103694875 A CN 103694875A
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Abstract
The invention discloses peelable antibacterial protection slurry. The peelable antibacterial protection slurry comprises the following components in parts by weight: 30-100 parts of modified polyurethane emulsion, 0-50 parts of modified acrylate emulsion, 1-9 parts of rheological additives, 0-10 parts of film-forming additives, 0-3 parts of wetting and feeling agent, 0.001-0.5 part of nano-silver powder, 0-30 parts of fast-drying solvent and 5-30 parts of water. The bactericidal effect of the peelable antibacterial protection slurry disclosed by the invention is lasting in comparison with ordinary bactericidal liquid and disinfection water; a coating has a very high strength and can not fall off along with the using time and the increase in number of times; and a nano-sliver bactericidal ingredient can be continuously released, the very high concentration can be always maintained before failure of the product, and the stable bactericidal function can be further provided. Simultaneously, a protection layer has a peelable effect; and when the antibacterial effect of the coating decreases after the coating is used for a period of time, the coating can be conveniently peeled off a protection device, and the new coating can be further applied.
Description
Technical field:
The invention belongs to antibiotic paint field, be specifically related to a kind of peelable antimicrobial protection slurries and preparation method thereof.
Background technology:
At MCO, the public place of high-risk infection: station, hotel, hotel, airport etc., and domestic environment.All kinds of malignant bacterias, comprise multi-drug resistant bacteria and pathogenic bacteria, threaten human health.The use of antibiotic paint, can reduce cross infection probability, and the transmissible disease occurred frequently of burst is played to control effect.
Summary of the invention:
The object of this invention is to provide a kind of can removable peelable antimicrobial protection slurries and preparation method thereof, for various needs, often carry out sterilization and disinfection processing element or position, as: the water tap of Public toilets, hospital, all kinds of handrail, chair handle, bus handrail etc.; On peelable antimicrobial protection slurries spraying or brushing and such device, solidify to form quickly one deck antimicrobial protection layer, coating contains nanometer silver antimicrobial composition; Nanometer silver is by slowly-releasing to protective layer surface, and kill bacteria, stops bacterial reproduction, plays the effect of antibacterial and protective.Protective layer has peelable effect simultaneously, when coating is used for some time antibacterial effect to decline to some extent, can from protective device, tear off easily, then execute the new film of last layer.
Peelable antimicrobial protection slurries of the present invention; it is characterized in that; according to the mass fraction, by following component, formed: 5~30 parts, 30~100 parts of modified polyurethane emulsions, 0~50 part of modified acrylate emulsion, 1~9 part of auxiliary rheological agents, 0~10 part of film coalescence aid, 0~3 part of wetting hand feeling agent, 0.001~0.5 part of nano-silver powder, 0~30 part of quick-drying solvent and water.
Described modified polyurethane emulsion is: a kind of or its mixture in organic silicon modified polyurethane emulsion, organic fluorine modified polyurethane emulsion;
Described modified acrylate emulsion is: a kind of or its mixture in organosilicon-modified acrylate emulsion, organic fluorine modified acrylate emulsion;
Described auxiliary rheological agents is: a kind of or its combination in Li-montmorillonite, hydrophobically modified propylene soda acid, hydrophobically modified ethoxylation urethane, hydrophobically modified polyether glycol, Natvosol, methyl hydroxyethylcellulose, Type 3U, methylhydroxypropylcellulose, methylcellulose gum, xanthan gum, aerosil;
Described film coalescence aid is: a kind of or its combination in Lauryl Alcohol ester, propylene glycol phenylate, dipropylene glycol methyl ether, propandiol butyl ether, dipropylene glycol butyl ether, dipropylene glycol propyl ether, glycol propyl ether, butyl glycol ether, Diethylene Glycol butyl ether, diethylene glycol ether, diethylene glycol dimethyl ether, triethylene glycol butyl ether, tri ethylene glycol ethyl ether, triethylene glycol methyl ether, tripropylene glycol butyl ether, ethylene glycol phenyl ether, diacetone alcohol, dipropylene glycol methyl ether acetic ester, dibutyl phthalate;
Described wetting hand feeling agent is: a kind of or its combination in multi-amino silicone, polysiloxane, polydimethylsiloxane, polyether-modified polydimethylsiloxane, phenmethyl modified dimethyl polysiloxane, polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane, amino modified polydimethylsiloxane, water-soluble silicon wax, alkyl-silicone oil, aminophenyl silicone oil, fluorinated alkyl sulfonate, fluorine carbon wetting agent;
Described quick-drying solvent is: a kind of or its mixture in ethanol, acetone.
