CN103668764A - Nylon lace and preparation method thereof - Google Patents
Nylon lace and preparation method thereof Download PDFInfo
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- CN103668764A CN103668764A CN201310671893.8A CN201310671893A CN103668764A CN 103668764 A CN103668764 A CN 103668764A CN 201310671893 A CN201310671893 A CN 201310671893A CN 103668764 A CN103668764 A CN 103668764A
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Abstract
The invention relates to nylon lace and a preparation method of the nylon lace. The nylon lace is of a two-layer composite structure, and a surface layer is arranged on a bottom layer. The surface layer is made of cation polyester fibers, the bottom layer is made of spandex fibers and polyamide fibers, and the mass ratio of the spandex fibers to the polyamide fibers is one to thirty. The preparation method includes the steps that the nylon lace is formed by weaving the spandex fibers, the polyamide fibers and the cation polyester fibers through a lace machine, and after weaving is completed, the warp knitted nylon lace is obtained through a dyeing after treatment procedure. The nylon lace is simple in process and easy to popularize.
Description
[technical field]
The present invention relates to lace technical field, specifically, is a kind of roses and lace and preparation method thereof.
[background technology]
Roses and lace is a kind of thing from abroad, is the earliest by the hand-knitted eyelet stitch of crochet hook.
Roses and lace generally all can appear at clothes, underwear, above household textile.Roses and lace is thin, stereovision is strong.The underwear in summer is common to be the theme with roses and lace.Roses and lace on clothes can produce a kind of sweet sensation especially.The roses and lace that family is spun is that household increases a kind of beyond thought sensation.Increased the household textile of roses and lace, for household textile has increased stereovision.The household textile of multiple roses and lace design can reach sweet sensation, likes the beauty of Japanese sensation, and textiles that can DIY roses and lace, for oneself Wo Ju produces the sensation of oneself liking.We also often can see that some curtain, the tablecloth can incorporate this design, in summer, use, and can build a kind of refrigerant sensation to household.
The lace of China is started late, before the eighties in last century, the machine of weaving lace is mainly from foreign import, phase at the beginning of the nineties in last century, Guangzhou and Zhejiang one band have absorbed the feature of external machine, in conjunction with domestic actual conditions, independent research China's First lace machine, and the Yi Ge lace factory by Shenzhen is as test unit. the problem of China's lace machinery requirement import that is from then on through with.
And to after 2000, lace is produced just progressively from mechanical chain piece knitted lace machine to the transition of computer lace machine.The appearance of computer lace machine, makes again lace industry occur the variation of revolution.It overcomes chain piece knitted lace machine complicated production technique, is tending towards adopting advanced computer to control, and strengthens automated production scale, save time, and the usefulness of raising.
[summary of the invention]
The object of the invention is to overcome the deficiencies in the prior art, a kind of roses and lace and preparation method thereof is provided.
The object of the invention is to be achieved through the following technical solutions:
A roses and lace, is two layer composite structure, is provided with top layer on bottom; The material on described top layer is CATION terylene fiber; The material of described bottom is spandex fibre and nylon fibre, and the mass ratio of spandex fibre and nylon fibre is 1: 30.
Described top layer be shaped as various geometric figures, such as flower, bird, insect, and fish, and personalized design configuration.
A roses and lace, its concrete preparation method is: adopt spandex fibre and nylon fibre, and two kinds of raw materials of CATION terylene fiber form through the braiding of lace machine, after having weaved, through dyeing finishing process, obtain through compiling roses and lace.
Described nylon fibre, is cut into slices and modification capsule forms by nylon-6, and wherein, the mass fraction that modification capsule accounts for nylon fibre is 0.1～2%; By two kinds of raw material melt-spun methods, be prepared from.
Described nylon-6 can be replaced by nylon-66.
