CN103666892A - Low density sponge-shaped cleaning solid and preparation method thereof - Google Patents
Low density sponge-shaped cleaning solid and preparation method thereof Download PDFInfo
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- CN103666892A CN103666892A CN201310730112.8A CN201310730112A CN103666892A CN 103666892 A CN103666892 A CN 103666892A CN 201310730112 A CN201310730112 A CN 201310730112A CN 103666892 A CN103666892 A CN 103666892A
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Abstract
The invention relates to the technical field of the processing of household chemical toiletries and discloses a low density sponge-shaped cleaning solid and a preparation method thereof. The solid comprises the following components by weight percentage: 40-100 percent of foaming solid substance and 0-60 percent of additives. The low density sponge-shaped cleaning solid is a novel cleaning product form and has a wide application range. By foaming solid raw materials and adding additives with different functions, products meeting different requirements and in different application fields can be prepared for daily clothes washing, kitchen cleaning, automobile cleaning or body and face washing and protection of personal nurse supplies, the use is very convenient and quick, even if the size of the solid is very small, worrying about that the solid falls into the water bottom to cause waste is still not required, as a result, resources are better utilized, and the environment is better protected.
Description
Technical field
The present invention relates to daily-use chemical industry washing product technology manufacture field, be specifically related to clean solid of a kind of low-density sponge shape and preparation method thereof.
Background technology
Soap is that the mankind use articles for washing with the longest history, so far the history of existing thousands of years.In a broad sense, grease, wax or lipid acid etc. and bases play the soap of saponification or neutralization reaction gained, all can be described as soap.Soap is divided into hard soap conventionally, soft soap and superfatted soap.Yet, be no matter that the soap of which kind of type is solid-type in the market.General in the larger place of the darker volume of water, solid-type soap can sink to the bottom, is difficult for picking up, and when the long-pending hour easier landing of soap body, to use, makes troubles especially, more causes waste.
Summary of the invention
The present invention is directed to problems of the prior art, provide a kind of preparation technology simple, can be at cavernous body shape solid of floating on water and preparation method thereof when retaining the clean power of soap body.
In order to solve the problems of the technologies described above, the present invention is solved by following technical proposals:
Low-density sponge shape cleans a solid, the component that described solid contains following weight percent:
Foaming solid matter 40 ~ 100%;
Additive 0 ~ 60%.
As preferably, described foaming solid matter is for the soap base by fat saponification or have one or more in the curing Zoomeric acid sodium of certain foaming power temperature influence, coconut oil sodium, cocounut oil acyl sodium isethionate.
As preferably, described spongy clean solid foamed power meets foam (40 ℃)/mm >=20, solidification value >=35 ℃ according to the mensuration of GB/T13173.11-2008 washing composition foaming power.
As preferably, described additive is one or more in deionized water, mild surfactants, activeconstituents, essence, pigment, solid particulate.
As preferably, the preparation method of the described clean solid of low-density sponge shape, method is as follows:
Described foaming solid matter is heated to 35 ~ 80 ℃, after thawing completely, passes into gas, it is fully mixed with gas, gas enters in the liquid of thawing, foaming and intumescing; Measure density, reach 0.3 ~ 0.8 and stop foaming, at once, in impouring mould, make it to solidify rapidly; Cavernous body after solidifying, through ventilating, be dried and standing 1-3 week, obtains finished product.
1. particularly, when passing into normal air, its method is as follows: above-mentioned foaming solid matter is heated to 35 ~ 80 ℃, when needs add thermally sensitive additive, the liquid of fusing need remain on 60 ℃ of following or its molten states more than zero pour, then melt liquid is moved in the agitator kettle than the large 2-9 of its volume times, temperature remains on 35 ~ 60 ℃ or its more than zero pour, imposes fast homogeneous, make and air mixed, air enters in melt liquid, makes to expand, and capacity increases.With glass cylinder, contained one glass of liquid, with specific gravity hydrometer, measured density, reached 0.3 ~ 0.8 and can stop stirring, at once, in impouring mould, made it to solidify rapidly.