The preparation method of peelable antimicrobial protection slurries of the present invention is: by modified polyurethane emulsion, modification acrylate breast, auxiliary rheological agents; film coalescence aid, wetting hand feeling agent mix; dispersed with stirring, obtains polymkeric substance water slurry, is distributed in a small amount of water nanometer silver is ultrasonic; the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry; stir on instillation limit, limit, after having instiled, adds remaining water; continue sealing and stir, obtain thus peelable antimicrobial protection slurries.
Than prior art, beneficial effect of the present invention is as follows:
Peelable antimicrobial protection slurries of the present invention can often carry out on sterilization and disinfection processing element or position by spraying or brush various needs, as all types of plastic, metal, pottery, the surface such as wooden, even if surface tissue is complicated, also can realizes good coating protection effect and film; Under natural condition, automatic air-drying solidifies (or hot blast drying solidifies) in the short period of time; the antimicrobial protection layer that forms one deck densification, coating contains broad-spectrum antimicrobial composition---nanometer silver, and nanometer silver is discharged into protective layer surface; kill rapidly various bacteria, play antibacterial and protective effect.The relatively common disinfecting liquid of sterilization effect of the present invention, sterilized water are lasting; Coating has very high intensity, can not produce and come off with the increase of duration of service and number of times; And constantly discharge bactericidal nano-silver composition, and before product failure, can maintain effective concentration always, stable sterilizing function is provided.Protective layer has peelable effect simultaneously, when coating is used for some time antibacterial effect to decline to some extent, can from protective device, tear off easily, then execute the coating that last layer is new.
Embodiment
Following examples are to further illustrate of the present invention, rather than limitation of the present invention, and the simple modifications that essence according to the present invention is carried out the present invention all belongs to the scope of protection of present invention.
Embodiment 1.
Peelable antimicrobial protection slurries, described peelable antimicrobial protection slurries are comprised of according to parts by weight following component: 7 parts, 100 parts of organic silicon modified polyurethane emulsions, 4 parts of hydrophobically modified polyether glycols, 1 part of Type 3U, 2 parts of Lauryl Alcohol esters, 0.5 part of propandiol butyl ether, 0.7 part of polyether-modified polydimethylsiloxane, 0.05 part of fluorine carbon wetting agent, 0.005 part of nano-silver powder, 10 parts of ethanol and water.
By organic silicon modified polyurethane emulsion, hydrophobically modified polyether glycol, Type 3U, Lauryl Alcohol ester, propandiol butyl ether, polyether-modified polydimethylsiloxane, ethanol and fluorine carbon wetting agent component are mixed, with 1000r/min sealing, disperse to stir 30 minutes above to mixing, obtain polymkeric substance water slurry, be distributed in a small amount of water nanometer silver is ultrasonic, the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry, stir on instillation limit, limit, after having instiled, add remaining water, continuing sealing stirs more than 1.5 hours, obtain thus peelable antimicrobial protection slurries.
Peelable antimicrobial protection slurries are coated in to sample surfaces formation and film, then to filming, with reference to following standard, test.
With reference to GB/T21866-2008 method, the anti-microbial property of filming is tested;
With reference to ASTMD-3330, the sticking power of filming at SUS304 stainless steel surface is detected;
With reference to ASTMD3759, film tensile strength and elongation are detected.Its result is as shown in the table.
Project | Antibacterium performance | Antibacterium endurance quality | Sticking power | Tensile strength | Elongation | Peel off effect |
Numerical value | 99.47% | 93.03% | 0.57N/25mm | 11.9Mpa | 262% | Well |
Embodiment 2.