A preparation method for modification capsule, its concrete steps are:
(1) pretreatment of raw material:
Tea grounds is dried to 2 hours at 50 ℃, obtains processing rear tea grounds;
(2) charing is processed:
Tea grounds after the processing that step (1) is obtained, then carries out charing simultaneously, then obtains modification powder;
Described charring process is for adopting quartz tube furnace to carry out segmentation charing: the heating rate with 8 ℃/min rises to 200 ℃, tea grounds is charing 100min at 200 ℃, then the heating rate with 16 ℃/min rises to 400 ℃, again at 400 ℃ of charing 100min, finally the heating rate with 24 ℃/min rises to 600 ℃, and 2～3h is processed in charing at this temperature; After charing, obtained product is ground at high energy ball mill, until fine-powdered obtains modification powder, the particle diameter of modification powder is 0.1～0.5 μ m; Adopt low-temperature carbonization, save on the one hand cost, keep on the one hand in addition the original function of tea charcoal, can be used as the carrier performance tea charcoal effect of absorption, the excess Temperature of charing and long, will destroy original performance of tea charcoal, advantage and the strong point of Here it is low-temperature carbonization; This is also the reason that does not adopt high temperature carbonization.
(3) aging modification:
Step (2) modification powder is carried out to aging modification, obtain composite powder;
The modification powder that step (2) is obtained is dissolved in strong acid solution, and the solution of the modification powder obtaining adds functional material and aging dose, stir again and ultrasonic dispersion, then centrifugation obtains solid material, and solid material is dried to 1～3 hour at 30～50 ℃, obtains composite powder;
Described functional material is nano boron carbide powder and nano indium tin metal oxide; The mass ratio of the two is 1: 2～1: 6, is preferably 1: 4;
The mass ratio of described functional material and aging dose is 3: 1;
Described strong acid is the concentrated sulfuric acid, red fuming nitric acid (RFNA), hydrofluoric acid or other.
The described addition of aging dose is 1～5% of modification powder mass fraction;
Described aging dose is antioxidant, ultraviolet absorber and light stabilizer, and three's mass ratio is 1: 1: 1;
Described antioxidant is commercially available prod, such as antioxidant 1010 and irgasfos 168;
Described ultraviolet absorber is the ultraviolet absorber of hydroxyl, such as ESCALOL 567, and Octabenzone, the materials such as 2,4-DihydroxyBenzophenone; For commercially available prod;
Described light stabilizer is the light stabilizer of hydroxyl, such as O-hydroxyl-diphenyl ketone, and 2-(2 ', 4 '-dihydroxy phenyl)-5, the materials such as 6-dihydroxy benzo triazole and 1,6-dihydroxy benzo triazole; For commercially available prod;
The aging modification of this step has 2 effects, be that physical absorption and valence bond cooperation are used, after tea powder and nano material acidifying, its surface forms hydrogen bond, and carry out chemical strong closing with the hydroxyl of aging dose, moreover utilize the space of modification powder and nano material self more, carry out the suction-operated of a physics.
(4) modification capsule
By sandwich layer be composite powder to be wrapped in cystoblast be chitosan material the inside, make the modification capsule containing composite powder; Wherein, the Thickness Ratio of cystoblast and sandwich layer is 1: 18; The diameter of function reagent is 0.4～4 μ m;
Modification capsule adopts complex coacervation synthetic, also can adopt interfacial polymerization or situ aggregation method, is ripe technology.
The diameter of modification capsule is 0.4～4 μ m, and it is conducive to capsule smoothly by spinneret orifice, and guarantees that the combination of capsule and fiber is firm, can't affect the mechanical performance of fiber;
Capsule/the core of modification capsule is greater than 1: 15 than generally, guarantees that microcapsules have certain mechanical strength and heat resistance;
The effect of modification capsule is, plays the effect of slow release nano functional particle, is conducive to its nanometer effect and is able to permanent maintenance; The preparation that its nanometer effect is better than conventional master batch type functional particles is used further to the technique effect of spinning;
Compared with prior art, good effect of the present invention is:
(1) technique of the present invention is simple, is easy to promote;
(2) nano indium tin metal oxide, has good electric conductivity and the transparency, can cut off harmful electron radiation, ultraviolet ray and far infrared;
(3) the present invention adopts the nano boron carbide powder that plasma arc gas chemistry synthetic method is produced, and its purity is high, particle diameter is little, be evenly distributed, and specific area is large, high surface, and apparent density is low; Nanoscale carbonization boron powder has stable physics and chemistry character, nonmagnetic, resistance to strong acid, resistance to highly basic; Be added on material, be beneficial to extend the service life of material;
(4) the present invention will carry out modification after composite powder and nano material mixing, can make like this nano material be more prone to be dispersed in the space of composite powder, the carrier the inside of nano material absorption composite powder, make its effect be able to permanent maintenance, be conducive to bring into play the special role of nano material, effect is significantly higher than direct employing nano material and adds the technique effect that carries out spinning.