2. particularly, when passing into pressurized gas, its method is as follows: above-mentioned foaming solid matter is heated to 35 ~ 80 ℃, and when needs add thermally sensitive additive, the liquid of fusing need remain on 60 ℃ of following or its molten states more than zero pour, then melt liquid is moved in heat-preserving equipment, temperature remains on 35 ~ 60 ℃ or its molten state more than zero pour, then passes into pressurized gas, and pressurized gas expands rapidly,, gas-liquid mixed is bubbled naturally.With glass cylinder, contained one glass and liquid, with specific gravity hydrometer, measured density, reached 0.3 ~ 0.8 and can stop stirring, at once, in impouring mould, made it to solidify rapidly.
As preferably, the stir speed (S.S.) in described fast homogeneous process is 2000 ~ 4500rpm/min.Fusing fluid is fully mixed with gas, and gas enters in liquid, makes to expand, and has increased capacity.The excessive cavernous body of the too large foaming of rotating speed is relatively crisp, and rotating speed is too little is unfavorable for that gas enters fusing fluid, can affect the flotation property of cavernous body.
As preferably, the pressurized gas passing in described preparation method is any one or several in normal air, carbonic acid gas, nitrogen, nitrogen dioxide gas.
The present invention, owing to having adopted above technical scheme, has significant technique effect:
A kind of spongy clean solid the present invention relates to, is a kind of novel cleaning product form, and has wide range of applications.By foaming solid material and the additive that adds various difference in functionalitys, can prepare the product of various different demands and Application Areas, as can be used for washing of health in daily washing clothes, kitchen cleaning, car cleaning or personal care articles, face etc. and protect.
The present invention can meet common requirement for cleaning, can prepare the personal care articles with powerful property again, because cavernous body has floating characteristic, use more portable, have more interest, even if also needn't worry when volume is very little that the landing bottom causes waste, make resource obtain better utilised, more environmental protection.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail:
The measuring method of the gas content the present invention relates to is as follows:
First the liquid having melted is got in right amount with glass cylinder, with specific gravity hydrometer, recording soap lye density is ρ 1, and the cavernous body liquid having foamed is got in right amount with glass cylinder, claims to such an extent that quality is M
2, with specific gravity hydrometer, recording soap lye density is ρ 2, by formula, records cavernous body volume V2=M2/ ρ 2, can calculate that former fusing fluid volume is V3=M2/ ρ 1, the gas content of cavernous body=(V2-V3)/V2*100%.
embodiment 1
Low-density sponge shape cleans a solid, the component of following weight percent, consists of:
Soap base 88%;
Cocounut oil acyl glycine potassium 10%;
Herba Lysimachiae foenumgraeci quintessence oil 2%.
Soap base is cut into sheet and puts into reactor, be heated to 60 ~ 70 ℃, low rate mixing (350 ~ 400rpm/min) is complete to soap base fusing; Then be cooled to 50 ℃, add cocounut oil acyl glycine potassium and Herba Lysimachiae foenumgraeci quintessence oil to mix, keep constant temperature.The good soap lye of above-mentioned melting is poured into than in the reactor of large 6 times of soap lye volume, keep 50 ℃ ~ 55 ℃ of constant temperature, open homogeneous (3500 ~ 4000rpm/min), make air constantly enter soap lye, when soap lye volume is increased to original 2 ~ 3 times, with glass cylinder, take out, proportion instrumentation density, the density of survey is 0.55, be that gas content is 54%, stop stirring, at once, in impouring mould, make it to solidify rapidly.Cavernous body after solidifying is sent in the drying shed of ventilation installation after taking out, and standing 1 ~ 3 week, allows its seasoning.Cavernous body state homogeneous after solidifying, when its shape is symmetrical, floating steady; When it is shaped as asymmetric body, floating deflection to some extent, but do not affect floating performance.
The clean power of spongy clean solid is evaluated with foaming power and detersive power two aspects, foaming power is according to the mensuration of GB/T13173.11-2008 washing composition foaming power, and the ability that detersive power deposits by washing composition detersive power and anti-stain according to GBT 13174-2003 dress material is again measured.