Peelable antimicrobial protection slurries, described peelable its raw material of antimicrobial protection slurries is comprised of according to parts by weight following component: 15 parts, 50 parts of organic silicon modified polyurethane emulsions, 10 parts of organosilicon-modified acrylate emulsions, 4 parts of hydrophobically modified polyether glycols, 0.5 part of aerosil, 1.5 parts of Lauryl Alcohol esters, 0.5 part of diacetone alcohol, 0.6 part of polydimethylsiloxane, 0.05 part of fluorine carbon wetting agent, 0.001 part of nano-silver powder, 5 parts of ethanol and water
By organic silicon modified polyurethane emulsion, organosilicon-modified acrylate emulsion, hydrophobically modified polyether glycol, aerosil, Lauryl Alcohol ester, diacetone alcohol, polydimethylsiloxane, ethanol and fluorine carbon wetting agent component are mixed, with 1000r/min sealing, disperse to stir 30 minutes above to mixing, obtain polymkeric substance water slurry, be distributed in a small amount of water nanometer silver is ultrasonic, the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry, stir on instillation limit, limit, after having instiled, add remaining water, continuing sealing stirs more than 1.5 hours, obtain thus peelable antimicrobial protection slurries.
Peelable antimicrobial protection slurries are coated in to sample surfaces formation and film, then to filming, with reference to following standard, test.
With reference to GB/T21866-2008 method, anti-microbial property is tested;
With reference to ASTMD-3330, to rete, the sticking power at SUS304 stainless steel surface detects;
With reference to ASTMD3759, film stretching intensity and elongation are detected.Its result is as shown in the table.
Embodiment 3.
Peelable antimicrobial protection slurries, described peelable its raw material of antimicrobial protection slurries is comprised of according to parts by weight following component: 5 parts, 30 parts of organic silicon modified polyurethane emulsions, 50 parts of organic fluorine modified polyurethane emulsions, 3 parts of hydrophobically modified ethoxylation urethane, 1 part of aerosil, 4 parts of Lauryl Alcohol esters, 0.02 part of polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane, 0.3 part of nano-silver powder and water.
By organic silicon modified polyurethane emulsion, organic fluorine modified polyurethane emulsion, hydrophobically modified ethoxylation urethane, aerosil, Lauryl Alcohol ester and polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane component are mixed, with 1000r/min sealing, disperse to stir 30 minutes above to mixing, obtain polymkeric substance water slurry, be distributed in a small amount of water nanometer silver is ultrasonic, the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry, stir on instillation limit, limit, after having instiled, add remaining water, continuing sealing stirs more than 1.5 hours, obtain thus peelable antimicrobial protection slurries.
Peelable antimicrobial protection slurries are coated in to sample surfaces formation and film, then to filming, with reference to following standard, test.
With reference to GB/T21866-2008 method, anti-microbial property is tested;
With reference to ASTMD-3330, to rete, the sticking power at SUS304 stainless steel surface detects;
With reference to ASTMD3759, film stretching intensity and elongation are detected.Its result is as shown in the table.
Embodiment 4.
A kind of peelable antimicrobial protection slurries; described peelable its raw material of antimicrobial protection slurries is comprised of according to parts by weight following component: 100 parts of organic silicon modified polyurethane emulsions, 8 parts of hydrophobically modified propylene soda acids; 1 part of hydrophobic type aerosil, 30 parts, 0.03 part of polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane, 0.01 part of nano-silver powder and water.
By organic silicon modified polyurethane emulsion, hydrophobically modified acrylate; hydrophobic type aerosil and polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane component are mixed; with 1000r/min sealing, disperse to stir 30 minutes above to mixing; obtain polymkeric substance water slurry; be distributed in a small amount of water nanometer silver is ultrasonic; the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry; stir on instillation limit, limit; after having instiled; add remaining water; continue sealing and stir more than 1.5 hours, obtain thus peelable antimicrobial protection slurries.
Peelable antimicrobial protection slurries are coated in to sample surfaces formation and film, then to filming, with reference to following standard, test.
With reference to GB/T21866-2008 method, anti-microbial property is tested;
With reference to ASTMD-3330, to rete, the sticking power at SUS304 stainless steel surface detects;
With reference to ASTMD3759, film stretching intensity and elongation are detected.Its result is as shown in the table.
Embodiment 5.