[specific embodiment]
The specific embodiment of a kind of roses and lace of the present invention and preparation method thereof is below provided.
Embodiment 1
A roses and lace, is two layer composite structure, is provided with top layer on bottom; The material on described top layer is CATION terylene fiber; The material of described bottom is spandex fibre and nylon fibre, and the mass ratio of spandex fibre and nylon fibre is 1: 30.
Described top layer be shaped as various geometric figures, such as flower, bird, insect, and fish, and personalized design configuration.
A roses and lace, its concrete preparation method is: adopt spandex fibre and nylon fibre, and two kinds of raw materials of CATION terylene fiber form through the braiding of lace machine, after having weaved, through dyeing finishing process, obtain through compiling roses and lace.
Described nylon fibre, is cut into slices and modification capsule forms by nylon-6, and wherein, the mass fraction that modification capsule accounts for nylon fibre is 0.3%; By two kinds of raw material melt-spun methods, be prepared from.
A preparation method for modification capsule, its concrete steps are:
(1) pretreatment of raw material:
Tea grounds is dried to 2 hours at 50 ℃, obtains processing rear tea grounds;
(2) charing is processed:
Tea grounds after the processing that step (1) is obtained, then carries out charing simultaneously, then obtains modification powder;
Described charring process is for adopting quartz tube furnace to carry out segmentation charing: the heating rate with 8 ℃/min rises to 200 ℃, tea grounds is charing 100min at 200 ℃, then the heating rate with 16 ℃/min rises to 400 ℃, again at 400 ℃ of charing 100min, finally the heating rate with 24 ℃/min rises to 600 ℃, and 2～3h is processed in charing at this temperature; After charing, obtained product is ground at high energy ball mill, until fine-powdered obtains modification powder, the particle diameter of modification powder is 0.1～0.5 μ m; Adopt low-temperature carbonization, save on the one hand cost, keep on the one hand in addition the original function of tea charcoal, can be used as the carrier performance tea charcoal effect of absorption, the excess Temperature of charing and long, will destroy original performance of tea charcoal, advantage and the strong point of Here it is low-temperature carbonization; This is also the reason that does not adopt high temperature carbonization.
(3) aging modification:
The modification powder that step (2) is obtained is dissolved in strong acid solution, and the solution of the modification powder obtaining adds functional material and aging dose, stir again and ultrasonic dispersion, then centrifugation obtains solid material, and solid material is dried to 1～3 hour at 30～50 ℃, obtains composite powder;
Described functional material is nano boron carbide powder and nano indium tin metal oxide; The mass ratio of the two is 1: 2;
The mass ratio of described functional material and aging dose is 3: 1;
Described strong acid is the concentrated sulfuric acid, red fuming nitric acid (RFNA), hydrofluoric acid or other.
The described addition of aging dose is 1.5% of modification powder mass fraction;
Described aging dose is antioxidant, ultraviolet absorber and light stabilizer, and three's mass ratio is 1: 1: 1;
Described antioxidant is commercially available prod, such as antioxidant 1010 and irgasfos 168;
Described ultraviolet absorber is the ultraviolet absorber of hydroxyl, such as ESCALOL 567, and Octabenzone, the materials such as 2,4-DihydroxyBenzophenone; For commercially available prod;
Described light stabilizer is the light stabilizer of hydroxyl, such as O-hydroxyl-diphenyl ketone, and 2-(2 ', 4 '-dihydroxy phenyl)-5, the materials such as 6-dihydroxy benzo triazole and 1,6-dihydroxy benzo triazole; For commercially available prod;
The aging modification of this step has 2 effects, be that physical absorption and valence bond cooperation are used, after tea powder and nano material acidifying, its surface forms hydrogen bond, and carry out chemical strong closing with the hydroxyl of aging dose, moreover utilize the space of modification powder and nano material self more, carry out the suction-operated of a physics.
(4) modification capsule
By sandwich layer be composite powder to be wrapped in cystoblast be chitosan material the inside, make the modification capsule containing composite powder; Wherein, the Thickness Ratio of cystoblast and sandwich layer is 1: 18; The diameter of function reagent is 0.4～4 μ m;
Modification capsule adopts complex coacervation synthetic, also can adopt interfacial polymerization or situ aggregation method, is ripe technology.