The spongy clean solid cleaning power performance evaluation of table 1 embodiment 1
| Project | Foam (40 ℃)/mm | Detersive power |
| Common soap | 50 | (detersive power >=standard of two kinds of soiled cottons is divided detersive power to II level |
| Low-density sponge shape cleans solid | 60 | (detersive power >=standard of two kinds of soiled cottons is divided detersive power to II level |
embodiment 2
Low-density sponge shape cleans a solid, the component of following weight percent, consists of:
Zoomeric acid sodium 25%;
Coconut oil sodium 20%;
Sodium lauroyl glutamate 15%;
Deionized water 23%;
Glycerine 15%;
Herba Lysimachiae foenumgraeci quintessence oil 2%.
Zoomeric acid sodium, coconut oil sodium, sodium lauroyl glutamate, deionized water and glycerine are added to reactor, be heated to 60-70 ℃, stir fusing completely.Then be cooled to 50 ℃, add Herba Lysimachiae foenumgraeci quintessence oil to mix, keep 50 ℃ ~ 55 ℃ of constant temperature, the liquid that above-mentioned melting is good connects injector mixer, the injector the other end passes into carbonic acid gas compression gas, gets the cavernous body liquid ejecting in right amount, proportion instrumentation density with glass cylinder, record density 0.65, gas content is 46%.At once spray and fill with mould, make it to solidify rapidly.Cavernous body after solidifying is sent in the drying shed of ventilation installation after taking out, and standing 1 ~ 3 week, allows its seasoning.
The continuous shape of table 2 embodiment 2 cleans solid cleaning power performance evaluation
| Project | Foam (40 ℃)/mm | Detersive power |
| Common soap | 50 | (detersive power >=standard of two kinds of soiled cottons is divided detersive power to II level |
| Low-density sponge shape cleans solid | 55 | (detersive power >=standard of two kinds of soiled cottons is divided detersive power to II level |
In a word, the foregoing is only preferred embodiment of the present invention, all equalizations of doing according to the present patent application the scope of the claims change and modify, and all should belong to the covering scope of patent of the present invention.
Claims (9)
1. low-density sponge shape cleans a solid, it is characterized in that the component that described solid contains following weight percent:
Foaming solid matter 40 ~ 100%;
Additive 0 ~ 60%.
2. the clean solid of low-density sponge shape according to claim 1, is characterized in that: described foaming solid matter is for the soap base by fat saponification or have one or more in the curing Zoomeric acid sodium of certain foaming power temperature influence, coconut oil sodium, cocounut oil acyl sodium isethionate.
3. the clean solid of low-density sponge shape according to claim 1, is characterized in that: described spongy clean solid foamed power meets foam (40 ℃)/mm >=20, solidification value >=35 ℃ according to the mensuration of GB/T13173.11-2008 washing composition foaming power.
4. the clean solid of low-density sponge shape according to claim 1, is characterized in that: described additive is one or more in deionized water, mild surfactants, activeconstituents, essence, pigment, solid particulate.
5. according to the preparation method of the clean solid of the arbitrary described low-density sponge shape of claim 1-4, it is characterized in that, method is as follows:
Described foaming solid matter is heated to 35 ~ 80 ℃, after thawing completely, passes into gas, it is fully mixed with gas, gas enters in the liquid of thawing, foaming and intumescing; Measure density, reach 0.3 ~ 0.8 and stop foaming, at once, in impouring mould, make it to solidify rapidly; Cavernous body after solidifying, through ventilating, be dried and standing 1-3 week, obtains finished product.
6. low-density sponge shape according to claim 5 cleans the preparation method of solid, it is characterized in that: described foaming solid matter moves in agitator kettle after melting completely, pass into normal air, temperature remains on 35 ~ 60 ℃ or its molten state more than zero pour, impose fast homogeneous, it is fully mixed with air, and air enters in liquid, foaming and intumescing.
7. the preparation method of the clean solid of low-density sponge shape according to claim 6, is characterized in that: the stir speed (S.S.) in described fast homogeneous process is 2000 ~ 4500rpm/min.