A kind of peelable antimicrobial protection slurries; described peelable antimicrobial protection slurries are comprised of according to parts by weight following component: 100 parts of organic silicon modified polyurethane emulsions, 1 part of Natvosol, 10 parts of Lauryl Alcohol esters, 0.5 part of polyether-modified polydimethylsiloxane, 1.5 parts of multi-amino silicones, 7 parts, 1 part of fluorine carbon wetting agent, 0.5 part of nano-silver powder, 30 parts of ethanol and water.
Organic silicon modified polyurethane emulsion, Natvosol, Lauryl Alcohol ester, polyether-modified polydimethylsiloxane, multi-amino silicone, ethanol and fluorine carbon wetting agent component are mixed; with 1000r/min sealing, disperse to stir 30 minutes above to mixing; obtain polymkeric substance water slurry; be distributed in a small amount of water nanometer silver is ultrasonic; the dispersion liquid of nanometer silver is instiled at a slow speed and added in polymkeric substance water slurry; stir on instillation limit, limit; after having instiled; add remaining water; continue sealing and stir more than 1.5 hours, obtain thus peelable antimicrobial protection slurries.
Peelable antimicrobial protection slurries are coated in to sample surfaces formation and film, then to filming, with reference to following standard, test.
With reference to GB/T21866-2008 standard, anti-microbial property is tested;
With reference to ASTMD-3330 standard, to rete, the sticking power at SUS304 stainless steel surface detects;
With reference to ASTMD3759 standard, rete tensile strength and elongation are detected.Its result is as shown in the table.
Project | Antibacterium performance | Antibacterium endurance quality | Sticking power | Tensile strength | Elongation | Peel off effect |
Numerical value | 99.99% | 99.92% | 0.46N/25mm | 6.3Mpa | 93% | Well |
Claims (8)
1. peelable antimicrobial protection slurries; it is characterized in that; according to the mass fraction, by following component, formed: 5~30 parts, 30~100 parts of modified polyurethane emulsions, 0~50 part of modified acrylate emulsion, 1~9 part of auxiliary rheological agents, 0~10 part of film coalescence aid, 0~3 part of wetting hand feeling agent, 0.001~0.5 part of nano-silver powder, 0~30 part of quick-drying solvent and water.
2. peelable antimicrobial protection slurries according to claim 1, is characterized in that, described modified polyurethane emulsion is: a kind of or its mixture in organic silicon modified polyurethane emulsion, organic fluorine modified polyurethane emulsion.
3. peelable antimicrobial protection slurries according to claim 1, is characterized in that, described modified acrylate emulsion is: a kind of or its mixture in organosilicon-modified acrylate emulsion, organic fluorine modified acrylate emulsion.
4. peelable antimicrobial protection slurries according to claim 1; it is characterized in that, described auxiliary rheological agents is: a kind of or its composition in Li-montmorillonite, hydrophobically modified propylene soda acid, hydrophobically modified ethoxylation urethane, hydrophobically modified polyether glycol, Natvosol, methyl hydroxyethylcellulose, Type 3U, methylhydroxypropylcellulose, methylcellulose gum, xanthan gum, aerosil.
5. peelable antimicrobial protection slurries according to claim 1; it is characterized in that, described film coalescence aid is: a kind of or its composition in Lauryl Alcohol ester, propylene glycol phenylate, dipropylene glycol methyl ether, propandiol butyl ether, dipropylene glycol butyl ether, dipropylene glycol propyl ether, glycol propyl ether, butyl glycol ether, Diethylene Glycol butyl ether, diethylene glycol ether, diethylene glycol dimethyl ether, triethylene glycol butyl ether, tri ethylene glycol ethyl ether, triethylene glycol methyl ether, tripropylene glycol butyl ether, ethylene glycol phenyl ether, diacetone alcohol, dipropylene glycol methyl ether acetic ester, dibutyl phthalate.
6. peelable antimicrobial protection slurries according to claim 1; it is characterized in that, described wetting hand feeling agent is: a kind of or its composition in multi-amino silicone, polysiloxane, polydimethylsiloxane, polyether-modified polydimethylsiloxane, phenmethyl modified dimethyl polysiloxane, polyoxyalkylene alkyl modification by copolymerization polydimethylsiloxane, amino modified polydimethylsiloxane, water-soluble silicon wax, alkyl-silicone oil, aminophenyl silicone oil, fluorinated alkyl sulfonate, fluorine carbon wetting agent.