The diameter of modification capsule is 0.4～4 μ m, and it is conducive to capsule smoothly by spinneret orifice, and guarantees that the combination of capsule and fiber is firm, can't affect the mechanical performance of fiber;
Capsule/the core of modification capsule is greater than 1: 15 than generally, guarantees that microcapsules have certain mechanical strength and heat resistance;
The effect of modification capsule is, plays the effect of slow release nano functional particle, is conducive to its nanometer effect and is able to permanent maintenance; The preparation that its nanometer effect is better than conventional master batch type functional particles is used further to the technique effect of spinning;
The nylon-6 of the present embodiment can be replaced by nylon-66, and other is constant.
Embodiment 2
A roses and lace, is two layer composite structure, is provided with top layer on bottom; The material on described top layer is CATION terylene fiber; The material of described bottom is spandex fibre and nylon fibre, and the mass ratio of spandex fibre and nylon fibre is 1: 30.
Described top layer be shaped as various geometric figures, such as flower, bird, insect, and fish, and personalized design configuration.
A roses and lace, its concrete preparation method is: adopt spandex fibre and nylon fibre, and two kinds of raw materials of CATION terylene fiber form through the braiding of lace machine, after having weaved, through dyeing finishing process, obtain through compiling roses and lace.
Described nylon fibre, is cut into slices and modification capsule forms by nylon-6, and wherein, the mass fraction that modification capsule accounts for nylon fibre is 0.8%; By two kinds of raw material melt-spun methods, be prepared from.
A preparation method for modification capsule, its concrete steps are:
(1) pretreatment of raw material:
Tea grounds is dried to 2 hours at 50 ℃, obtains processing rear tea grounds;
(2) charing is processed:
Tea grounds after the processing that step (1) is obtained, then carries out charing simultaneously, then obtains modification powder;
(3) aging modification:
The modification powder that step (2) is obtained is dissolved in strong acid solution, and the solution of the modification powder obtaining adds functional material and aging dose, stir again and ultrasonic dispersion, then centrifugation obtains solid material, and solid material is dried to 1～3 hour at 30～50 ℃, obtains composite powder;
Described functional material is nano boron carbide powder and nano indium tin metal oxide; The mass ratio of the two is 1: 4;
The mass ratio of described functional material and aging dose is 3: 1;
Described strong acid is the concentrated sulfuric acid, red fuming nitric acid (RFNA), hydrofluoric acid or other.
The described addition of aging dose is 2.8% of modification powder mass fraction;
Described aging dose is antioxidant, ultraviolet absorber and light stabilizer, and three's mass ratio is 1: 1: 1;
(4) modification capsule
By sandwich layer be composite powder to be wrapped in cystoblast be chitosan material the inside, make the modification capsule containing composite powder; Wherein, the Thickness Ratio of cystoblast and sandwich layer is 1: 18; The diameter of function reagent is 0.4～4 μ m.
The nylon-6 of the present embodiment can be replaced by nylon-66, and other is constant.
Embodiment 3
A roses and lace, is two layer composite structure, is provided with top layer on bottom; The material on described top layer is CATION terylene fiber; The material of described bottom is spandex fibre and nylon fibre, and the mass ratio of spandex fibre and nylon fibre is 1: 30.
Described top layer be shaped as various geometric figures, such as flower, bird, insect, and fish, and personalized design configuration.
A roses and lace, its concrete preparation method is: adopt spandex fibre and nylon fibre, and two kinds of raw materials of CATION terylene fiber form through the braiding of lace machine, after having weaved, through dyeing finishing process, obtain through compiling roses and lace.
Described nylon fibre, is cut into slices and modification capsule forms by nylon-6, and wherein, the mass fraction that modification capsule accounts for nylon fibre is 1.8%; By two kinds of raw material melt-spun methods, be prepared from.
A preparation method for modification capsule, its concrete steps are:
(1) pretreatment of raw material:
Tea grounds is dried to 2 hours at 50 ℃, obtains processing rear tea grounds;
(2) charing is processed:
Tea grounds after the processing that step (1) is obtained, then carries out charing simultaneously, then obtains modification powder;
Described charring process is with embodiment 1;
(3) aging modification:
The modification powder that step (2) is obtained is dissolved in strong acid solution, and the solution of the modification powder obtaining adds functional material and aging dose, stir again and ultrasonic dispersion, then centrifugation obtains solid material, and solid material is dried to 1～3 hour at 30～50 ℃, obtains composite powder;
Described functional material is nano boron carbide powder and nano indium tin metal oxide; The mass ratio of the two is 1: 6;
The mass ratio of described functional material and aging dose is 3: 1;
Described strong acid is the concentrated sulfuric acid, red fuming nitric acid (RFNA), hydrofluoric acid or other.