8. low-density sponge shape according to claim 5 cleans the preparation method of solid, it is characterized in that: described foaming solid matter moves in heat-preserving equipment after melting completely, passes into pressurized gas, and temperature remains on 35 ~ 60 ℃, pressurized gas expands rapidly, and liquid is bubbled naturally.
9. the preparation method of the clean solid of low-density sponge shape according to claim 8, is characterized in that: the pressurized gas passing in described preparation method is any one or several in normal air, carbonic acid gas, nitrogen, nitrogen dioxide gas.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310730112.8A CN103666892A (en) | 2013-12-26 | 2013-12-26 | Low density sponge-shaped cleaning solid and preparation method thereof |
| TW103114646A TW201524446A (en) | 2013-12-26 | 2014-04-23 | Low density sponge-shaped cleaning solid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310730112.8A CN103666892A (en) | 2013-12-26 | 2013-12-26 | Low density sponge-shaped cleaning solid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103666892A true CN103666892A (en) | 2014-03-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310730112.8A Pending CN103666892A (en) | 2013-12-26 | 2013-12-26 | Low density sponge-shaped cleaning solid and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN103666892A (en) |
| TW (1) | TW201524446A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN109234085A (en) * | 2018-08-16 | 2019-01-18 | 惠州兆婷化妆品有限公司 | A kind of floating soap and preparation method thereof |
| CN109589279A (en) * | 2019-01-08 | 2019-04-09 | 明辉实业（深圳）有限公司 | A kind of solid shampoo and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073204A (en) * | 1991-12-11 | 1993-06-16 | 刘汉生 | The manufacture method of soap floating on water |
| CN1501972A (en) * | 2001-04-10 | 2004-06-02 | Low density detergent bar composition | |
| CN101287822A (en) * | 2005-10-12 | 2008-10-15 | 西姆莱斯有限责任两合公司 | Floating complex soap and mixture for producing said floating complex soap |
| CN101659912A (en) * | 2008-08-28 | 2010-03-03 | 北京玉佳明三态离子科学研究院有限公司 | Composite ion-exchange type broad-spectrum disinfection-sterilization tourist soap |
| CN102888303A (en) * | 2011-07-18 | 2013-01-23 | 孟凡丽 | Whitening floating soap |
| CN103361203A (en) * | 2012-03-30 | 2013-10-23 | 李雪娇 | Floating toilet soap |
-
2013
- 2013-12-26 CN CN201310730112.8A patent/CN103666892A/en active Pending
-
2014
- 2014-04-23 TW TW103114646A patent/TW201524446A/en unknown
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073204A (en) * | 1991-12-11 | 1993-06-16 | 刘汉生 | The manufacture method of soap floating on water |
| CN1501972A (en) * | 2001-04-10 | 2004-06-02 | Low density detergent bar composition | |
| CN101287822A (en) * | 2005-10-12 | 2008-10-15 | 西姆莱斯有限责任两合公司 | Floating complex soap and mixture for producing said floating complex soap |
| CN101659912A (en) * | 2008-08-28 | 2010-03-03 | 北京玉佳明三态离子科学研究院有限公司 | Composite ion-exchange type broad-spectrum disinfection-sterilization tourist soap |
| CN102888303A (en) * | 2011-07-18 | 2013-01-23 | 孟凡丽 | Whitening floating soap |
| CN103361203A (en) * | 2012-03-30 | 2013-10-23 | 李雪娇 | Floating toilet soap |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN109234085A (en) * | 2018-08-16 | 2019-01-18 | 惠州兆婷化妆品有限公司 | A kind of floating soap and preparation method thereof |
| CN109234085B (en) * | 2018-08-16 | 2020-08-25 | 惠州兆婷化妆品有限公司 | Floating soap and preparation method thereof |
| CN109589279A (en) * | 2019-01-08 | 2019-04-09 | 明辉实业（深圳）有限公司 | A kind of solid shampoo and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201524446A (en) | 2015-07-01 |
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Application publication date: 20140326 |