7. peelable antimicrobial protection slurries according to claim 1, is characterized in that, described quick-drying solvent is: a kind of or its mixture in ethanol, acetone.
8. the preparation method of peelable antimicrobial protection slurries claimed in claim 1; it is characterized in that; by modified polyurethane emulsion, modification acrylate breast, auxiliary rheological agents; film coalescence aid, wetting hand feeling agent mix; dispersed with stirring; obtain polymkeric substance water slurry; be distributed in a small amount of water nano-silver powder is ultrasonic; the dispersion liquid of nano-silver powder is instiled at a slow speed and added in polymkeric substance water slurry; stir on instillation limit, limit, after having instiled, adds remaining water; continue sealing and stir, obtain thus peelable antimicrobial protection slurries.
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CN104530806A (en) * | 2014-12-19 | 2015-04-22 | 江南大学 | Preparation method and application of high-golss and high-leveling-property water-based coating additive |
CN106381690A (en) * | 2016-09-08 | 2017-02-08 | 东北林业大学 | Method for preparing high-strength antibacterial oil-water separation type material through cold plasma pretreatment |
CN107083170A (en) * | 2017-06-02 | 2017-08-22 | 青岛光辉彩饰有限公司 | A kind of water paint and its preparation and application method |
CN108841306A (en) * | 2018-05-04 | 2018-11-20 | 广州市鼎茂新材料科技有限公司 | A kind of aqueous printing table coating and preparation method thereof |
CN111253845A (en) * | 2020-03-09 | 2020-06-09 | 广东四维新材料有限公司 | Nano-silver antibacterial spray-formed protective film and preparation method thereof |
CN111607272A (en) * | 2020-06-12 | 2020-09-01 | 四川星波科技有限公司 | Bactericidal membrane with bactericidal function and preparation process and application thereof |
CN115537106A (en) * | 2022-09-23 | 2022-12-30 | 中华制漆(深圳)有限公司 | Water-based hand-feeling rubber coating and using method thereof |
CN116656201A (en) * | 2023-06-07 | 2023-08-29 | 苏州热工研究院有限公司 | Anti-contamination film composition for nuclear power plant, preparation method thereof and anti-contamination film for nuclear power plant |
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Cited By (11)
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CN104530806A (en) * | 2014-12-19 | 2015-04-22 | 江南大学 | Preparation method and application of high-golss and high-leveling-property water-based coating additive |
CN106381690A (en) * | 2016-09-08 | 2017-02-08 | 东北林业大学 | Method for preparing high-strength antibacterial oil-water separation type material through cold plasma pretreatment |
CN107083170A (en) * | 2017-06-02 | 2017-08-22 | 青岛光辉彩饰有限公司 | A kind of water paint and its preparation and application method |
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CN108841306A (en) * | 2018-05-04 | 2018-11-20 | 广州市鼎茂新材料科技有限公司 | A kind of aqueous printing table coating and preparation method thereof |
CN111253845A (en) * | 2020-03-09 | 2020-06-09 | 广东四维新材料有限公司 | Nano-silver antibacterial spray-formed protective film and preparation method thereof |
CN111607272A (en) * | 2020-06-12 | 2020-09-01 | 四川星波科技有限公司 | Bactericidal membrane with bactericidal function and preparation process and application thereof |
CN115537106A (en) * | 2022-09-23 | 2022-12-30 | 中华制漆(深圳)有限公司 | Water-based hand-feeling rubber coating and using method thereof |
CN115537106B (en) * | 2022-09-23 | 2024-02-09 | 中华制漆(深圳)有限公司 | Water-based hand feeling rubber coating and application method thereof |
CN116656201A (en) * | 2023-06-07 | 2023-08-29 | 苏州热工研究院有限公司 | Anti-contamination film composition for nuclear power plant, preparation method thereof and anti-contamination film for nuclear power plant |
CN116656201B (en) * | 2023-06-07 | 2023-11-28 | 苏州热工研究院有限公司 | Anti-contamination film composition for nuclear power plant, preparation method thereof and anti-contamination film for nuclear power plant |
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