The described addition of aging dose is 4.5% of modification powder mass fraction;
Described aging dose is antioxidant, ultraviolet absorber and light stabilizer, and three's mass ratio is 1: 1: 1;
(4) modification capsule
By sandwich layer be composite powder to be wrapped in cystoblast be chitosan material the inside, make the modification capsule containing composite powder; Wherein, the Thickness Ratio of cystoblast and sandwich layer is 1: 18; The diameter of function reagent is 0.4～4 μ m.
The nylon-6 of the present embodiment can be replaced by nylon-66, and other is constant.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, without departing from the inventive concept of the premise; can also make some improvements and modifications, these improvements and modifications also should be considered within the scope of protection of the present invention.
Claims (10)
1. a roses and lace, is characterized in that, is two layer composite structure, is provided with top layer on bottom; The material on described top layer is CATION terylene fiber; The material of described bottom is spandex fibre and nylon fibre, and the mass ratio of spandex fibre and nylon fibre is 1: 30.
2. a kind of roses and lace as claimed in claim 1, is characterized in that, described top layer be shaped as various geometric figures.
3. a roses and lace, its concrete preparation method is: adopt spandex fibre and nylon fibre, and two kinds of raw materials of CATION terylene fiber form through the braiding of lace machine, after having weaved, through dyeing finishing process, obtain through compiling roses and lace.
4. a kind of roses and lace as claimed in claim 1, is characterized in that, described nylon fibre is cut into slices and modification capsule forms by nylon-6, and wherein, the mass fraction that modification capsule accounts for nylon fibre is 0.1～2%; By two kinds of raw material melt-spun methods, be prepared from.
5. a kind of roses and lace as claimed in claim 4, is characterized in that, the preparation method of described modification capsule, and its concrete steps are:
(1) pretreatment of raw material:
Tea grounds is dried to 2 hours at 50 ℃, obtains processing rear tea grounds;
(2) charing is processed:
Tea grounds after the processing that step (1) is obtained, then carries out charing simultaneously, then obtains modification powder;
(3) aging modification:
Step (2) modification powder is carried out to aging modification, obtain composite powder;
(4) modification capsule
By sandwich layer be composite powder to be wrapped in cystoblast be chitosan material the inside, make the modification capsule containing composite powder.
6. a kind of roses and lace as claimed in claim 5, it is characterized in that, in described step (2), described charring process is for adopting quartz tube furnace to carry out segmentation charing: the heating rate with 8 ℃/min rises to 200 ℃, tea grounds is charing 100min at 200 ℃, and then the heating rate with 16 ℃/min rises to 400 ℃, then at 400 ℃ of charing 100min, finally the heating rate with 24 ℃/min rises to 600 ℃, and 2～3h is processed in charing at this temperature; After charing, obtained product is ground at high energy ball mill, until fine-powdered obtains modification powder.
7. a kind of roses and lace as claimed in claim 5, it is characterized in that, in described step (3), the modification powder that step (2) is obtained is dissolved in strong acid solution, and the solution of the modification powder obtaining adds functional material and aging dose, stir again and ultrasonic dispersion, then centrifugation obtains solid material, and solid material is dried to 1～3 hour at 30～50 ℃, obtains composite powder.
8. a kind of roses and lace as claimed in claim 7, is characterized in that, described functional material is nano boron carbide powder and nano indium tin metal oxide; The mass ratio of the two is 1: 2～1: 6, is preferably 1: 4.
9. a kind of roses and lace as claimed in claim 7, is characterized in that, the mass ratio of described functional material and aging dose is 3: 1; The described addition of aging dose is 1～5% of modification powder mass fraction.
10. a kind of roses and lace as claimed in claim 4, is characterized in that, the described cystoblast of modification capsule and the Thickness Ratio of sandwich layer are 1: 18; The diameter of modification capsule is 0.4～4 μ m.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310671893.8A CN103668764A (en) | 2013-12-11 | 2013-12-11 | Nylon lace and preparation method thereof |
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| CN201310671893.8A CN103668764A (en) | 2013-12-11 | 2013-12-11 | Nylon lace and preparation method thereof |
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| CN103668764A true CN103668764A (en) | 2014-03-26 |
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| CN201310671893.8A Pending CN103668764A (en) | 2013-12-11 | 2013-12-11 | Nylon lace and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104060392A (en) * | 2014-06-17 | 2014-09-24 | 福建省百凯经编实业有限公司 | Production method for nylon lace |
| CN104894860A (en) * | 2015-06-23 | 2015-09-09 | 南通市安博纺织品有限公司 | Aromatic lace fabric |
| CN105063887A (en) * | 2015-08-03 | 2015-11-18 | 安徽创荣服装辅料有限公司 | Multifunctional garment lace and processing method thereof |
| CN105951262A (en) * | 2016-06-16 | 2016-09-21 | 东莞市联洲知识产权运营管理有限公司 | Anti-pilling anti-snagging lace fabric and making method thereof |
| CN106012272A (en) * | 2016-06-28 | 2016-10-12 | 宏达高科控股股份有限公司 | Making method of warp-knitted material showing gradient-color due to stretching |
| CN106174727A (en) * | 2016-09-22 | 2016-12-07 | 袁惠芬 | A kind of bra ring for fixing and preparation method thereof |
| CN106498617A (en) * | 2015-09-07 | 2017-03-15 | 宫城花边株式会社 | Lace fabric and the method for weaving of lace fabric |
| CN111013506A (en) * | 2019-12-30 | 2020-04-17 | 杭州传化精细化工有限公司 | Microcapsule emulsion of micromolecular anti-aging agent with degradable capsule wall and preparation method and application thereof |
| CN118029038A (en) * | 2024-02-02 | 2024-05-14 | 广东启悦未来科技股份有限公司 | Soft skin-friendly lace fabric and preparation method thereof |
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2013
- 2013-12-11 CN CN201310671893.8A patent/CN103668764A/en active Pending
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104060392B (en) * | 2014-06-17 | 2015-07-08 | 福建省百凯经编实业有限公司 | Production method for nylon lace |
| CN104060392A (en) * | 2014-06-17 | 2014-09-24 | 福建省百凯经编实业有限公司 | Production method for nylon lace |
| CN104894860A (en) * | 2015-06-23 | 2015-09-09 | 南通市安博纺织品有限公司 | Aromatic lace fabric |
| CN105063887A (en) * | 2015-08-03 | 2015-11-18 | 安徽创荣服装辅料有限公司 | Multifunctional garment lace and processing method thereof |
| CN106498617B (en) * | 2015-09-07 | 2020-03-31 | 宫城花边株式会社 | Lace fabric and weaving method thereof |
| CN106498617A (en) * | 2015-09-07 | 2017-03-15 | 宫城花边株式会社 | Lace fabric and the method for weaving of lace fabric |
| CN105951262A (en) * | 2016-06-16 | 2016-09-21 | 东莞市联洲知识产权运营管理有限公司 | Anti-pilling anti-snagging lace fabric and making method thereof |
| CN106012272A (en) * | 2016-06-28 | 2016-10-12 | 宏达高科控股股份有限公司 | Making method of warp-knitted material showing gradient-color due to stretching |
| CN106012272B (en) * | 2016-06-28 | 2017-09-29 | 宏达高科控股股份有限公司 | A kind of stretching preparation method of the gradient color through woven material |
| CN106174727A (en) * | 2016-09-22 | 2016-12-07 | 袁惠芬 | A kind of bra ring for fixing and preparation method thereof |
| CN106174727B (en) * | 2016-09-22 | 2017-12-01 | 袁惠芬 | A kind of brassiere retainer plate |
| CN111013506A (en) * | 2019-12-30 | 2020-04-17 | 杭州传化精细化工有限公司 | Microcapsule emulsion of micromolecular anti-aging agent with degradable capsule wall and preparation method and application thereof |
| CN111013506B (en) * | 2019-12-30 | 2022-04-19 | 杭州传化精细化工有限公司 | Microcapsule emulsion of micromolecular anti-aging agent with degradable capsule wall and preparation method and application thereof |
| CN118029038A (en) * | 2024-02-02 | 2024-05-14 | 广东启悦未来科技股份有限公司 | Soft skin-friendly lace fabric and preparation method thereof |
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Application publication date: 20140326 |